NMR study of polyacrylamide tacticity synthesized by precipitated polymerization method

Iranian Polymer Journal (English Edition)

Volumn 18, Issue 12, 2009, Pages 947-956

  Ziaee, Farshid ^a   Bouhendi, Hosein ^a   Ziaie, Farhood ^b  

^a IRAN POLYMER AND PETROCHEMICAL INSTITUTE   (Iran)

^b AGRICULTURAL MEDICAL AND INDUSTRIAL RESEARCH SCHOOL   (Iran)

Author keywords

Microstructure; NMR; Polyacrylamide; Precipitated polymerization; Tacticity

Indexed keywords

ATACTIC; CARBONYL CARBON; ETHYL ACETATES; EXPERIMENTAL DATA; HETERONUCLEAR MULTIPLE QUANTUM COHERENCES; ISOTACTICS; MARKOV STATISTICS; METHINE; METHINE GROUP; METHINE PROTONS; MOLAR RATIO; NMR; NMR SPECTROSCOPY; NMR STUDIES; POLYACRY LAMIDE; POLYMERIZATION METHOD; PRECIPITATED POLYMERIZATION; ROOM TEMPERATURE; STATISTICS MODEL; SYNDIOTACTICS; TACTICITIES;

DEUTERIUM; ESTERS; ETHANOL; FREE RADICAL POLYMERIZATION; HEAVY WATER; MICROSTRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PROBABILITY DENSITY FUNCTION; QUANTUM THEORY; RESONANCE;

NUCLEAR MAGNETIC RESONANCE;

EID: 73849101117     PISSN: 10261265     EISSN: 10261265     Source Type: Journal    
DOI: None     Document Type: Article

References (39)

