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int = 0.0219), final il indices I > 2a(I)\. Rl = 0.0353, wR2 = 0.0715
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int = 0.0219), final il indices [I > 2a(I)\. Rl = 0.0353, wR2 = 0.0715.
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int = 0.0516), final R indices [I > 2a(I)]: Rl = 0.0576, wR2 = 0.1621. Synthesis of 2-4: A DMF solution (30 mL) containing HTriNA (268 mg, 1.0 mmol) was heated to 120 deg C until dissolved, at which point 0.5 mmol of metal nitrate hydrates predissolved in 5 mL of DMF was added. Reaction times lasted for 1-5
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int = 0.0516), final R indices [I > 2a(I)]: Rl = 0.0576, wR2 = 0.1621. Synthesis of 2-4: A DMF solution (30 mL) containing HTriNA (268 mg, 1.0 mmol) was heated to 120 deg C until dissolved, at which point 0.5 mmol of metal nitrate hydrates predissolved in 5 mL of DMF was added. Reaction times lasted for 1-5 h.
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Structures 2-4 were assumed equal to 1 except the metals were exchanged and recalculated to determine surface area and pore size
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