Characterisation using x-ray photoelectron spectroscopy (XPS) and secondary ion mass spectrometry (SIMS)

Tissue Engineering Using Ceramics and Polymers

Volumn , Issue , 2007, Pages 175-203

  Urquhart, Andrew J ^a   Alexander, Morgan R ^a  

^a UNIVERSITY OF NOTTINGHAM   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

MASS SPECTROMETRY; SECONDARY ION MASS SPECTROMETRY;

X RAY PHOTOELECTRON SPECTROSCOPY;

EID: 70449527413     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1533/9781845693817.1.176     Document Type: Chapter

References (73)

1. Ablett R. An investigation of the angle of contact between paraffin wax and water. Philosophical Magazine 1923, 46:244-256.
2. Alexander M.R. Editorial: bio surface and interface analysis. Surface and Interface Analysis 2006, 28:1379.
3. Alexander M.R., Duc T.M. The chemistry of deposits formed from acrylic acid plasmas. Journal of Materials Chemistry 1998, 8:937-943.
4. Alexander M.R., Wright P.V., Ratner B.D. Trifluoroethanol derivatization of carboxylic acid-containing polymers for quantitative XPS analysis. Surface and Interface Analysis 1996, 24:217-220.
5. Alexander M.R., Short R.D., Jones F.R., Michaeli W., Blomfield C.J. A study of HMDSO/O-2 plasma deposits using a high-sensitivity and -energy resolution XPS instrument: curve fitting of the Si 2p core level. Applied Surface Science 1999, 137:179-183.
6. Anderson D., Levenberg S., Langer R. Nanotiter-scale synethesis of arrayed biomaterials and application to human embryonic stem cells. Nature Biotechnology Letters 2004, 22:863-866.
7. Andrade J.D. Surface and Interfacial Aspects of Biomedical Polymers 1985, Plenum Press, New York.
8. Attard G., Barnes C. Surfaces 2003, Oxford University Press, Oxford.
9. Bain C.D., Whitesides G.M. Depth sensitivity of wetting - monolayers of omega-mercapto ethers on gold. Journal of the American Chemical Society 1988, 110:5897-5898.
10. Barry J.J.A., Silva M., Shakesheff K.M., Howdle S.M., Alexander M.R. Using plasma deposits to promote cell population of the porous interior of three-dimensional poly(D,L-lactic acid) tissue-engineering scaffolds. Advanced Functional Materials 2005, 15:1134-1140.
11. Barry J.J., Howard D., Shakesheff K.M., Howdle S.M., Alexander M.R. Cover picture: using a core-sheath distribution of surface chemistry through 3D tissue engineering scaffolds to control cell ingress. Advanced Materials 2006, 18:1406-1410.
12. Beamson G., Alexander M.R. Angle-resolved XPS of fluorinated and semi-fluorinated side-chain polymers. Surface and Interface Analysis 2004, 36:323.
13. Beamson G., Briggs D. High Resolution XPS of Organic Polymers - TheScienta ESCA300 Database 1992, now avalable from, Wiley, Chichester. http://www.surfacespectra.com/.
14. Brewer N.J., Foster T.T., Leggett G.J., Alexander M.R., McAlpine E. Comparative investigations of the packing and ambient stability of self-assembled monolayers of alkanethiols on gold and silver by friction force microscopy. Journal of Physical Chemistry B 2004, 108:4723-4728.
15. Briggs D., Grant J.T. Surface Analysis by Auger and X-Ray Photoelectron Spectroscopy 2003, IM Publications, Chichester.
16. Briggs D., Seah M.P. Practical Surface Analysis: Auger and X-ray Photoelectron Spectroscopy 1990, Wiley, Chichester.
17. Briggs D., Seah M. Practical Surface Analysis: Ion and Neutral Spectroscopy 1992, John Wiley &Sons, New York.
18. Briggs D., Seah M.P. Practical Surface Analysis: Ion and Neutral Spectroscopy 1996, John Wiley &Sons, Chichester.
19. Briggs D., Wootton A.B. Analysis of polymer surfaces by SIMS. 1. An investigation of practical problems. Surface and Interface Analysis 1982, 4:109-115.
20. Briggs D., Brewis D.M., Konieczo M.B. X-ray photoelectron-spectroscopy studies of polymer surfaces. 1. Chromic acid etching of polyolefins. Journal of Materials Science 1976, 11:1270-1277.
21. Briggs D., Brown A., Vickerman J.C. Handbook of Static Secondary Ion Mass Spectrometry (SIMS) 1989, Wiley, Chichester.
22. Briggs D., Brewis D.M., Dahm R.H., Fletcher I.W. Analysis of the surface chemistry of oxidized polyethylene: comparison of XPS and ToF-SIMS. Surface and Interface Analysis 2003, 35:156-167.
23. Brown A., Vickerman J.C. A comparison of positive and negative-ion static SIMS spectra of polymer surfaces. Surface and Interface Analysis 1986, 8:75-81.
