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Crystal data for 1: [C108H162B2O 4F8CrAg22, monoclinic, P 2 1]n, a, 21.8762(5, 6, 21.6612(6, c, 28.2026(8) Å, β, 91.033(2, V= 13362.0(6) Å3, Z, 4, T=173K, 77080 reflections measured, 35799 unique (Rint, 0.148, final R 1, 0.0529, wR 2, < 0.0723 for 8235 observed reflections [I > 20(I, Crystal data for 2, C108H 162B O4F4SAg21, monoclinic, Pn, a, 15.3810(3, b, 15.7752(4, c, 27.3409(5) Å, β, 94.834(2, V= 6610.4(2) Å3, Z, 2, T=173K, 47221 reflections measured, 27050 unique (Rint, 0.0548, final R 1, 0.0438, wR 2, 0.0708 for 11807 observed reflections [I>2σI, Crystal data for 3, C248H 204B3
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int = 0.1424), final R 1 = 0.0760, wR 2 = 0.1607 for 14639 observed reflections [I> 2σ(I)]. CCDC 729707 (1), CCDC 729708 (2) and CCDC 729709 (3) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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