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Volumn 14, Issue 6, 2009, Pages 402-408

Applications of stopped-flow in SAXS and SANS

Author keywords

Biology; Kinetics; Small angle neutron scattering; Small angle X ray scattering; Soft condensed matter; Stopped flow

Indexed keywords

DETECTION TECHNIQUE; DURING PHASE; INTERMEDIATE STATE; SMALL ANGLE NEUTRON; SMALL ANGLE NEUTRON SCATTERING; SMALL ANGLE SCATTERING; SMALL ANGLE X-RAY SCATTERING; SOFT CONDENSED MATTER; SOFT MATTER; STOPPED-FLOW; STOPPED-FLOW APPARATUS; TECHNICAL ADVANCES; TIME RESOLUTION;

EID: 70349434775     PISSN: 13590294     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cocis.2009.04.005     Document Type: Review
Times cited : (60)

References (59)
  • 1
    • 0001533281 scopus 로고    scopus 로고
    • Micelle-to-vesicle transition: a time-resolved structural Study
    • One of the first SANS TR-resolved experiments to follow the transition from micelle to vesicle induced by dilution of aqueous mixture of lecithin and bile salt. Upon dilution, the shape of the monodisperse micelles changes from small spherical to elongated, flexible and locally cylindrical structures that close after several hours.
    • Egelhaaf S.U., and Schurtenberger P. Micelle-to-vesicle transition: a time-resolved structural Study. PRL 82 (1999) 2804-2807. One of the first SANS TR-resolved experiments to follow the transition from micelle to vesicle induced by dilution of aqueous mixture of lecithin and bile salt. Upon dilution, the shape of the monodisperse micelles changes from small spherical to elongated, flexible and locally cylindrical structures that close after several hours.
    • (1999) PRL , vol.82 , pp. 2804-2807
    • Egelhaaf, S.U.1    Schurtenberger, P.2
  • 2
    • 0001498978 scopus 로고
    • La diffraction des rayons X aux très petits angles: Application à l'étude de phénomènes ultramicroscopique
    • Guinier A. La diffraction des rayons X aux très petits angles: Application à l'étude de phénomènes ultramicroscopique. Ann Phys Paris 12 (1939) 161-237
    • (1939) Ann Phys Paris , vol.12 , pp. 161-237
    • Guinier, A.1
  • 3
    • 0013404780 scopus 로고
    • Neutron small-angle scattering of biological macromolecules in solution
    • Stuhrmann H.B. Neutron small-angle scattering of biological macromolecules in solution. J Appl Cryst 7 (1974) 173-178
    • (1974) J Appl Cryst , vol.7 , pp. 173-178
    • Stuhrmann, H.B.1
  • 4
    • 0009122071 scopus 로고
    • The determination of the scattering density distribution of polydisperse solutions by contrast variation: a neutron scattering study of ferritin
    • Stuhrmann H.B., and Duee E.D. The determination of the scattering density distribution of polydisperse solutions by contrast variation: a neutron scattering study of ferritin. J Appl Cryst 8 (1975) 538-542
    • (1975) J Appl Cryst , vol.8 , pp. 538-542
    • Stuhrmann, H.B.1    Duee, E.D.2
  • 5
    • 0016640142 scopus 로고
    • Comparison of neutron and X-ray scattering of dilute myoglobin solutions
    • Ibel K., and Stuhrmann H.B. Comparison of neutron and X-ray scattering of dilute myoglobin solutions. J Mol Biol 93 (1975) 255-265
    • (1975) J Mol Biol , vol.93 , pp. 255-265
    • Ibel, K.1    Stuhrmann, H.B.2
  • 6
    • 2942542780 scopus 로고    scopus 로고
    • Design criteria for electronics for resistive charge division in thermal neutron detection
    • van Esch P., Gahl T., and Guérard B. Design criteria for electronics for resistive charge division in thermal neutron detection. Nucl Instrum Methods Phys Res A 526 (2004) 493-500
    • (2004) Nucl Instrum Methods Phys Res A , vol.526 , pp. 493-500
    • van Esch, P.1    Gahl, T.2    Guérard, B.3
  • 7
    • 0348196865 scopus 로고    scopus 로고
    • Optimal lookup table construction with respect to efficiency flatness
    • van Esch P., and Millier F. Optimal lookup table construction with respect to efficiency flatness. Rev Sci Instrum 74 (2003) 5058-5061
