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Volumn 64, Issue 11-12, 2009, Pages 1639-1652

Stereoselective synthesis of bromopiperidinones and their conversion to annulated heterocycles

Author keywords

Bromopiperidinones; Glycosylamines; Stereoselective mannich reactions; Stereoselective michael addition; Thiazolopiperidinones

Indexed keywords

ADDITION REACTIONS; CONDENSATION REACTIONS; STEREOCHEMISTRY;

BROMOPIPERIDINONES; GLYCOSYLAMINES; MANNICH REACTIONS; MICHAEL ADDITIONS; THIAZOLOPIPERIDINONES;

STEREOSELECTIVITY;

EID: 73849092217 PISSN: 09320776 EISSN: None Source Type: Journal
DOI: 10.1515/znb-2009-11-1251 Document Type: Article

Times cited : (4)

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- Crystal structure data of 10e: mol weight, 787.16 gmol -1, crystal size: 0.10 × 0.30 × 0.30 mm3, orthorhombic space group P212121, lattice parameters: a, 50.241 (13, b, 14.959 (2, c, 11.0402 (15) Å, V, 8298 (3) Å, Z, 8, F(000, 3312 e, T, 80 °C, Dcalcd, 1.26 gcm -3, μ(MoKα, 2.4 mm-1. Enraf-Nonius Turbo-CAD4 diffractometer, MoKα radiation, graphite monochromator, number of reflections: measured: 11586, independent: 11538, observed: 8204 with |F| ≥ 4.0σ(F, discrepancy factors: wR2, 0.1881 (R1, 0.064 for all observed reflections, 0.1043 for all reflections, x(Flack, 0.02, Δρfin max/min, 1.03, 0.60 eÅ. CCDC 745336 contains the supplementary crystallographic data for this paper. Thes
- ρfin (max/min) = 1.03 / -0.60 eÅ. CCDC 745336 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data- request/cif.

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