24. Brunette D.M., Tengvall P., Textor M., Thomsen P. Titanium in Medicine 2001, Springer-Verlag, Berlin/Heidelberg/New York.
25. Chilkoti A., Ratner B.D. An X-ray photoelectron spectroscopic investigation of the selectivity of hydroxyl derivatization reactions. Surface and Interface Analysis 1991, 17:567-574.
26. Clark D.T., Musgrave W.K., Kilcast D., Feast W.J. Applications of ESCA to polymer chemistry - studies of some nitroso rubbers. Journal of Polymer Science Part A - 1 - Polymer Chemistry 1972, 10:1637.
27. Cohen H. Chemically resolved electrical measurements using X-ray photoelectron spectroscopy. Applied Physics Letters 2004, 85:1271-1273.
28. Cumpson P.J. Angle-resolved XPS and AES - depth-resolution limits and a general comparison of properties of depth-profile reconstruction methods. Journal of Electron Spectroscopy and Related Phenomena 1995, 73:25-52.
29. Curtis A., Riehle M. Tissue engineering: the biophysical background. Physics in Medicine and Biology 2001, 46:R47-R65.
30. Dehili C., Lee P., Shakesheff K., Alexander M. Comparison of primary rat hepatocyte attachment to collagen and plasma polymerised allylamine on glass. Plasmas Processes and Polymers 2006, 3:474-484.
31. Even-Ram S., Artym V., Yamada K.M. Matrix control of stem cell fate. Cell 2006, 126:645-647.
32. Fahlman A., Hagstrom S., Hamrin K., Nordberg R., Nordling C., Siegbahn K. An apparatus for ESCA method. Arkiv for Fysik 1966, 31:479-485.
33. Fally F., Doneux C., Riga J., Verbist J.J. Quantification of the functional-groups present at the surface of plasma polymers deposited from propylamine, allylamine, and propargylamine. Journal of Applied Polymer Science 1995, 56:597-614.
34. Fletcher J., Lockery N., Vickerman J.C. C60, buckminsterfullerene: its impact on biological ToF-SIMS analysis. Surface and Interface Analysis 2006, 38:1393-1400.
35. Foster T.T., Alexander M.R., Leggett G.J., McAlpine E. Friction force microscopy of self-assembled monolayers on aluminium surfaces - influence of alkyl chain length. Langmuir 2006, 22:9254-9259.
36. Fraser H.J., Collings M.P., McCoustra M.R.S., Williams D.A. Thermal desorption of water ice in the interstellar medium. Monthly Notices of the Royal Astronomical Society 2001, 327:1165.
37. Gardella J.A., Hercules D.M. Static secondary ion mass spectrometry. Analytical Chemistry 1980, 22:226-232.
38. Gilmore I.S., Seah M.P. G-SIMS of biodegradable homo-polyesters. Applied Surface Science 2003, 252:6797-6800.
39. Haddow D.B., MacNeil S., Short R.D. A cell therapy for chronic wounds based upon a plasma polymer delivery surface. Plasma Processes and Polymers 2006, 3:419-430.
40. Hou Q.P., Rutten F.J.M., Smith E.F., Briggs D., Davies M.C., Buttery L.D.K., Freeman R., Shakesheff K.M. Surface characterization of pre-formed alginate fibres incorporated with a protein by a novel entrapment process. Surface and Interface Analysis 2005, 37:1077-1081.
41. Johansson B. ToF-SIMS imaging of lipids in cell membranes. Surface and Interface Analysis 2006, 38:1401-1412.
42. Lewis K.B., Ratner B.D. Observation of surface rearrangement of polymers using ESCA. Journal of Colloid and Interface Science 1993, 159:77-85.
43. Magnani A., Barbucci R., Lewis K.B., Leachscampavia D., Ratner B.D. Surface-properties and restructuring of a cross-linked polyurethane-poly(amido-amine) network. Journal of Materials Chemistry 1995, 5:1321-1330.
44. McArthur S.L. XPS in bioengineering. Surface and Interface Analysis 2006, 38:1381-1385.
45. Michel R., Castner D.G. Advances in ToF SIMS analysis of protein films. Surface and Interface Analysis 2006, 38:1386-1392.
46. Ogaki R., Green F., Li S., Vert M., Alexander M.R., Gilmore I.S., Davies M.C. G-SIMS of biodegradable homo-polyesters. Applied Surface Science 2006, 252:6797-6800.
47. Ogaki R., Green F.M., Gilmore I.S., Shard A.G., Alexander M.R., Davies M.C. Study of the end group contribution to ToF-SIMS and G-SIMS spectra of poly(lactic acid) using deuterium labelling. Surface and Interface Analysis. 2007, in press.
48. Parry K., Shard A., Short R.D., White R., Whittle J., Wright A. ARXPS characterisation of plasma polymerised surface chemical gradients. Surface and Interface Analysis 2006, 38:1497-1504.
49. Pertays K., Thompson G.E., Alexander M.R. Self assembly of stearic acid on aluminium: the importance of oxide surface chemistry. Surf. Interface Anal. 2004, 36:1361-1366.
