Development and validation of a stability-indicating RP-UPLC method for the quantitative analysis of sparfloxacin

Journal of Chromatographic Science

Volumn 48, Issue 1, 2010, Pages 1-6

  Gupta, Himanshu ^a   Aqil, M ^a   Khar, R K ^a   Ali, Asgar ^a   Sharma, Aarti ^b   Chander, Prakash ^c  

^a HAMDARD UNIVERSITY   (India)

^b RANBAXY RESEARCH LABORATORIES   (India)

^c CSC India Pvt Ltd   (India)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 74349124940     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/48.1.1     Document Type: Article

References (20)

1. A.D. Jerkovich, J.S. Mellors, and J.W. Jorgenson. The use of micrometer-sized particles in ultrahigh pressure liquid chromatography. LC-GC 21: 600 (2003).
2. V.G. Dongre, P.P. Karmuse, P.P. Rao, and A. Kumar. Development and validation of UPLC method for determination of primaquine phosphate and its impurities. J. Pharm. Biomed. Anal. 46(3): 236-242 (2008).
3. R. Plumb, J.C. Perez, J. Granger, I. Beattie, K. Joncour, and A. Wright, Ultra-performance liquid chromatography coupled to quadrupole-orthogonal time-offlight mass spectrometry. J. Rapid Commun. Mass Spectrom. 18: 2331-2337 (2004).
4. S.A.C. Wren and P. Tchlitcheff. Use of ultra-performance liquid chromatography in pharmaceutical development. J. Chromatogr. A 1119: 140 (2006)
5. S.A.C. Wren and P. Tchlitcheff. UPLC/MS for the identification of β-blockers. J. Pharm. Biomed. Anal. 40: 571-580 (2006).
6. R. Li, L. Dong, and J. Huang. Ultra-performance liquid chromatography-tandem mass spectrometry for the determination of epirubicin in human plasma. Anal. Chim. Acta 546: 167-173 (2005).
7. Sweetman S (Ed), Martindale: The Complete Drug Reference, London: Pharmaceutical Press. Electronic version, 2009.
8. L.D. Ming, F. Zhe, Q. JinLi, and J.P. Wang. Determination of sparfloxacin in human urine by reversed-phase high performance liquid chromatography with nitrous acid and hydroiodic pre-column derivatization. Chin. Chem. Lett. 12: 1007-1010 (2000).
9. K. Borner, E. Borner, and H. Lode. Determination of sparfloxacin in serum and urine by high performance liquid chromatography. J. Chromatogr. 579: 285-289 (1992).
10. M. Kamberi, P. Kamberi, N. Hajime, N. Uemura, K. Nakamura, and S. Nakano. Simultaneous determination of grepofloxacin, ciprofloxacin and theophylline in human plasma and urine by HPLC. Ther. Drug Monit. 21: 411 (1999).
11. D.J. Lyon, S.W. Cheung, C.Y. Chan, and A.F.B. Cheng. Rapid HPLC assay of clinafloxacin, fleroxacin, levofloxacin, sparfloxacin and tosufloxacin. J.Antimicrob. Chemother. 34: 446-448 (1994).
12. D.H. Wright, V.K. Herman, F.N. Konstantinides, and J.C. Rotschafer. Determination of quinolone antibiotics in growth media by reversed-phase high-performance liquid chromatography. J. Chromatogr. B Biomed. Sci. Appl. 709: 97-104 (1998).
13. H. R. N. Marona, J.A.S. Zuanazzib, and E.E.S. Schapoval. Determination of sparfloxacin and its degradation products by HPLC-PDA. J. Antimicrob. Chemother. 44: 301-302 (1999).
14. H.R.N. Marona and E.E.S. Schapova. A high-performance liquid chromatographic assay fpr sparfloxacin. J. Pharm. Biomed. Anal. 20: 413-417 (1999).
15. H.R.N. Marona and E.E.S. Schapoval. Spectrophotometric determination ofsparfloxacin in pharmaceutical formulations using bromothymol blue. J. Pharm. Biomed. Anal. 26: 501-504 (2001).
16. Text on Validation of analytical procedures, international conference on harmonization, September 1993.
17. Proceedings of the International Conference on Harmonization of Technical Requirements of Registration of Pharmaceuticals for Human Use (ICH Harmonized Tripartite Guidelines). Validation of Analytical Procedures: Methodology, ICH-Q2B, Geneva, 1996.
18. Q2 (R1) ICH guidelines, Validation of Analytical Procedures: Text and Methodology.
19. Proceedings of the International Conference on Harmonization of Technical Requirements of Registration of Pharmaceuticals for Human Use. Validation of Analytical Procedures, ICH-Q2A, Geneva, 1995.
20. Center for Drug Evaluation and Research, Reviewers Guidance, Validation of Chromatographic Methods, 1994.