1. Guyot A, Precipitation Polymerization. in: Comprehensive Polymer Science, 1st ed, Pergamon, London, 4, 261-273, 1989.
2. Guyot A, Precipitation Polymerization. in: Polymeric Material Encyclopedia, 1st ed, CRC, Boca Raton, 9, 7228-7238, 1996.
3. Bouhendi H, Haddadi-Asl V, Rafizadeh M, Effect of non-solvent type and purification process on precipitation polymerization of acrylic acid in organic media, Iran Polym J, 18, 777-787, 2009.
4. Nakano T, Okamoto Y, In Controlled Radical Polymerization, ACS Symp Ser, 685, 451-462, 1998.
5. Yuki H, Hatada K, Stereospecific polymerization of alpha-substituted acrylic acid esters polymerization, Adv Polym Sci, 31, 1-45, 1979.
6. Hatada K, Kitayama T, Ute K, Stereoregular polymerization of α-substituted acrylates, Prog Polym Sci, 13, 189-276, 1988.
7. Habaue S, Okamoto Y, Stereocontrol in radical polymerization, Chem Rec, 1, 46-52, 2001.
8. Porter NA, Allen TR, Breyer RA, Chiral auxiliary control of tacticity in free radical polymerization, J Am Chem Soc, 114, 7676-7683, 1992.
9. Nakano T, Mori M, Okamoto Y, Stereospecific radical polymerization of 1-phenyldibenzosuberyl methacrylate affording a highly isotactic polymer, Macromolecules, 26, 867-868, 1993.
10. Yamada K, Nakano T, Okamoto Y, Stereospecific polymerization of vinyl acetate in fluoroalcohols. Synthesis of syndiotactic poly (vinyl alcohol), Proc Jpn Acad, 74B, 46-49, 1998.
11. Gibbons O, Carrol WM, Aldabbagh F, Nitroxiide-mediated controlled statistical copolymerizations of N-isopropylacrylamide with N-tert-butylacry-lamide, J Polym Sci A Polym Chem, 44, 6410-6418, 2006.
12. Benoit D, Harth E, Fox P, Accurate structural control and block formation in the living polymerization of 1,3-dienes by nitroxide-mediated procedures, Macromolecules, 33, 363-370, 2000.
13. Matyjaszewski K, Atom transfer radical polymerization, Chem Rev, 101, 2921-2990, 2001.
14. Xiao Q, Zhang X, Yi1 J, Wang X, Zhang H, Synthesis of poly(ethylene oxide)-b-polystyrene-b-poly(4-vinylpyridine) ABC triblock copolymers by two-step atom transfer radical polymerization, Iran Polym J, 17, 781-790, 2008.
15. Semsarzadeh MA, Rostami-Daronkola MR, 1H NMR Studies of the molecular structure of PVAc-b-(MA-co-MMA) block terpolymer in atom transfer radical copolymerization reaction, Iran Polym J, 16, 47-54, 2007.
16. McCormick CL, Lowe AB, Aqueous RAFT polymerization: recent developments in synthesis of functional water-soluble (co)polymers with controlled structures, Acc Chem Res, 37, 312-325, 2004.
17. Barner L, Davis TP, Stenzel MH, Barner-Kowollik C, Complex macromolecular architectures by reversible addition fragmentation chain transfer chemistry: theory and practice, Macromol Rapid Commun, 28, 539-559, 2007.
18. Kamigaito M, Ando T, Sawamoto M, Metal catalyzed living radical polymerization, Chem Rev, 101, 3689-3746, 2001.
19. Wang JS, Matyjaszewski K, Controlled / "living" radical polymerization. Atom transfer radical polymerization in the presence of transition-metal complexes, J Am Chem Soc, 117, 5614-5615, 1995.
20. Kato M, Kamigaito M, Sawamoto M, Higashimura T, Polymerization of methyl methacrylate with the carbon tetrachloride/dichlorotris - (triphenylphosphine) ruthenium(II)/ methylaluminum bis(2, 6-di-tert-butylphenoxide) initiating system: possibility of living radical polymerization, Macromolecules, 28, 1721-1723, 1995.
21. Chiefari J, Rizzardo E, Thang SH, Living free-radical polymerization by reversible addition fragmentation chain transfer: the RAFT process, Macromolecules, 31, 5559-5562, 1998.
22. Georges MK, Veregin RP, Kazmaier PM, Narrow molecular weight by a free-radical polymerization process, Macromolecules, 26, 2987-2990, 1993.
23. Jiang J, Lu X, Lu Y, Stereospecific preparation of polyacrylamide with low polydispersity by ATRP in the presence of Lewis acid, Polymer, 49, 1770-1776, 2008.
24. Elvira C, Roman JS, Synthesis and stereochemistry of isomeric methacrylic polymers derived from 4 - and 5 -aminosalicylic acids, Polymer, 38, 4743-4750, 1997.
25. Sanda F, Nakamura M, Endo T, Syntheses and radical polymerization behavior of novel optically active methacrylamides having (L)-leucine structure in the side chains, J Polym Sci A Polym Chem, 36, 2681-2690, 1998.
26. Zhang JZ, Liu W, Nakano T, Okamoto Y, Stereospecific radical polymerization of N-methyl methacrylamide, Polym J, 32, 694-699, 2000.
27. Liu W, Nakano T, Okamoto Y, Stereocontrol in radical polymerization of N,N-dimethylacry-lamide and N,N-diphenylacrylamide and thermal properties of syndiotactic poly(methyl acrylate)s derived from the obtained polymers, Polym J, 32, 771-777, 2000.
28. Lancaster JE, O'Conner MN, High field 13C NMR study of the stereoregularity of polyacrylamide, J Polym Sci Polym Let Edn, 20, 547-550, 1982.
29. Cais RE, Stuk GJ, Copolymerization of acrylamide with sulphur dioxide. Determination of the effect of copolymerization temperature on the monomer sequence distribution by 13C NMR, Polymer, 19, 179-187, 1978.
30. Bovey FA, Tiers GVD, Polymer NMR spectroscopy. IX. Polyacrylamide and poly-methacrylamide in aqueous solution, J Polym Sci A Polym Chem, 1, 849-861, 1963.
31. Isobe Y, Fujioka D, Habaue S, Okamoto Y, Efficient Lewis acid-catalyzed stereocontrolled radical polymerization of acrylamide, J Am Chem Soc, 123, 7180-7181, 2001.
32. Su X, Zhao Z, Li H, Li X, Wu P, Han Z, Stereocontrol during photo-initiated controlled/living radical polymerization of acrylamide in the presence of Lewis acids, Eur Polym J, 44, 1849-1856, 2008.
33. Habaue S, Isobe Y, Okamoto Y, Stereocontrol radical polymerization of acrylamides and methacry-lamides using Lewis acids, Tetrahedron, 58, 8205-8209, 2002.
34. Bovey F, Nuclear Magnetic Resonance Spectroscopy, 2nd ed, Bell Telephone Laboratories, Academic, London, 1988.
35. Tonelli AE, NMR Spectroscopy and Polymer Microstructure: The Conformational Connection, 1st ed, AT & T Bell Laboratories, VCH, New York, 1989.
36. Pham QT, Petiaud R, Watson H, Darricades MFL, Proton and Carbon NMR Spectra of Polymers, 4th ed, Penton, London, 1991.
37. Randall JC, Polymer Sequence Determination Carbon-13C NMR Method, 1st ed, Academic, London, 1977.
38. Hikichi K, Ikura M, Yasuda M, Two-dimensional 1H and 13C nuclear magnetic resonance studies of poly(acrylamide), Polym J, 20, 851-859, 1988.
39. Ziaee F, Nekoomanesh M, Salehi-Mobarake H, Arabi H, The effect of temperature on tacticity for bulk thermal polymerization of styrene, e-Polymers, No. 041, 2008.