50. Petrovykh D.Y., Kimura-Suda H., Tarlov M.J., Whitman L.J. Quantitative characterization of DNA films by X-ray photoelectron spectroscopy. Langmuir 2004, 20:429-440.
51. Quirk R.A., Briggs D., Davies M.C., Tendler S.J.B., Shakesheff K.M. Characterization of the spatial distributions of entrapped polymers following the surface engineering of poly(lactic acid). Surface and Interface Analysis 2001, 31:46-50.
52. Ratner B., Weathersby P., Hoffman A., Kelly Mascharpen L. Radiation-grafted hydrogels for biomaterial applications as studied by ESCA technique. Journal of Polymer Science 1978, 22:643-664.
53. Ratner B.D. Advances in the analysis of surfaces of biomedical interest. Surface and Interface Analysis 1995, 23:521-528.
54. Senshu K., Yamashita S., Mori H., Ito M., Hirao A., Nakahama S. Time-resolved surface rearrangements of poly(2-hydroxyethyl methacrylate-block-isoprene) in response to environmental changes. Langmuir 1999, 15:1754-1762.
55. Shakesheff K.M., Evora C., Soriano I., Langer R. The adsorption of poly(vinyl alcohol) to biodegradable microparticles studied by X-ray photoelectron spectroscopy (XPS). Journal of Colloid and Interface Science 1997, 185:538-547.
56. Shard A.G., Volland C., Davies M.C., Kissel T. Information on the monomer sequence of poly(lactic acid) and random copolymers of lactic acid and glycolic acid by examination of static secondary ion mass spectrometry ion intensities. Macromolecules 1996, 29:748-754.
57. Shard A.G., Brewer P.J., Green F.M., Gilmore I.S. Measurement of sputtering yields and damage in C60 SIMS depth profiling of model organic materials. Surface and Interface Analysis 2007, 38:294-298.
58. Sosnika A., Sodhia R.N.S., Brodersend P.M., Seftona M.V. Surface study of collagen/poloxamine hydrogels by a 'deep freezing' ToF-SIMS approach. Biomaterials 2006, 27:2340-2348.
59. Tougaard S. Universality classes of inelastic electron scattering cross-sections. Surface and Interface Analysis 1997, 25:137-154.
60. Tougaard S. Accuracy of the non-destructive surface nano-structure quantification technique based on analysis of the XPS or AES peakshape. Surface Interface Analysis 1998, 26:249-269.
61. Tsourapas G., Rutten F.J.M., Briggs D., Davies M.C., Shakesheff K.M. Surface spectroscopic imaging of PEG-PLA tissue engineering constructs with ToF-SIMS. Applied Surface Science 2006, 252:6693-6696.
62. Tyler B. ToF-SIMS image analysis. ToF-SIMS: Surface Analysis by Mass Spectrometry 2001, and IM. http://www.surfacespectra.com/, J.C. Vickerman, D. Briggs (Eds.).
63. Urquhart A., Taylor M., Anderson D., Langer R., Alexander M., Davies M.C. High through-put surface characterisation of arrayed biomaterials. Advanced Materials. 2007, in press.
64. Vickerman J.C., Briggs D., Henderson A. The Static SIMS Library 2000, Surface Science. http://www.surfacespectra.com/.
65. ToF-SIMS: Surface Analysis by MassSpectroscopy 2001, and IM. http://www.surfacespectra.com/, J.C. Vickerman, D. Briggs (Eds.).
66. Vitte J., Benoliel A.M., Pierres A., Bongrand P. Is there a predictable relationship between surface physical-chemical properties and cell behaviour at the interface?. European Cells and Materials 2004, 7:52-63.
67. Wagner M.S., Graham D.J., Ratner B.D., Castner D.G. Maximizing information obtained from secondary ion mass spectra of organic thin films using multivariate analysis. Surface Science 2004, 570:78-97.
68. Walton J., Fairley N. Quantitative surface chemical-state microscopy by x-ray photoelectron spectroscopy. Surface and Interface Analysis 2004, 36:89-91.
69. Walton J., Fairley N. Noise reduction in X-ray photoelectron spectromicroscopy by a singular value decomposition sorting procedure. Journal of Electron Spectroscopy and Related Phenomena 2005, 148:29-40.
70. Whitesides G.M., Laibinis P.E. Wet chemical approaches to the characterization of organic-surfaces - self-assembled monolayers, wetting, and the physical organic-chemistry of the solid liquid interface. Langmuir 1990, 6:87-96.
71. Whittle J.D., Barton D., Alexander M.R., Short R.D. A method for the deposition of controllable chemical gradients. Chemical Communications 2003, 14:1766-1767.
72. Wilson J., Hench L.L., Greenspan D. Bioceramics 1994, Pergamon Press, Oxford.
73. Wolstenholme J.F.W.J. An Introduction to Surface Analysis by XPS and AES 2003, John Wiley and Sons Ltd, Chichester.