    • (2003) Rev Sci Instrum , vol.74 , pp. 5058-5061
    • van Esch, P.1    Millier, F.2
  • 8
    • 0000670930 scopus 로고    scopus 로고
    • SAXS and USAXS on the high brilliance beamline at the ESRF
    • Narayanan T., Diat O., and Bosecke P. SAXS and USAXS on the high brilliance beamline at the ESRF. Nucl Instrum Methods Phys Res A 467-468 (2001) 1005-1009
    • (2001) Nucl Instrum Methods Phys Res A , vol.467-468 , pp. 1005-1009
    • Narayanan, T.1    Diat, O.2    Bosecke, P.3
  • 9
    • 34948814599 scopus 로고    scopus 로고
    • The fast readout low noise camera as a versatile X-ray detector for time resolved dispersive extended X-ray absorption fine structure and diffraction studies of dynamic problems in materials science, chemistry, and catalysis
    • Labiche J.C., Mathon O., Pascarelli S., Newton M.A., Guilera Ferre G., Curfs C., et al. The fast readout low noise camera as a versatile X-ray detector for time resolved dispersive extended X-ray absorption fine structure and diffraction studies of dynamic problems in materials science, chemistry, and catalysis. Rev Sci Instrum 78 (2007) 091301
    • (2007) Rev Sci Instrum , vol.78 , pp. 091301
    • Labiche, J.C.1    Mathon, O.2    Pascarelli, S.3    Newton, M.A.4    Guilera Ferre, G.5    Curfs, C.6
  • 10
    • 0018972460 scopus 로고
    • Stopped-flow X-ray scattering: the dissociation of aspartate transcarbamylase
    • Moody M.F., Vachette P., Foote A.M., Tardieu A., Kohc M.H.J., and Bordas J. Stopped-flow X-ray scattering: the dissociation of aspartate transcarbamylase. PNAS 77 (1980) 4040-4043
    • (1980) PNAS , vol.77 , pp. 4040-4043
    • Moody, M.F.1    Vachette, P.2    Foote, A.M.3    Tardieu, A.4    Kohc, M.H.J.5    Bordas, J.6
  • 11
    • 0000195894 scopus 로고    scopus 로고
    • Quantitative measurements of Ostwald ripening using time-resolved small-angle neutron scattering
    • TR-SANS is used to monitor the time evolution of radius and density number of droplets in a microemulsion. The paper presents a detailed and quantitative description of the process of formation and ripening in emulsion.
    • Egelhaaf S.U., Olsson U., Schurtenberger P., Morris J., and Wennerström H. Quantitative measurements of Ostwald ripening using time-resolved small-angle neutron scattering. Phys Rev E 60 (1999) 5681-5684. TR-SANS is used to monitor the time evolution of radius and density number of droplets in a microemulsion. The paper presents a detailed and quantitative description of the process of formation and ripening in emulsion.
    • (1999) Phys Rev E , vol.60 , pp. 5681-5684
    • Egelhaaf, S.U.1    Olsson, U.2    Schurtenberger, P.3    Morris, J.4    Wennerström, H.5
  • 12
    • 33845218265 scopus 로고    scopus 로고
    • Probing fast kinetics in complex fluids by combined raping mixing and small-angle X-ray scattering
    • This article describes in detail the stopped-flow technique coupled to SAXS measurements on synchrotron small angle beam line. Two examples in soft matter and biology are presented and limits of the techniques are discussed.
    • Panine P., Finet S., Weiss T.M., and Narayanan T. Probing fast kinetics in complex fluids by combined raping mixing and small-angle X-ray scattering. Adv Colloid and Interface Sci 127 (2006) 9-18. This article describes in detail the stopped-flow technique coupled to SAXS measurements on synchrotron small angle beam line. Two examples in soft matter and biology are presented and limits of the techniques are discussed.
    • (2006) Adv Colloid and Interface Sci , vol.127 , pp. 9-18
    • Panine, P.1    Finet, S.2    Weiss, T.M.3    Narayanan, T.4
  • 13
    • 0037905590 scopus 로고    scopus 로고
    • Formation and growth of anionic vesicles followed by small angle neutron scattering
    • 1/6, in a process controlled by micelle diffusion.
    • 1/6, in a process controlled by micelle diffusion.
