A calorimetric system based on the LKB 10700-1 flow microcalorimeter

Measurement Science and Technology

Volumn 20, Issue 7, 2009, Pages

  Leskiv, Miroslav ^a   Bernardes, Carlos E S ^a   Minas Da Piedade, Manuel E ^a  

^a UNIVERSITY OF LISBON   (Portugal)

Author keywords

Flow microcalorimetry; Hydrochloric acid; Sucrose; Thermochemistry

Indexed keywords

CALIBRATION; CALORIMETERS; HYDROCHLORIC ACID; LIQUIDS; SOLUTIONS; SUGAR (SUCROSE); THERMOCHEMISTRY;

CALIBRATION CONSTANTS; CALORIMETRIC LIQUID; ELECTRICAL CALIBRATIONS; ENTHALPIES OF DILUTION; EXPERIMENTAL CONDITIONS; EXPERIMENTAL PROCEDURE; FLOW MICROCALORIMETRY; NEW CALIBRATION SYSTEM;

CALORIMETRY;

EID: 70350697813     PISSN: 09570233     EISSN: 13616501     Source Type: Journal    
DOI: 10.1088/0957-0233/20/7/075107     Document Type: Article

References (36)

1. Johnson R E and Biltonen R L 1975 Determination of reaction-rate parameters by flow microcalorimetry J. Am. Chem. Soc. 97 2349
2. O'Neill M A A, Beezer A E, Labetoulle C, Nicolaides L, Mitchell J C, Orchard J A, Connor J A, Kemp R B and Olomolaiye D 2003 The base catalysed hydrolysis of methyl paraben: a test reaction for flow microcalorimeters used for determination of both kinetic and thermodynamic parameters Thermochim. Acta 399 63
3. O'Neill M A A, Beezer A E, Vine G J, Kemp R B, Olomolaiye D, Volpe P L O and Oliveira D 2004 Practical and theoretical consideration of flow-through microcalorimetry: determination of 'thermal volume' and its flow rate dependence Thermochim. Acta 413 193
4. Stoesser P R and Gill S J 1967 Precision flow- microcalorimeter Rev. Sci. Instrum. 38 422
5. Monk P and Wadsö I 1968 A flow micro reaction calorimeter Acta Chem. Scand. 22 1842
6. Tasker I R, Wood R H and Albert H J 1983 Modifications to a commercial flow microcalorimeter system J. Chem. Tech. Biotechnol. A 33 137
7. Dohnal V and Rehak K 2007 Refined flow microcalorimetric setup for measurement of mixing enthalpies at high dilutions: determination of infinite dilution dissolution enthalpies of some alkanol and ether solutes in water J. Chem. Eng. Data 52 1452
8. Harsted B S and Thomsen E S 1974 Excess enthalpies from flow microcalorimetry 1. Experimental method and excess enthalpies for carbon tetrachloride + cyclohexane, + benzene, and + octamethylcyclotetrasiloxane, and of n-hexane + cyclohexane J. Chem. Thermodyn. 6 549
9. Harsted B S and Thomsen E S 1974 Excess enthalpies from flow microcalorimetry 2. Excess enthalpies for carbon tetrachloride + n-hexane, + n-heptane, + n-octane, + n-hexadecane, + isooctane, and + neopentane, and of octamethylcyclotetrasiloxane + isooctane and + cyclohexane J. Chem. Thermodyn. 6 557
10. Harsted B S and Thomsen E S 1975 Excess enthalpies from flow microcalorimetry 3. Excess enthalpies for binary liquid mixtures of aliphatic and aromatic hydrocarbons, carbon tetrachloride, chlorobenzene, and carbon disulphide J. Chem. Thermodyn. 7 369
11. Tanaka R, Darcy P J and Benson G C 1975 Application of a flow microcalorimeter to determine excess enthalpies of binary mixtures of non-electrolytes Thermochim. Acta 11 163
12. Tamura K, Osaki A, Murakami S, Ohji H, Ogawa H, Laurent B and Grolier J P E 1999 Thermodynamic properties of binary mixtures {an alkoxyethanol plus n-octane}. Excess molar enthalpies and excess molar heat capacities at 298.15 K Fluid Phase Equilib. 156 137
13. Ogawa H and Murakami S 1985 Flow microcalorimeter for heat capacities of solutions Thermochim. Acta 88 255
