Simultaneous detection of selenium by atomic fluorescence and sulfur by molecular emission by flow-injection hydride generation with on-line reduction for the determination of selenate, sulfate and sulfite

Analytica Chimica Acta

Volumn 652, Issue 1-2, 2009, Pages 251-258

  Tyson, J F ^a   Palmer, C D ^b  

^a UNIVERSITY OF MASSACHUSETTS   (United States)

^b WADSWORTH CENTER   (United States)

Author keywords

Atomic fluorescence spectroscopy; Gas liquid separation; Molecular emission; On line microwave heating; Speciation; Sulfate reduction

Indexed keywords

ATOMIC FLUORESCENCE SPECTROSCOPY; GAS-LIQUID SEPARATION; MOLECULAR EMISSION; ON-LINE MICROWAVE HEATING; SPECIATION; SULFATE REDUCTION;

ACIDS; ARGON; ATOMIC SPECTROSCOPY; EMISSION SPECTROSCOPY; FLUORESCENCE; FLUORESCENCE SPECTROSCOPY; HEATING; HYDROCHLORIC ACID; HYDROGEN; INDUCTIVELY COUPLED PLASMA; LEAKAGE (FLUID); LIQUIDS; MICROWAVE GENERATION; MICROWAVE HEATING; MICROWAVE POWER TRANSMISSION; SELENIUM; SELENIUM COMPOUNDS; SODIUM; SODIUM SULFATE; SULFUR; SULFUR DETERMINATION;

HYDROGEN SULFIDE;

ACETIC ACID; ARGON; HYDROCHLORIC ACID; HYDROGEN; HYDROGEN SULFIDE; SELENIDE; SELENIUM; SULFATE; SULFITE; SULFUR;

ARTICLE; CALIBRATION; CHEMICAL REACTION; CHROMATOGRAPHY; CONTROLLED STUDY; DIFFUSION; FLOW INJECTION ANALYSIS; FLOW RATE; MICROWAVE RADIATION; PRIORITY JOURNAL; SPECTROFLUOROMETRY;

FLOW INJECTION ANALYSIS; MICROWAVES; SELENIUM COMPOUNDS; SPECTROMETRY, FLUORESCENCE; SPECTROPHOTOMETRY, ATOMIC; SULFATES; SULFITES; SULFUR;

EID: 70349332890     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2009.07.002     Document Type: Article

References (41)