    • (2003) Langmuir , vol.19 , pp. 4573-4581
    • Grillo, I.1    Kats, E.2    Muratov, A.R.3
  • 14
    • 70349409400 scopus 로고    scopus 로고
    • Synchrotron small-angle X-ray scattering
    • Borsali R., and Pecora (Eds), Springer-Verlag, Berlin Heidelberg
    • Naranayan T. Synchrotron small-angle X-ray scattering. In: Borsali R., and Pecora (Eds). Soft-matter characterization (2008), Springer-Verlag, Berlin Heidelberg
    • (2008) Soft-matter characterization
    • Naranayan, T.1
  • 16
    • 0007781972 scopus 로고
    • Theory of the kinetics of micellar equilibria and quantitative interpretation of chemical relaxation studies of micellar solutions of ionic surfactants
    • Aniansson E.A.C., Wall S.N., Almgren M., Hoffman H., Kielmann I., Ulbricht W., et al. Theory of the kinetics of micellar equilibria and quantitative interpretation of chemical relaxation studies of micellar solutions of ionic surfactants. J Phys Chem 80 (1976) 905-922
    • (1976) J Phys Chem , vol.80 , pp. 905-922
    • Aniansson, E.A.C.1    Wall, S.N.2    Almgren, M.3    Hoffman, H.4    Kielmann, I.5    Ulbricht, W.6
  • 17
    • 0346150417 scopus 로고    scopus 로고
    • Kinetics of morphological changes in surfactant systems
    • A review article on kinetics in surfactant assemblies.
    • Gradzielski M. Kinetics of morphological changes in surfactant systems. COCIS 8 (2003) 337-345. A review article on kinetics in surfactant assemblies.
    • (2003) COCIS , vol.8 , pp. 337-345
    • Gradzielski, M.1
  • 18
    • 0037844357 scopus 로고    scopus 로고
    • Vesicles and vesicle gels-structure and dynamics of formation
    • Gradzielski M. Vesicles and vesicle gels-structure and dynamics of formation. J Phys: Condens Matter 15 (2003) R655-R697
    • (2003) J Phys: Condens Matter , vol.15
    • Gradzielski, M.1
  • 19
    • 9744279754 scopus 로고    scopus 로고
    • Investigation of the dynamics of morphological transitions in amphiphilic systems
    • Gradzielski M. Investigation of the dynamics of morphological transitions in amphiphilic systems. COCIS 9 (2004) 256-263
    • (2004) COCIS , vol.9 , pp. 256-263
    • Gradzielski, M.1
  • 20
    • 0000356223 scopus 로고    scopus 로고
    • Behavior of ionically charged lamellar systems under the influence of a shear field
    • Bergmeier M., Gradzielski M., Hoffmann H., and Mortensen K. Behavior of ionically charged lamellar systems under the influence of a shear field. J Phys Chem B 103 (1999) 1605-1617
    • (1999) J Phys Chem B , vol.103 , pp. 1605-1617
    • Bergmeier, M.1    Gradzielski, M.2    Hoffmann, H.3    Mortensen, K.4
  • 21
    • 0037166829 scopus 로고    scopus 로고
    • Millisecond-range time-resolved small-angle X-ray scattering studies of micellar transformations
    • Schmölzer S., Gräbner D., Gradzielski M., and Narayanan T. Millisecond-range time-resolved small-angle X-ray scattering studies of micellar transformations. PRL 88 (2002) 258301
    • (2002) PRL , vol.88 , pp. 258301
    • Schmölzer, S.1    Gräbner, D.2    Gradzielski, M.3    Narayanan, T.4
  • 22
    • 10644271575 scopus 로고    scopus 로고
    • Dynamics of structural transitions in amphiphilic systems monitored by scattering techniques
    • Gradzielski M., Grillo I., and Narayanan T. Dynamics of structural transitions in amphiphilic systems monitored by scattering techniques. Progr Colloid Polym Sci (2004) 129-132
    • (2004) Progr Colloid Polym Sci , pp. 129-132
    • Gradzielski, M.1    Grillo, I.2    Narayanan, T.3
  • 23
    • 18244367129 scopus 로고    scopus 로고
    • Dynamics of self-assembly of unilamellar vesicles
    • TR-SAXS study of the transition from micelles to vesicles in a zwitterionic-anionic micellar mixture. The results reveal transient state of disklike micelles which grow during the initial few hundred milliseconds and then close to form unilamellar vesicles with a narrow size distribution. The radius evolves following an exponential law from 13 to 28 nm in about 600 s. The driving mechanism is very likely the unfavourable edge energy arising from packing constraints characterised by the mine tension. To reduce the edge energy, the floppy micelles coalesce until they reach a critical radius and close.
