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Crystal data for Gd2(fum)3(H2O)4·3H2O: C12H20O19Gd2, Mr, 782.78, monoclinic, space group P 21/n, a, 9.4793(1, b, 14.7439(3, c, 14.7929(2) Å, β, 91.2630(9)°, V, 2066.98(6) Å3, Z, 4, DC, 2.515 g cm-3, μ(Mo Kα, 6.457 mm-1, 40,311 reflections collected, 4728 unique (Rint, 0.0713, 3742 observations with I ≥ 2σ(I, R1, 0.0248 for observations, wR2, 0.0561 for all data, GOF, 0.985. The intensity data was collected on a NONIUS KappaCCD diffractometer with Mo Kα radiation (λ, 0.71073 Å) at 293 K. The structure of the isostructural Sm compound, where Sm was replaced with Gd, was used for the structure refinements
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int = 0.0713), 3742 observations with I ≥ 2σ(I), R1 = 0.0248 for observations, wR2 = 0.0561 for all data, GOF = 0.985. The intensity data was collected on a NONIUS KappaCCD diffractometer with Mo Kα radiation (λ = 0.71073 Å) at 293 K. The structure of the isostructural Sm compound, where Sm was replaced with Gd, was used for the structure refinements.
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