14. Bjurulf C 1972 Calorimetric titration of lysozyme Eur. J. Biochem. 30 33
15. Janssen L H M and Nelen T H A 1979 Influence of hydrogen and chloride ions on the interaction between sulfaethidole and bovine serum albumin studied by microcalorimetric and acid-base titrimetric methods J. Biol. Chem. 254 5300
16. Janssen L H M, Dröge J H M, Durlinger F C J and Fruytier F J 1985 The pH dependence of the thermodynamics of the interaction of diazepam with human serum albumin J. Biol. Chem. 260 11442
17. tefuca V, Votiar I, efoviov J, Katrlík J, Mastihuba V, Greifov M and Gemeiner P 2006 Development of enzyme flow calorimeter system for monitoring of microbial glycerol conversion Appl. Microbiol. Biotechnol. 72 1170
18. Monk P and Wadsö I 1969 Flow microcalorimetry as an analytical tool in biochemistry and related areas Acta Chem. Scand. 23 29
19. Debord J, Harel M, Bollinger J C, Verneuil B, Merle L and Dantoine T 2005 Flow microcalorimetric study of enzyme reactions: application to arylesterase from human serum Thermochim. Acta 427 85
20. Marsh K N 1987 Recommended Reference Materials for the Realization of Physicochemical Properties (Oxford: IUPAC-Blackwell Scientific Publications)
21. Briggner L E and Wadsö I 1991 Test and calibration processes for microcalorimeters, with special reference to heat-conduction instruments used with aqueous systems J. Biochem. Biophys. Methods 22 101
22. Sabbah R, Xu-wu A, Chickos J S, Planas Leito M L, Roux M V and Torres L A 1999 Reference materials for calorimetry and differential thermal analysis Thermochim. Acta 331 93
23. Wadsö I 2000 Needs for standards in isothermal microcalorimetry Thermochim. Acta 347 73
24. Wadsö I and Goldberg R N 2001 Standards in isothermal microcalorimetry (IUPAC technical report) Pure Appl. Chem. 73 1625
25. Bernardes C E S 2008 CBCAL 1.0: A program for calorimeter control and data acquisition (Lisbon: FCUL)
26. LKB 1969 LKB 10700-1 Flow Microcalorimeter Operation Manual (Stockholm-Bromma 1: LKB-Produkter AB)
27. Wieser M E 2006 Atomic weights of the elements 2005 (IUPAC technical report) Pure Appl. Chem. 78 2051
28. Hemminger W and Sarge S M 1998 Definitions, nomenclature, terms and literature Handbook of Thermal Analysis and Calorimetry vol 1 ed M E Brown (Amsterdam: Elsevier)
29. Laliberté M 2007 Model for calculating the viscosity of aqueous solutions J. Chem. Eng. Data 52 321
30. Laliberté M 2007 Model for calculating the viscosity of aqueous solutions J. Chem. Eng. Data 52 1507
31. Gucker F T Jr, Pickard H B and Planck R W 1939 A new micro-calorimeter: the heats of dilution of aqueous solutions of sucrose at 20° and 30° and their heat capacities at 25° J. Am. Chem. Soc. 61 459
32. Vallender R B and Perman E P 1931 Vapour pressure and heat of dilution: part VIII. Heat of dilution of cane sugar in aqueous solution and of urea and calcium chloride in alcoholic solution Trans. Farad. Soc. 27 124
33. Pratt F R 1918 Heats of dilution and their variations with temperature J. Franklin Inst. 185 663
34. Wagman D D, Evans W H, Parker V B, Schumm R H, Halow I, Bailey S M, Churney K L and Nuttall R L 1982 The NBS tables of chemical thermodynamics properties J. Phys. Chem. Ref. Data 11 (Suppl 12)
35. Olofsson G 1979 Assignment of uncertainties Experimental Chemical Thermodynamics vol 1 ed S Sunner and M Mnsson (Oxford: Pergamon Press) p 137
36. Cox J D 1972 Chlorine compounds "CATCH" Computer Analysis of Thermochemical Data ed J B Pedley (Brighton: University of Sussex)