    • Weiss T.M., Narayanan T., Gradzielski M., Panine P., Finet S., and Helsby W.I. Dynamics of self-assembly of unilamellar vesicles. PRL 94 (2005) 038303. TR-SAXS study of the transition from micelles to vesicles in a zwitterionic-anionic micellar mixture. The results reveal transient state of disklike micelles which grow during the initial few hundred milliseconds and then close to form unilamellar vesicles with a narrow size distribution. The radius evolves following an exponential law from 13 to 28 nm in about 600 s. The driving mechanism is very likely the unfavourable edge energy arising from packing constraints characterised by the mine tension. To reduce the edge energy, the floppy micelles coalesce until they reach a critical radius and close.
    • (2005) PRL , vol.94 , pp. 038303
    • Weiss, T.M.1    Narayanan, T.2    Gradzielski, M.3    Panine, P.4    Finet, S.5    Helsby, W.I.6
  • 24
    • 42449160636 scopus 로고    scopus 로고
    • Dynamics of spontaneous vesicle formation in fluorocarbon and hydrocarbon surfactant mixtures
    • Vesicles formation and growth in catanionic and zwitterionic systems are investigated by TR-SAXS. Transient disklike micelles are evidenced in the zwitterionic system, whereas vesicles are already formed 10 ms after the mixing for the catanionic mixture. The different mechanisms are explained by the role of electrostatic barrier and bending energy on the formation, growth and stability of vesicles are given.
    • Weiss T.M., Narayanan T., and Gradzielski M. Dynamics of spontaneous vesicle formation in fluorocarbon and hydrocarbon surfactant mixtures. Langmuir 24 (2008) 3759. Vesicles formation and growth in catanionic and zwitterionic systems are investigated by TR-SAXS. Transient disklike micelles are evidenced in the zwitterionic system, whereas vesicles are already formed 10 ms after the mixing for the catanionic mixture. The different mechanisms are explained by the role of electrostatic barrier and bending energy on the formation, growth and stability of vesicles are given.
    • (2008) Langmuir , vol.24 , pp. 3759
    • Weiss, T.M.1    Narayanan, T.2    Gradzielski, M.3
  • 25
    • 26844539903 scopus 로고    scopus 로고
    • The microstructure of di-alkyl chain cationic/nonionic surfactant mixtures: observation of coexisting lamellar and micellar phases and depletion induced phase separation
    • Penfold J., Staples E., Ugazio S., Soubiran L., Hubbard J., Noro M., et al. The microstructure of di-alkyl chain cationic/nonionic surfactant mixtures: observation of coexisting lamellar and micellar phases and depletion induced phase separation. J Phys Chem B 109 (2005) 18107-18116
    • (2005) J Phys Chem B , vol.109 , pp. 18107-18116
    • Penfold, J.1    Staples, E.2    Ugazio, S.3    Soubiran, L.4    Hubbard, J.5    Noro, M.6
  • 26
    • 1442308357 scopus 로고    scopus 로고
    • Surface and solution behavior of the mixed dialkyl chain cationic and nonionic surfactants
    • Penfold J., Staples E., Tucker I., and Thomas R.K. Surface and solution behavior of the mixed dialkyl chain cationic and nonionic surfactants. Langmuir 20 (2004) 1269-1283
    • (2004) Langmuir , vol.20 , pp. 1269-1283
    • Penfold, J.1    Staples, E.2    Tucker, I.3    Thomas, R.K.4
  • 27
    • 49649095470 scopus 로고    scopus 로고
    • Self-assembly in mixed dialkyl chain cationic-nonionic surfactant mixtures: dihexadecyldimethyl ammonium bromide-monododecyl hexaethylene glycol (monododecyl dodecaethylene glycol) mixtures
    • Tucker I., Penfold J., Thomas R.K., Grillo I., Barker J.G., and Mildner D.F.R. Self-assembly in mixed dialkyl chain cationic-nonionic surfactant mixtures: dihexadecyldimethyl ammonium bromide-monododecyl hexaethylene glycol (monododecyl dodecaethylene glycol) mixtures. Langmuir 24 (2008) 7674-7687
    • (2008) Langmuir , vol.24 , pp. 7674-7687
    • Tucker, I.1    Penfold, J.2    Thomas, R.K.3    Grillo, I.4    Barker, J.G.5    Mildner, D.F.R.6
