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Cell parameters measured for three different preparations confirmed this.
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72949088285
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note
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2) =0.2373 for 12035 reflections with I>20(1). CCDC 740338 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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