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Volumn 51, Issue 4, 2010, Pages 672-675

Synthesis and structures of heterasumanenes having different heteroatom functionalities

Author keywords

[No Author keywords available]

Indexed keywords

FLUORENE DERIVATIVE; HETERASUMANENE DERIVATIVE; LITHIUM DERIVATIVE; SILANE DERIVATIVE; TRIMETHYLSILYL DERIVATIVE; UNCLASSIFIED DRUG;

EID: 72149116182     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2009.11.102     Document Type: Article
Times cited : (61)

References (33)
  • 18
    • 70349916476 scopus 로고    scopus 로고
    • Very recently, trisilasumanene has been synthesized and characterized, see
    • Very recently, trisilasumanene has been synthesized and characterized, see: Furukawa, S.; Kobayashi, J.; Kawashima, T. J. Am. Chem. Soc. 2009, 131, 14192.
    • (2009) J. Am. Chem. Soc , vol.131 , pp. 14192
    • Furukawa, S.1    Kobayashi, J.2    Kawashima, T.3
  • 22
    • 72149131625 scopus 로고    scopus 로고
    • note
    • Experimental details, see Supplementary data.
  • 23
    • 72149116096 scopus 로고    scopus 로고
    • note
    • When 10 equiv of butyllithium were used for lithiation of 4, the reaction became complicated, probably because lithiation at more than two bay areas occurred.
  • 24
    • 72149123543 scopus 로고    scopus 로고
    • note
    • The structural details and the properties of 8 will appear elsewhere. CCDC 745674 contains the Supplementary data for this compound. These data can be obtained free of charge at www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; fax: (internat.) +44-1223/336-033; Email: deposit@ccdc.cam.ac.uk).
  • 25
    • 72149123821 scopus 로고    scopus 로고
    • note
    • Although the yield of 8 was slightly higher than that of 6, we think that the difference is within errors in integrations of the NMR spectroscopic analysis.
  • 27
    • 72149110513 scopus 로고    scopus 로고
    • note
    • 4: 598.2397. Found: 598.2396.
  • 28
    • 72149129070 scopus 로고    scopus 로고
    • note
    • 2 = 0.249 (for all reflections) for 8667 reflections and 393 parameters, GOF = 1.021. CCDC 745675 contains the Supplementary data for this compound. These data can be obtained free of charge at www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; fax: (internat.) +44-1223/336-033; Email: deposit@ccdc.cam.ac.uk).
  • 33
    • 72149127291 scopus 로고    scopus 로고
    • gaussian 03, Revision E.01; Gaussian: Wallingford, CT, 2004.
    • gaussian 03, Revision E.01; Gaussian: Wallingford, CT, 2004.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.