  • 28
    • 52649113225 scopus 로고    scopus 로고
    • Self-assembly in complex mixed surfactant solutions: the impact of dodecyl triethylene glycol on dihexadecyl dimethyl ammonium bromide
    • Tucker I., Penfold J., Thomas R.K., Grillo I., Mildner D.F.R., and Barker J.G. Self-assembly in complex mixed surfactant solutions: the impact of dodecyl triethylene glycol on dihexadecyl dimethyl ammonium bromide. Langmuir 24 (2008) 10089-10098
    • (2008) Langmuir , vol.24 , pp. 10089-10098
    • Tucker, I.1    Penfold, J.2    Thomas, R.K.3    Grillo, I.4    Mildner, D.F.R.5    Barker, J.G.6
  • 29
    • 65249178907 scopus 로고    scopus 로고
    • Spontaneous formation of nanovesicles in mixtures of nonionic and dialkyl chain cationic surfactants studied by surface tension and SANS
    • Grillo I., Penfold J., Tucker I., and Cousin F. Spontaneous formation of nanovesicles in mixtures of nonionic and dialkyl chain cationic surfactants studied by surface tension and SANS. Langmuir 25 (2009) 3932-3943
    • (2009) Langmuir , vol.25 , pp. 3932-3943
    • Grillo, I.1    Penfold, J.2    Tucker, I.3    Cousin, F.4
  • 32
    • 70349430195 scopus 로고    scopus 로고
    • R.F. Tabor, J. Eastoe, I. Grillo Time-resolved small-angle neutron scattering study of a lamellar to microemulsion phase transition. Soft matter, accepted for publication in march 2009. The lamellar to microemulsion phase transition induced by rapid dilution is followed by TR-SANS with a time resolution of 20 ms.
    • R.F. Tabor, J. Eastoe, I. Grillo Time-resolved small-angle neutron scattering study of a lamellar to microemulsion phase transition. Soft matter, accepted for publication in march 2009. The lamellar to microemulsion phase transition induced by rapid dilution is followed by TR-SANS with a time resolution of 20 ms.
  • 33
    • 3342900950 scopus 로고
    • Kinetics of step-wise micelle association
    • Aniansson E.A.G., and Wall S.N. Kinetics of step-wise micelle association. J Phys Chem 78 (1974) 1024-1030
    • (1974) J Phys Chem , vol.78 , pp. 1024-1030
    • Aniansson, E.A.G.1    Wall, S.N.2
  • 34
    • 0011063692 scopus 로고
    • On the kinetics of the micelle dissolution-formation equilibrium in solutions of cationic detergents. a comparison between temperature-jump and stopped-flow data
    • Tondre C., and Zana R. On the kinetics of the micelle dissolution-formation equilibrium in solutions of cationic detergents. a comparison between temperature-jump and stopped-flow data. J Colloid Interface Sci 66 (1978) 544-558
    • (1978) J Colloid Interface Sci , vol.66 , pp. 544-558
    • Tondre, C.1    Zana, R.2
  • 35
    • 33745788627 scopus 로고    scopus 로고
    • Prediction of an autocatalytic replication mechanism for micelle formation
    • Pool R., and Bolhuis P.G. Prediction of an autocatalytic replication mechanism for micelle formation. PRL 97 (2006) 018302-1:4
    • (2006) PRL , vol.97
    • Pool, R.1    Bolhuis, P.G.2
  • 36
    • 0032026068 scopus 로고    scopus 로고
    • Breakdown kinetics of fluorocarbon micelles studied by stopped-flow small-angle X-ray scattering
    • Eastoe J., Dalton J.S., DownerGareth Jones A., and Clarke D. Breakdown kinetics of fluorocarbon micelles studied by stopped-flow small-angle X-ray scattering. Langmuir 14 (1998) 1937-1939
    • (1998) Langmuir , vol.14 , pp. 1937-1939
    • Eastoe, J.1    Dalton, J.S.2    DownerGareth Jones, A.3    Clarke, D.4
  • 37
  • 38
    • 0036275341 scopus 로고    scopus 로고
    • Recent advances in the formation mechanisms of organized mesoporous materials
    • A review of possible mechanisms involved in the formation of mesoporous materials deduced by various in situ techniques.
    • Patarin J., Lebeau B., and Zana R. Recent advances in the formation mechanisms of organized mesoporous materials. COCIS 7 (2002) 102-115. A review of possible mechanisms involved in the formation of mesoporous materials deduced by various in situ techniques.
