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70349420323
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note
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-1.
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70349425158
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note
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2 = 0.0949 (I > 2σ(I)). Crystal structure measurements for complexes 1 and 2 were performed on Bruker AXS SMART APEX II CCD diffractometer with graphite monochromatized Mo Kα radiation (λ = 0.71073 Å). All absorption corrections were performed using the SADABS program. Crystal structures were solved by the direct method. All non-hydrogen atoms were refined anisotropically. All hydrogen atoms were fixed at calculated positions with isotropic thermal parameters. All calculations were performed using the SHELX-97 program.
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