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Crystal data for complex 3: C14H28CaO4, Mr, 300.44, T= 130 K, crystal size 0.21 × 0.26 × 0.27 mm3, MoKα radiation, λ, 0.71073 Å, μ, 0.382 mm-1; monoclinic, P 1/n, a, 8.4399(4) Å, b, 22.9328(11) Å, c, 9.0724(4) Å, β, 107.8020(10)°, V= 1671.89(13) Å3, Z, 4, ρcalcd, 1.194 Mgm-3, 2θmax, 61.8°, 24991 reflections collected, 4953 independent (Rint, 0.0356, final R 1, 0.0357, wR2, 0.0944 (I 2σI, GoF, 1.040, ρmax, 0.381 eÅ-3, ρmin, 0.483 eÅ-3. CCDC 721251 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic
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