Synthesis and characterization of Al13-oxalate gel with Keggin structure

Chinese Journal of Geochemistry

Volumn 28, Issue 4, 2009, Pages 364-368

  Liu, Jing ^a,b   Zhao, Fenghua ^b  

^a SOUTHWEST UNIVERSITY OF SCIENCE AND TECHNOLOGY   (China)

^b CHINA UNIVERSITY OF MINING AND TECHNOLOGY   (China)

Author keywords

Al13; Gel; Keggin structure; Oxalate

Indexed keywords

CHARACTERISTIC PEAKS; CHEMICAL FORMULAE; DIFFRACTION PEAKS; FTIR; KEGGIN STRUCTURE; NATURAL ENVIRONMENTS; OXALATE COMPLEXES; OXALATE PRECIPITATION; SOLID STATE NMR; STRETCH VIBRATIONS; SYNTHESIS AND CHARACTERIZATION; XRD;

FOURIER TRANSFORM INFRARED SPECTROSCOPY; GELS; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION; X RAY DIFFRACTION ANALYSIS;

ALUMINUM;

ALUMINUM; FTIR SPECTROSCOPY; GEL; MAS; NUCLEAR MAGNETIC RESONANCE; OXALATE; PH; X-RAY DIFFRACTION;

EID: 70749119419     PISSN: 10009426     EISSN: None     Source Type: Journal    
DOI: 10.1007/s11631-009-0364-7     Document Type: Article

References (23)

1. Bertsch P.M. and Paker D.R. (1996) Aqueous polynuclear aluminum species. In The Environmental Chemistry of Aluminum (second edition) (ed. Spositio G.) [M]. pp.117-168. CRC Press Inc. Florida in America.
2. S.M. Bradley R.A. Kydd R.F. Howe 1993 The structure of Al gels formed through the base hydrolysis of Al3+ aqueous solutions [J] Journal of Colloid and Interface Science. 159 405 412 10.1006/jcis.1993.1340
3. W.H. Casey 2006 Large aqueous aluminum hydroxide molecules [J] Chemical Reviews. 106 1 16 10.1021/cr040095d (Pubitemid 43159620)
4. A.D. Cristofaro J.Z. He D.H. Zhou, et al. 2000 Adsorption of phosphate and tartrate on hydroxy-aluminum-oxalate precipitates [J] Soil Sci. Soc. Am. J. 64 1347 1355
5. J.J. Dynes P.M. Huang 1997 Influence of organic acids on selenite sorption by poorly ordered aluminum hydroxides [J] Soil Sci. Soc. Am. J. 61 772 783
6. G. Furrer B.L. Phillips K.U. Ulrich, et al. 2002 The origin of aluminum flocs in polluted streams [J] Science. 297 2245 2247 10.1126/science.1076505
7. J. Fujita A.E. Martell K. Nakamoto 1996 Infrared spectra of metal chelate compounds. IV. A normal coordinate treatment of oxalate metal complexes [J] J. Chem. Phys. 36 324 331 10.1063/1.1732504
8. 13 under simulated natural conditions [J] Geochimica et Cosmochimica Acta. 56 831 838 10.1016/0016-7037(92)90174-H
9. 13 polycation in natural soil solutions and surface waters[J] Applied Geochemistry. 16 513 529 10.1016/S0883-2927(00)00048-2
10. H. He J. Guo Xiexiande J. Peng 2000 Experimental study of the selective adsorption of heavy metals onto clay minerals [J] Chinese Journal of Geochemistry. 19 105 109 10.1007/BF03166865
11. Huang and Schniter (1986) Interactions of Soil Minerals With Natural Organics and Microbes [M]. pp. 159-221. Soil Science Society of America. Inc. Madison, Wisconsin in America.
12. D. Hunter D.S. Ross 1991 Evidence for a phytotoxic hydroxyaluminum polymer in organic soil horizons [J] Science. 251 1056 1058 10.1126/science.251. 4997.1056
13. G. Johansson 1960 On the crystal structure of some basic aluminum sulfates [J] Acta Chemica Scandinavica. 14 771 773 10.3891/acta.chem.scand.14- 0771
14. 13 species in environment [J] Advances in Earth Science. 22 85 92
15. 27Al NMR [J] Chinese Journal of Geochemistry. 28 61 69 10.1007/s11631-009-0061-6
16. A. Masion F. Thomas J.Y. Bottero, et al. 1994 Formation of amorphous precipitates from aluminum-organic ligands solutions: Macroscopic and molecular study [J] Journal of Non-crystalline solids. 171 191 200 10.1016/0022-3093(94) 90355-7
17. 13 polycation by organic ligands [J] Langmuir. 10 4353 4356 10.1021/la00023a069
18. S.L. Nail J.L. White S.L. Hem 1976 Structure of aluminum hydroxide gel. I: Initial precipitate [J] Journal of Pharmaceutical Science. 65 1188 1191 10.1002/jps.2600650814
19. R.L. Parfitt V.C. Farmer J.D. Russell 1997 Adsorption on hydrous oxides. I. Oxalate and benzoate on goethite [J] J. Soil Sci. 28 289 296 10.1111/j.1365-2389.1977.tb02237.x
20. D.R. Parker T.B. Kinraide L.W. Zelazny 1989 On the phytotoxicity of polynuclear hydroxyl-aluminum complexes [J] Soil Science Society of America Journal. 53 789 796
21. 30) molecule and aqueous solution [J] Geochimica et Cosmochimica Acta. 67 2725 2733 10.1016/S0016-7037(03)00108-X (Pubitemid 36965313)
22. M.P.B. Van Bruggen M. Donker H.N.W. Lekkerkerker, et al. 1999 Anomalous stability of aqueous boehmite dispersions induced by hydrolyzed aluminum poly-cations [J] Colloids and Surfaces. 150 115 128 10.1016/S0927-7757(98)00728- 6 (Pubitemid 29122005)
23. D. Wu G. Diao J. Peng 1998 Experimental study on the competitive adsorption of metal ions onto minerals [J] Chinese Journal of Geochemistry. 17 213 220 10.1007/BF02834596