The true structures of the vannusals, part 2: Total synthesis and revised structure of vannusal b

Angewandte Chemie - International Edition

Volumn 48, Issue 31, 2009, Pages 5648-5652

  Nicolaou, K C ^a,b   Ortiz, Adrian ^a,b   Zhang, Hongjun ^a,b  

^a SCRIPPS RESEARCH INSTITUTE   (United States)

^b UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

Natural products; NMR spectroscopy; Revised structures; Structure elucidation; Total synthesis

Indexed keywords

NATURAL PRODUCTS; NMR SPECTROSCOPY; REVISED STRUCTURES; STRUCTURE ELUCIDATION; TOTAL SYNTHESIS;

NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

SYNTHESIS (CHEMICAL);

SPIRO COMPOUND; VANNUSAL B;

ARTICLE; CHEMISTRY; CONFORMATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

CRYSTALLOGRAPHY, X-RAY; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR CONFORMATION; SPIRO COMPOUNDS;

EID: 70349904880     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200902029     Document Type: Article

References (11)

1. K. C. Nicolaou, H. Zhang, A. Ortiz, Angew. Chem. 2009, 121, 5752;
2. Angew. Chem. Int. Ed. 2009, 48, 5642, see the preceding communication in this issue.
3. K. C. Nicolaou, H. Zhang, A. Ortiz, P. Dagneau, Angew. Chem. 2008, 120, 8733-8738;
4. Angew. Chem. Int. Ed. 2008, 47, 8605-8610.
5. CCDC 726955 (9d) contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
6. Details of these studies will be reported in the full account of this work.
7. M. Shibuya, M. Tomizawa, I. Suzuki, Y. Iwabuchi, J. Am. Chem. Soc. 2006, 128, 8412-8413.
8. G. Guella, F. Dini, F. Pietra, Angew. Chem. 1999, 111, 1217-1220;
9. Angew. Chem. Int. Ed. 1999, 38, 1134-1136.
10. 13C NMR spectra of vannusals A and B as well as their reduction derivative 27.
11. CCDC 726954 (4) contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.