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Crystal data for 8: Formula, C39H42Cl 2F6N2O6S2Te, T= 150(2) K, Mτ= 1011.37 g mol-1, crystal size: 0.31 × 0.26 × 0.08 mm, orthorhombic, space group Pna2(1, a, 18.491(4, b, 12.156(2, c, 19.453(4) Å, V= 4372(2) Å3, Z, 4, ρcalcd= 1.536 g cm-3, μ= 0.969 mm-1, 2θmax, 27.49°, 9395 reflections measured, 9395 unique, refined parameters, 524, R1(I) > 2σ(I, 0.0524, wR 2(F2, 0.1146, R1(all data, 0.0875, wR 2(all data, 0.1310, ρ(e)(min/max, 1.183/0.970 e Å-3. Crystal data for 9: Formula, C 31.5H42F6N8O6S 2Te, T= 150(2) K, Mr= 1040.80 g mol-1, crystal size: 0.30 × 0.30 × 0.20 mm, tricl
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