메뉴 건너뛰기




Volumn 51, Issue 1, 2010, Pages 112-114

An indicator displacement assay with independent dual wavelength emission

Author keywords

[No Author keywords available]

Indexed keywords

BORONIC ACID DERIVATIVE; FLUORESCENT DYE; INDICATOR; METAL; SUGAR; SUGAR PHOSPHATE;

EID: 70649099201     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2009.10.097     Document Type: Article
Times cited : (11)

References (18)
  • 11
    • 0034674309 scopus 로고    scopus 로고
    • Britovsek, G. J. P, Mastroianni, S, Solan, G. A, Baugh, S. P. D, Redshaw, C, Gibson, V. C, White, A. J. P, Williams, D. J, Elsegood, M. R. J. Chem. Eur. J. 2000, 6, 2221-2231. 2,2′-Bipyridine-6-carbaldehyde (90 mg, 0.49 mmol) and 3-aminophenyl-boronic acid were added to ethanol (10 ml) in an oven-dried flask with condenser under N2. The solution was allowed for 1 h then ZnCl2 (0.49 ml, 1 M in ether, 0.49 mmol) was added, and then refluxed overnight. The solvent was removed in vacuo and methanol (5 ml) was added. The solution was allowed to reflux for 10 min then the solvent was removed by centrifugation and decantation. The process was repeated twice to yield compound 3 as a yellow solid powder. Mp 290 °C (decomposed, 1H NMR (300 MHz, CD3OD/CD3CN (1:1, δ 8.96 (d, J, 2.8 Hz, 1H, 8.87 (s, 1H, 8.64 (d, J, 7.7 Hz, 1H, 8.48 (d, J, 8.0 Hz, 2H, 8.10-8.25 (m, 3H, 7.93 (d, J, 6.9Hz, 1H, 7.78-7.80 m, 1H
    • +, calculated: 459.973980, observed: 459.972848.
  • 15
    • 70649091590 scopus 로고    scopus 로고
    • note
    • Compound 4 was prepared in a fashion identical to compound 3 starting with 4-bromo-aniline.
  • 17
    • 0004187703 scopus 로고
    • John Wiley and Sons, New York pp 175-177
    • Connors K.A. Binding Constants (1987), John Wiley and Sons, New York pp 175-177
    • (1987) Binding Constants
    • Connors, K.A.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.