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70350502734
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note
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2 obtained as above was taken into a 25 ml r.b. flask and to this, dimethyl-p-tolyl silane 1l (0.4 g, 2.6 mmol) and THF (5 ml) were added and stirred for 4 h at room temperature keeping open to air. After completion of the reaction, 0.38 g (92%) of disiloxane 2l was obtained upon purification and its spectral data were identical to that obtained above.
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