Synthesis of Wiberg's tetrasilatetrahedrane (tBu3Si) 4Si4 by a one-pot procedure

Organometallics

Volumn 28, Issue 23, 2009, Pages 6835-6837

  Frank, Meyer Wegner ^a   Scholz, Stefan ^a   Sänger, Inge ^a   Schödel, Frauke ^a   Bolte, Michael ^a   Wagner, Matthias ^a   Lerner, Hans Wolfram ^a  

^a GOETHE UNIVERSITY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ONE POT; ONE-POT PROCEDURES; ONE-POT SYNTHESIS; RECRYSTALLIZATIONS;

BENZENE; MOLECULES; SILANES; SINGLE CRYSTALS; SODIUM;

SILICON;

EID: 71949113651     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om900763y     Document Type: Article

References (23)

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17. 3 : Klinkhammer, K. W. Thesis, University of Stuttgart, Germany, 1998.
18. 3] results in the formation of the tetrasilatetrahedrane 1; see ref 12.
19. Structural details: CCDC 744853.
20. Lerner, H.-W.; Scholz, S.; Bolte, M. Organometallics 2002, 21, 3827.
21. Structural details: CCDC 744852.
22. 29Si) 36.1): Meyer-Wegner, F.; Nadj, A.; Tüllmann, S.; Bolte, M.; Holthausen, M. C.; Wagner, M.; Lerner, H.-W. Unpublished results.
23. 29Si NMR spectrum.