Interlamellar silylation of magadiite by octyl triethoxysilane in the presence of dodecylamine

Applied Clay Science

Volumn 46, Issue 3, 2009, Pages 251-254

  Park, Kyeong Won ^a   Jung, Jong Hwa ^a   Kim, Sung Kyu ^b   Kwon, Oh Yun ^c  

^a Gyeongsang National University   (South Korea)

^b Chinju National University   (South Korea)

^c Chonnam National University   (South Korea)

Author keywords

Hydrothermal; Intercalation; Layered silicate; Magadiite; octyl triethoxysilane; Silylation

Indexed keywords

HYDROTHERMAL; LAYERED SILICATE; MAGADIITE; OCTYL TRIETHOXYSILANE; SILYLATION;

ETHANOL; SILICATES;

SILANES;

CATALYST; ETHANOL; MAGADIITE; NUCLEAR MAGNETIC RESONANCE; SILICATE;

EID: 70350342871     PISSN: 01691317     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.clay.2009.08.012     Document Type: Article

References (23)

1. Beneke K., and Lagaly G. Kenyaite-synthesis and properties. Am. Mineral. 68 (1983) 818-826
2. Caravajal G.S., Lyden D.E., Quinting G.R., and Maciel G.E. Structural characterization of (3-aminopropyl)triethoxysilane-modified silicas by silicon-29 and carbon-13 nuclear magnetic resonance. Anal. Chem. 60 (1988) 1776-1786
3. Choi S., Coronas J., Jordan E., et al. Layered silicates by swelling of AMH-3 and nanocomposite membranes. Angew. Chem. Int. Ed. 47 (2008) 552-555
4. Corma A., Fornes V., and Rey F. Delaminated zeolites: an efficient support for enzymes. Adv. Mater. 14 (2002) 71-74
5. +-magadiite, a crystalline hydrated silica. Chem. Mater. 4 (1992) 855-863
6. Galarneau A., Barodawalla A., and Pinnavaia T.J. Porous clay heterostructures formed by gallery-templated synthesis. Nature 374 (1995) 529-531
7. Impens N.R.E.N., van der Voort P., and Vansant E.F. Silylation of micro-, meso- and non-porous oxides: a review. Microporous Mesoporous Mater. 28 (1999) 217-232
8. 4. J. Colloid Interface Sci. 175 (1995) 253-255
9. Kelly D.J., and Leyden D.E. Thermodynamic and kinetic investigation of the protonation of silica-immobilized 3-aminopropylsilane. J. Colloid Interface Sci. 147 (1991) 213-224
10. Kwon O.Y., and Choi S.W. Silica-pillared H-kenyaites: interlamellar base catalyzed-reaction of tetraethylorthosilicate in water suspension. Bull. Korean Chem. Soc. 20 (1999) 69-75
11. Kwon O.Y., and Park K.W. Intercalation behavior of dodecylamine into layered silicates in organic solvents. J. Ind. Eng. Chem. 7 (2001) 44-49
12. +-magadiite and intragallery amine-catalyzed hydrolysis of tetraethylorthosilicate. Chem. Mater. 12 (2000) 1273-1278
13. Kwon O.Y., Jeong S.Y., Suh J.K., and Lee J.M. Hydrothermal syntheses of Na-magadiite and Na-kenyaite in the presence of carbonate. Bull. Korean Chem. Soc. 16 (1995) 737-741
14. Kwon O.Y., Jeong S.Y., Seo J.K., Ryu B.H., and Lee J.M. Effects of organic solvents in the intercalation of octylamine into H-magadiite. J. Colloid Interface Sci. 177 (1996) 677-680
15. Landis M.E., Aufdembrink A.B., Chu P., Johnson I.D., Kirker G.W., and Rubin M.K. Preparation of molecular sieves from dense layered metal oxides. J. Am. Chem. Soc. 113 (1991) 3189-3190
16. Ogawa M., and Kuroda K. Preparation of inorganic-organic nanocomposites through intercalation of organoammonium ions into layered silicates. Bull. Chem. Soc. Jpn. 70 (1997) 2593-2618
17. Ogawa M., Okutomo S., and Kuroda K. Control of interlayer microstructures of a layered silicate by surface modification with organochlorosilanes. J. Am. Chem. Soc. 120 (1998) 7361-7362
18. Okutomo S., Kuroda K., and Ogawa M. Preparation and characterization of silylated-magadiites. Appl. Clay Sci. 15 (1999) 253-264
19. Ruiz-Hitzky E., and Rojo J.M. Intracrystalline grafting on layer silicic acids. Nature 287 (1980) 28-30
20. Ruiz-Hitzky E., Rojo J.M., and Lagaly G. Mechanism of the grafting of organosilanes on mineral surfaces III. Interlamellar grafting of layer silicic acids. Colloid Polym. Sci. 263 (1985) 1025-1030
21. Shimojima A., Mochizuki D., and Kuroda K. Synthesis of silylated derivatives of a layered polysilicate kanemite with mono-, di-, and trichloro(alkyl)silanes. Chem. Mater. 13 (2001) 3603-3609
22. Thiesen P.H., Beneke K., and Lagaly G. Silylation of a crystalline silicic acid: an MAS NMR and porosity study. J. Mater. Chem. 12 (2002) 3010-3015
23. Yanagisawa T., Kuroda K., and Kato C. Organic derivatives of layered polysilicates : I. Trimethylsilylation of magadiite and kenyaite. React. Solids 5 (1988) 167-175