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-1, KBr): 3418 (s), 2074 (s), 2043 (s), 1601 (s), 1543 (w), 1418 (m), 1221 (w), 1066 (w), 1012 (w), 846 (s), 814 (w), 725 (w).
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11
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72249109440
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note
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3) were collected on a Bruker SMART APEX CCD diffractometer using graphite-monochromatized Mo Kα radiation (λ = 0.71073 Å) at room temperature using the ω-scan technique. Data reductions and absorption corrections were performed with the saint and sadabs software packages, respectively. The structures were solved by direct methods using the shelxs-97 program and were further refined by the full-matrix least-squares technique using the shelxl-97 program. All non-hydrogen atoms were refined with anisotropic displacement parameters. Hydrogen atoms were generated geometrically with assigned isotropic thermal parameters.
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