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Volumn 48, Issue 23, 2009, Pages 10898-10900

Three-dimensional frameworks of cubic (NH4)5Ga 4SbS10, (NH4)4Ga4SbS 9(OH) · H2O, and (NH4) 3Ga4SbS9(OH2) · 2H 2O

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Indexed keywords

EID: 72949123083 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic901927r Document Type: Article

Times cited : (37)

References (34)

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- Compound 1 was synthesized hydrothermally in a 23 mL Teflon-lined autoclave using Ga, Sb, and S (1.0 mmol Ga, 1.0 mmol Sb, 10 mmol S) and a 6 mL 50% mixture of NH4OH (30% in water) and triethylamine (TEA, 30% in water) at 160 °C for one week. There are at least three phases within the system that can be identified: Sb2S3, NH 4Sb5S8, and (NH4)5Ga 4SbS10 (1, Dark red crystals of 1 were removed manually and used for further analyses, NH4)4Ga 4SbS9(OH) · H2O (2a) and(NH 4)3Ga4SbS9(OH2) · 2H2O (2b) were synthesized hydrothermally using 8 mm o.d. pyrex tubes, to which was added Ga2S3, Sb2S 3, S 0.4 mmol Ga2S3,0.1 mmol Sb 2S3, 0.9 mmol S, and 0.3 mL of NH
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30
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- Pore sizes calculated by removing the atoms and calculating the void space in the crystal structure using PLATON software. See the Supporting Information
- Pore sizes calculated by removing the atoms and calculating the void space in the crystal structure using PLATON software. See the Supporting Information.

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- See the Supporting Information
- See the Supporting Information.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.