A 3-D bismuth-organic framework containing 1-D cationic inorganic [Bi2O2]2+ chains

Inorganic Chemistry Communications

Volumn 12, Issue 10, 2009, Pages 1081-1084

  Tran, Dat T ^a   Chu, Deryn ^a   Oliver, Allen G ^b   Oliver, Scott R J ^b  

^a U S ARMY RESEARCH LABORATORY   (United States)

^b UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

1 D bismuth oxide chains; 1 D extended inorganic chains; 3,5 Pyridinedicarboxylate; Bismuth organic framework; Hydrothermal synthesis; Metal organic framework

Indexed keywords

EID: 70349424705     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2009.08.030     Document Type: Article

References (33)

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24. 2O (Aldrich, 98+%) and 0.25 g of pdc (Matrix Scientific, 95%) were added to a Nalgene beaker. After ca. 15 min. stirring, the solution was transferred to a 45 mL capacity Teflon-lined stainless steel autoclave. The autoclave was sealed and heated at 130 to 200 °C for 3 days. The crystals were collected by vacuum filtration, rinsed with deionized water and allowed to air-dry overnight. The crystal product from 130 °C weighed ca. 770 mg (yield: 83.7%). The crystal product from 165 °C weighed ca. 790 mg (yield: 85.9%), while the 200 °C product yielded a total of 809 mg (yield: 87.9%). Elemental analysis (Galbraith Laboratories Inc., Knoxville, TN) agrees well with the structural formula. Analyzed percentages of C, H and N were 9.39%, < 0.5% and 2.28%, compared with 13.6%, 0.48% and 2.28% calculated from the structure solution, respectively.
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