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Volumn 9, Issue 12, 2009, Pages 5021-5023

Cocrystal controlled solid-state synthesis of a thermally stable nicotinate analogue that sustains an isostructural series of porous metal-organic materials

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EID: 75349108236     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg9013366     Document Type: Article
Times cited : (22)

References (59)
  • 50
    • 75349105022 scopus 로고    scopus 로고
    • int = 0.0219), final il indices I > 2a(I)\. Rl = 0.0353, wR2 = 0.0715
    • int = 0.0219), final il indices [I > 2a(I)\. Rl = 0.0353, wR2 = 0.0715.
  • 52
    • 75349104678 scopus 로고    scopus 로고
    • int = 0.0516), final R indices [I > 2a(I)]: Rl = 0.0576, wR2 = 0.1621. Synthesis of 2-4: A DMF solution (30 mL) containing HTriNA (268 mg, 1.0 mmol) was heated to 120 deg C until dissolved, at which point 0.5 mmol of metal nitrate hydrates predissolved in 5 mL of DMF was added. Reaction times lasted for 1-5
    • int = 0.0516), final R indices [I > 2a(I)]: Rl = 0.0576, wR2 = 0.1621. Synthesis of 2-4: A DMF solution (30 mL) containing HTriNA (268 mg, 1.0 mmol) was heated to 120 deg C until dissolved, at which point 0.5 mmol of metal nitrate hydrates predissolved in 5 mL of DMF was added. Reaction times lasted for 1-5 h.
  • 59
    • 75349084763 scopus 로고    scopus 로고
    • Structures 2-4 were assumed equal to 1 except the metals were exchanged and recalculated to determine surface area and pore size
    • (b) Structures 2-4 were assumed equal to 1 except the metals were exchanged and recalculated to determine surface area and pore size.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.