    • (2002) COCIS , vol.7 , pp. 102-115
    • Patarin, J.1    Lebeau, B.2    Zana, R.3
  • 39
    • 0141905061 scopus 로고    scopus 로고
    • 2/surfactant mesophase nucleate? Formation mechanism
    • The formation of mesoporous material is followed by TR-resolved SANS an SAXS. The precipitation occurs through a two-step mechanism, a random nucleation/growing process and a first order reorganisation from locally ordered cylinder to a hexagonal lattice.
    • 2/surfactant mesophase nucleate? Formation mechanism. Langmuir 19 (2003) 8503-8510. The formation of mesoporous material is followed by TR-resolved SANS an SAXS. The precipitation occurs through a two-step mechanism, a random nucleation/growing process and a first order reorganisation from locally ordered cylinder to a hexagonal lattice.
    • (2003) Langmuir , vol.19 , pp. 8503-8510
    • Né, F.1    Testard, F.2    Zemb, T.h.3    Grillo, I.4
  • 40
    • 3242661972 scopus 로고    scopus 로고
    • 3 from a supersaturated salt solution
    • 3 particles is investigated by means of TR-SAXS. The spherical particles are formed within the first 10 ms after mixing and have an amorphous structure. They rapidly aggregate without change of size. Addition of block-copolymer does not influence the size and morphology of the particles but slows the aggregation process. After 50 min, a transformation from an amorphous state to vaterite nanocrystallites has taken place.
    • 3 particles is investigated by means of TR-SAXS. The spherical particles are formed within the first 10 ms after mixing and have an amorphous structure. They rapidly aggregate without change of size. Addition of block-copolymer does not influence the size and morphology of the particles but slows the aggregation process. After 50 min, a transformation from an amorphous state to vaterite nanocrystallites has taken place.
    • (2004) J Colloid Interface Sci , vol.277 , pp. 84-94
    • Bolze, J.1    Pontoni, D.2    Ballauff, M.3    Narayanan, T.4    Cölfen, H.5
  • 41
    • 70349414883 scopus 로고    scopus 로고
    • C.N. Rochette, S. Rosenfeldt, A. Heiss, T. Narayanan, M. Ballauf, W. Jahnen-Dechent A shielding topology stabilizes the early stage protein-mineral complexes of fetuin-A and calcium phosphate: a time-resolved small angle X-ray study. Submitted 2009. The early stages of formation of complexes of calcium phosphate in presence of fetuin-A are followed by TR-SAXS. The formation of primary particles is very fast, less than 35 ms. Acting as a surface stabilizing layer, fetuin-A prevent the aggregation of the primary particles.
    • C.N. Rochette, S. Rosenfeldt, A. Heiss, T. Narayanan, M. Ballauf, W. Jahnen-Dechent A shielding topology stabilizes the early stage protein-mineral complexes of fetuin-A and calcium phosphate: a time-resolved small angle X-ray study. Submitted 2009. The early stages of formation of complexes of calcium phosphate in presence of fetuin-A are followed by TR-SAXS. The formation of primary particles is very fast, less than 35 ms. Acting as a surface stabilizing layer, fetuin-A prevent the aggregation of the primary particles.
  • 42
    • 34547372192 scopus 로고    scopus 로고
    • Probing in situ the nucleation and growth of gold nanoparticles by small-angle X-ray scattering
    • Formation and growth of gold particles are followed by time-resolved UV-vis, SAXS and WAXS coupled with a stopped-flow device with 200 ms time resolution. Two mechanisms are evidenced according to the ligand used.
    • Abécassis B., Testard F., Spalla O., and Barboux P. Probing in situ the nucleation and growth of gold nanoparticles by small-angle X-ray scattering. Nano Letter 7 (2007) 1723-1727. Formation and growth of gold particles are followed by time-resolved UV-vis, SAXS and WAXS coupled with a stopped-flow device with 200 ms time resolution. Two mechanisms are evidenced according to the ligand used.
    • (2007) Nano Letter , vol.7 , pp. 1723-1727
    • Abécassis, B.1    Testard, F.2    Spalla, O.3    Barboux, P.4
  • 43
    • 41149137733 scopus 로고    scopus 로고
    • Gold nanoparticle superlattice crystallisation probed in situ
    • 115504-1-4. The nucleation and growth of a 3D fcc super-lattice of gold nanoparticles is followed by TR-SAXS trigger by stopped-flow device. The super lattice nucleate around 10 s after the formation of the particles, they are limited in size and have a globular shape. Inside, the nanoparticles are separated by a capping agent bilayer. In a second step, they coalesce with time.
