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70349974102
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Various 1,2-dihalogenoethanes were compared. See the Supporting Information.
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Various 1,2-dihalogenoethanes were compared. See the Supporting Information.
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32
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70349976571
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See the Supporting Information, Table S4
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See the Supporting Information, Table S4.
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70349970322
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2Zn⇄ArZnAlk; see: C Bolm, N. Hermanns, J. P. Hildebrand, K. Muñiz, Angew. Chem. 2000,112, 3607; Angew. Chem. Int. Ed. 2000, 39, 3465.
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4243489506
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Zn dust was activated by treatment with 1,2-dibromoethane (5mol%) then with trimethylsilyl chloride (3mol%). For a practical procedure see: B. H. Lipshutz, M. R. Wood, R. Tirado, Org. Synth. 1999, 76, 252.
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Zn dust was activated by treatment with 1,2-dibromoethane (5mol%) then with trimethylsilyl chloride (3mol%). For a practical procedure see: B. H. Lipshutz, M. R. Wood, R. Tirado, Org. Synth. 1999, 76, 252.
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