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38
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70649108262
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-
note
-
2: C, 16.98; N{cyrillic}, 2.14; Cl, 25.04; Se, 55.84. Found: C, 17.23; N{cyrillic}, 2.29; Cl, 24.54; Se, 56.38.
-
-
-
-
39
-
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70649109176
-
-
note
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2: C, 12.92; H, 1.63; Br, 42.98; Se, 42.47. Found: C, 13.10; H, 1.78; Br, 42.78; Se, 42.22.
-
-
-
-
40
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70649113334
-
-
note
-
2Se), 49.24 (SeCHCl).
-
-
-
-
41
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70649111755
-
-
note
-
2Se), 38.21 (SeCHBr). The amount of the minor diastereomer of diselenane 9 was too low to make assignment possible. The mixture was filtered, and the solvent was distilled in vacuo. NMR analysis showed that the residue (3.93 g) contained diselenolane 7 (the purity was about 95%, the yield was virtually quantitative). The cis/trans isomer ratio was 2:1.
-
-
-
-
43
-
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70649114018
-
-
note
-
2: C, 19.49; N{cyrillic}, 2.04; Cl, 14.39. Found: C, 19.89; N{cyrillic}, 1.87; Cl, 13.98.
-
-
-
-
44
-
-
70649103383
-
-
note
-
3): δ 539.
-
-
-
-
45
-
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0011244432
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Lambert J.B., Papay J.J., Khan S.A., Kappauf K.A., and Magyar E.S. J. Am. Chem. Soc. 96 (1974) 6112
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46
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70649110834
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Patai S., and Rappoport Z. (Eds), John Wiley & Sons, New York
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Luthra N.P., and Odom J.D. In: Patai S., and Rappoport Z. (Eds). The Chemistry of Organic Selenium and Tellurium Compounds Vol. 1 (1986), John Wiley & Sons, New York 198
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Liotta D. (Ed), John Wiley and Sons, New York
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Wudl F. In: Liotta D. (Ed). Organoselenium Chemistry (1987), John Wiley and Sons, New York 395
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Wudl, F.1
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