    • Abécassis B., Testard F., and Spalla O. Gold nanoparticle superlattice crystallisation probed in situ. PRL 100 (2008) 115504-1-4. The nucleation and growth of a 3D fcc super-lattice of gold nanoparticles is followed by TR-SAXS trigger by stopped-flow device. The super lattice nucleate around 10 s after the formation of the particles, they are limited in size and have a globular shape. Inside, the nanoparticles are separated by a capping agent bilayer. In a second step, they coalesce with time.
    • (2008) PRL , vol.100
    • Abécassis, B.1    Testard, F.2    Spalla, O.3
  • 44
    • 42249099208 scopus 로고    scopus 로고
    • Directed motion of proteins along tethered polyelectrolytes
    • The motion of proteins into densely grafted layer polyelectrolyte brushes is investigated by TR-SAXS combined with 20 ms time resolution. The system is composed by a colloidal particles composed of polystyrene sphere (SPB) with chemically grafted chains of polyacrylic acid. The protein is the bovine serum albumine (BSA). The uptake of the BSA is relatively fast and the final state is reached after 3 s. The total amount of adsorbed proteins scales with time as t1/4. The motion is governed by a balance of frictional and external forces.
    • Henzler K., Rosenfelt S., Wittenmann A., Harnau L., Finet S., Narayanan T., et al. Directed motion of proteins along tethered polyelectrolytes. PRL 100 (2008) 158301. The motion of proteins into densely grafted layer polyelectrolyte brushes is investigated by TR-SAXS combined with 20 ms time resolution. The system is composed by a colloidal particles composed of polystyrene sphere (SPB) with chemically grafted chains of polyacrylic acid. The protein is the bovine serum albumine (BSA). The uptake of the BSA is relatively fast and the final state is reached after 3 s. The total amount of adsorbed proteins scales with time as t1/4. The motion is governed by a balance of frictional and external forces.
    • (2008) PRL , vol.100 , pp. 158301
    • Henzler, K.1    Rosenfelt, S.2    Wittenmann, A.3    Harnau, L.4    Finet, S.5    Narayanan, T.6
  • 46
    • 0033532201 scopus 로고    scopus 로고
    • Characterization of transient intermediates in lysozyme folding with time-resolved small-angle X-ray scattering
    • Segel D.J., Bachmann A., James Hofrichter J., Hodgson K.O., Doniach S., and Kiefhaber T. Characterization of transient intermediates in lysozyme folding with time-resolved small-angle X-ray scattering. JMB 288 (1999) 489:499
    • (1999) JMB , vol.288
    • Segel, D.J.1    Bachmann, A.2    James Hofrichter, J.3    Hodgson, K.O.4    Doniach, S.5    Kiefhaber, T.6
  • 47
    • 0036349865 scopus 로고    scopus 로고
    • Fast compaction of a-lactalbumin during folding studied by stopped-flow X-ray scattering
    • Arai M., Ito K., Inobe T., Nakao M., Maki K., Kamagata K., et al. Fast compaction of a-lactalbumin during folding studied by stopped-flow X-ray scattering. JMB 321 (2002) 121-132
    • (2002) JMB , vol.321 , pp. 121-132
    • Arai, M.1    Ito, K.2    Inobe, T.3    Nakao, M.4    Maki, K.5    Kamagata, K.6
  • 48
    • 0037137630 scopus 로고    scopus 로고
    • Formation of a compact structural ensemble without fluorescence signature early during ubiquitin folding
    • Qin Z., Ervon J., Larios E., Gruebele M., and Kihara H. Formation of a compact structural ensemble without fluorescence signature early during ubiquitin folding. J Phys Chem B 106 (2002) 13040-13046
    • (2002) J Phys Chem B , vol.106 , pp. 13040-13046
    • Qin, Z.1    Ervon, J.2    Larios, E.3    Gruebele, M.4    Kihara, H.5
  • 49
    • 2942623941 scopus 로고    scopus 로고
    • Multiple probes reveal a native-like intermediate during low-temperature refolding of ubiquitin
    • Larios E., Li J.S., Schulten K., Kihara H., and Gruebele M. Multiple probes reveal a native-like intermediate during low-temperature refolding of ubiquitin. JMB 340 (2004) 115-125
    • (2004) JMB , vol.340 , pp. 115-125
    • Larios, E.1    Li, J.S.2    Schulten, K.3    Kihara, H.4    Gruebele, M.5
  • 52
    • 16244398102 scopus 로고    scopus 로고
