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39
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74149083271
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note
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2 (0.106 g, 0.32 mmol) was added and the reactants were maintained for an additional 2 h before being cooled. Methanol (30 ml) was added to attain the precipitate (pale yellow color), which was carefully washed with methanol and ether before vacuum drying.
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41
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74149088896
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note
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1H NMR and IR spectral data.
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