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3 methyl protons of the adduct which appear at 1.24 ppm.
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2] according to a modified PFT methodology. Polymerization conditions: MAO as cocatalyst, heptane as solvent, Al/MWNT = 2, AVZr = 2000, N/E = 2, T = 30 °C MAO was kept in contact with MWNTs for 10 h, then sonicated for 30 min at room temperature, and vacuum dried for 2 h at 200 °C After the addition of heptane, norbornene, ethylene, and metallocene were added. The copolymer MWNTs mixture was precipitated in MeOH/HCl.
-
2] according to a modified PFT methodology. Polymerization conditions: MAO as cocatalyst, heptane as solvent, Al/MWNT = 2, AVZr = 2000, N/E = 2, T = 30 °C MAO was kept in contact with MWNTs for 10 h, then sonicated for 30 min at room temperature, and vacuum dried for 2 h at 200 °C After the addition of heptane, norbornene, ethylene, and metallocene were added. The copolymer MWNTs mixture was precipitated in MeOH/HCl.
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