    • Influence of nucleotide effectors on the kinetics of the quaternary structure transition of allosteric aspartate transcarbamylase
    • Tsuruta H., Kihara H., Sano T., Amemiya Y., and Vachette P. Influence of nucleotide effectors on the kinetics of the quaternary structure transition of allosteric aspartate transcarbamylase. JMB 348 (2005) 195-204
    • (2005) JMB , vol.348 , pp. 195-204
    • Tsuruta, H.1    Kihara, H.2    Sano, T.3    Amemiya, Y.4    Vachette, P.5
  • 53
    • 18844437767 scopus 로고    scopus 로고
    • A single amino acid substitution in the active site of Escherichia coli aspartate transcarbamoylase prevents the allosteric transition
    • Kimberly A., Stieglitz K.A., Pastra-Landis S.C., Xia J., Tsuruta H., and Kantrowitz E.R. A single amino acid substitution in the active site of Escherichia coli aspartate transcarbamoylase prevents the allosteric transition. JMB 349 (2005) 413-423
    • (2005) JMB , vol.349 , pp. 413-423
    • Kimberly, A.1    Stieglitz, K.A.2    Pastra-Landis, S.C.3    Xia, J.4    Tsuruta, H.5    Kantrowitz, E.R.6
  • 54
    • 54249099898 scopus 로고    scopus 로고
    • Time evolution of the quaternary structure of Escherichia coli aspartate transcarbamoylase upon reaction with the natural substrates and a slow, tight-binding inhibitor
    • A high time resolution (5 ms) study of the T to R transition of the quaternary structure of aspartate transcarbamoylase upon mixing with various affectors.
    • West J.M., Xia J., Tsuruta H., Wenyue Guo W., Elizabeth M., O'Day E.M., et al. Time evolution of the quaternary structure of Escherichia coli aspartate transcarbamoylase upon reaction with the natural substrates and a slow, tight-binding inhibitor. JMB 384 (2008) 206-218. A high time resolution (5 ms) study of the T to R transition of the quaternary structure of aspartate transcarbamoylase upon mixing with various affectors.
    • (2008) JMB , vol.384 , pp. 206-218
    • West, J.M.1    Xia, J.2    Tsuruta, H.3    Wenyue Guo, W.4    Elizabeth, M.5    O'Day, E.M.6
  • 56
    • 0042009114 scopus 로고    scopus 로고
    • The fastest global events in RNA folding: electrostatic relaxation and tertiary collapse of the tetrahymena ribozyme
    • The early stages of RNA refolding upon different salt conditions are followed by TR-SAXS. Three steps are observed: a partial collapse within a few milliseconds due to electrostatic screening; the collapse to a globular state in 100 ms and the tertiary native structure is formed after 1 s.
    • Das R., Kwok L.W., Millett I.S., Bai Y., Mills T.T., Jacobs J., et al. The fastest global events in RNA folding: electrostatic relaxation and tertiary collapse of the tetrahymena ribozyme. JMB 332 (2003) 311-319. The early stages of RNA refolding upon different salt conditions are followed by TR-SAXS. Three steps are observed: a partial collapse within a few milliseconds due to electrostatic screening; the collapse to a globular state in 100 ms and the tertiary native structure is formed after 1 s.
    • (2003) JMB , vol.332 , pp. 311-319
    • Das, R.1    Kwok, L.W.2    Millett, I.S.3    Bai, Y.4    Mills, T.T.5    Jacobs, J.6
  • 58
    • 0038810192 scopus 로고    scopus 로고
    • Mechanism of formation of DNA-cationic vesicle complexes
    • Barreleiro P.C.A., May R.P., and Lindman B. Mechanism of formation of DNA-cationic vesicle complexes. Faraday Discuss 122 (2002) 191-201
    • (2002) Faraday Discuss , vol.122 , pp. 191-201
    • Barreleiro, P.C.A.1    May, R.P.2    Lindman, B.3
  • 59
    • 33746825870 scopus 로고    scopus 로고
    • Dynamics of field-induced ordering in magnetic colloids studied by new time-resolved small-angle neutron-scattering techniques
    • Wiedenmann A., Keiderling U., Habicht K., Russina M., and Gähler R. Dynamics of field-induced ordering in magnetic colloids studied by new time-resolved small-angle neutron-scattering techniques. PRL 057202 (2006) 4
    • (2006) PRL , vol.057202 , pp. 4
    • Wiedenmann, A.1    Keiderling, U.2    Habicht, K.3    Russina, M.4    Gähler, R.5


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