1. Coombs G.F., and Clark L.C. Selenium and cancer. In: Heber D., Blackburn G.L., and Go V.L.W. (Eds). Nutritional Oncology (1999), Academic Press, New York 215-222
2. Whanger P.D. Selenium and its relationship to cancer: an update. Br. J. Nutr. 91 (2004) 11-28
3. Pryzynska K. Speciation analysis of some organic selenium compounds-a review. Analyst 121 (1996) 77R-83R
4. McSheehy S., Pohl P., Szpunnar J., Potin-Gauthier M., and Lobinski R. Analysis for selenium speciation in selenized yeast extracts by two-dimensional liquid chromatography with ICP-MS and electrospray MS-MS detection. J. Anal. At. Spectrom. 16 (2001) 68-73
5. Ogra Y., Ishiwata K., Iwashita Y., and Suzuki K.T. Simultaneous speciation of selenium and sulfur species in selenized odorless garlic (Allium sativum L. Shiro) and shallot (Allium ascalonicum) by HPLC-inductively coupled plasma-(octopole reaction system)-mass spectrometry and electrospray ionization-tandem mass spectrometry. J. Chromatogr. A 1093 (2005) 118-125
6. Uden P.C., Boakye H.T., Kahakachchi C., Hafezi R., Nolibos P., Block E., Johnson S., and Tyson J.F. Element selective characterization of stability and reactivity of selenium species in selenized yeast. J. Anal. At. Spectrom. 19 (2004) 65-73
7. Gabel-Jensen C., Lunoe K., Madsen K.G., Bendix J., Cornett C., Sturup S., Hansen H.R., and Gammelgaard B. Separation and identification of the selenium-sulfur amino acid S-(methylseleno)cysteine in intestinal epithelial cell homogenates by LC-ICP-MS and LC-ESI-MS after incubation with methylseleninic acid. J. Anal. At. Spectrom. 23 (2008) 727-732
8. Sturup S., Bendahl S., and Gammelgaard B. Optimization of LC-DRC-ICP-MS for the speciation of selenotrisulfides with simultaneous detection of sulfur and selenium as oxides combined with the determination of elemental and isotope ratios. J. Anal. At. Spectrom. 21 (2006) 201-203
9. Jensen B.P., Smith C., Wilson I.D., and Weidolf L. Sensitive sulfur specific detection of omeprazole metabolites in rat urine by high-performance liquid chromatography/inductively coupled plasma mass spectrometry. Rapid Commun. Mass Spectrom. 18 (2004) 181-183
10. In: Calokerinos A.C., in D.A., Stiles A.C., Calokerinos A., and Townshend (Eds). Flame Chemiluminescence Analysis by Molecular Cavity Detection (1994), John Wiley, Chichester
11. Dagnall R.M., Thompson K.C., and West T.S. Molecular-emission spectroscopy in cool flames. I. The behavior of sulfur species in a hydrogen-nitrogen diffusion flame and in a shielded air-hydrogen flame. Analyst 92 (1967) 506-512
12. Arowolo T.A., and Cresser M.S. Automated determination of sulfide by cool flame molecular emission spectrometry. Microchem. J. 45 (1992) 97-100
13. Thompson K.C. Atomic fluorescence determination of antimony, arsenic, selenium and tellurium using the hydride generation technique. Analyst 100 (1975) 307-310
14. Ebdon L.C., Wilkinson J.R., and Jackson K.W. A simple and sensitive continuous hydride generation system for the determination of arsenic and selenium by atomic absorption and atomic fluorescence spectrometry. Anal. Chim. Acta 136 (1982) 191-199
15. Tsujii K., and Kuga K. Determination of arsenic by nondispersive atomic fluorescence spectrometry with a gas sampling technique. Anal. Chim. Acta 72 (1974) 85-90
16. D'Ulivo A., Papoff P., and Festa D. A simultaneous multielement nondispersive atomic-fluorescence spectrometer using modulate sources and frequency discrimination of fluorescence signals. Talanta 30 (1983) 907-913
17. D'Ulivo A., Lampugnani L., and Zamboni R. Combined electrothermally heated quartz-tube atomizer for the hydride generation non-dispersive atomic fluorescence determination of selenium. J. Anal. At. Spectrom. 5 (1990) 225-229
18. Dedina J., and D'Ulivo A. Argon-shielded, highly fuel-rich, hydrogen-oxygen diffusion microflame: a new hydride atomizer. Spectrochim. Acta Part B 52 (1997) 1737-1746
19. Corns W.T., Stockwell P.B., Ebdon L., and Hill S.J. Development of an atomic fluorescence spectrometer for the hydride forming elements. J. Anal. At. Spectrom. 8 (1993) 71-77
20. Pitts L., Worsfold P., and Hill S.J. Selenium speciation-a flow-injection approach employing online microwave reduction followed by hydride generation-quartz furnace atomic-absorption spectrometry. Analyst 119 (1994) 2785-2788
21. Bryce D.W., Izquierdo A., and Decastro M.D.L. Speciation of selenium using flow injection hydride generation atomic fluorescence spectrometry. J. Anal. At. Spectrom. 10 (1995) 1059-1063
22. Moreno A.E., Perez-Conde C., and Camara C. Speciation of selenium in environmental matrices by flow injection analysis-hydride generation-atomic fluorescence spectrometry. Comparison of off-line, pseudo on-line and on-line extraction and reduction methods. J. Anal. At. Spectrom. 15 (2000) 681-686
23. Cobo-Fernandez M.G., Palacios M.A., Chakraborti D., Quevauviller P., and Camara C. On-line speciation of Se(VI), Se(IV) and trimethylselenium by HPLC microwave-oven hydride generation atomic-absorption spectrometry. Fresenius J. Anal. Chem. 351 (1995) 438-442
24. LaFuente J.M.G., Sanchez M.L.F., and Sanz-Medel A. Speciation of inorganic selenium and selenoaminoacids by on-line reversed-phase high-performance liquid chromatography focused microwave digestion hydride generation atomic detection. J. Anal. At. Spectrom. 11 (1996) 1163-1169
25. LaFuente J.M.G., Sanchez M.L.F., Marchante-Gayon J.M., Uria J.E.S., and Sanz-Medel A. On-line focused microwave digestion-hydride generation of inorganic and organic selenium: total determination and inorganic selenium speciation by atomic absorption spectrometry. Spectrochim. Acta Part B 51 (1996) 1849-1857
26. Bryce D.W., Izquierdo A., and Luque de Castro M.D. Use of focused microwaves for expeditive shortening of sample pretreatment digestion and reduction procedures prior to selenium speciation as selenium (IV) or selenium (VI). Analyst 120 (1995) 2171-2174
27. Arowolo T.A., and Cresser M.S. Automated determination of sulfite and sulfur dioxide by cool flame molecular emission spectrometry after reduction to hydrogen sulfide with sodium tetrahydroborate (III). Talanta 11 (1992) 1471-1478
28. Santos J.C.C., and Korn M. Exploiting sulphide generation and gas diffusion separation in a flow system for indirect sulphite determination in wines and fruit juices. Microchim. Acta 153 (2006) 87-94
29. Cmelik J., Machat J., Niedobova E., Otruba V., and Kanicky V. Determination of free and total sulfur dioxide in wine samples by vapour-generation inductively coupled plasma-optical-emission spectrometry. Anal. Bioanal. Chem. 383 (2005) 483-488
30. Rancke-Madsen E. Determination of sulfate by reduction with stannous chloride. Acta Chem. Scand. 773 (1949) 1952-1957
31. Kiba T., Takagi T., Yoshimur Y., and Kishi I. Tin(II) strong phosphoric acid, a new reagent for the determination of sulfate by reduction to hydrogen sulfide. Bull. Chem. Soc. Jpn. 28 (1955) 641-644
32. Steinbergs A., Iismaa O., Freney J.R., and Barrow N.J. Determination of total sulfur in soil and plant material. Anal. Chim. Acta 27 (1962) 158-164
33. Johnson C.M., and Arkley T. Microestimation of sulfur in plant materials, soils and irrigation waters. Anal. Chem. 26 (1954) 1525
34. Norwitz G. Spectrophotometric determination of sulfate in propellants, nitrocellulose. Analyst 96 (1971) 494-501
35. Gustafsson L. Determination of ultramicro amounts of sulfate as methylene blue-II. Talanta 4 (1960) 236-243
36. P. Yehl, Studies of Chemical Speciation Using Atomic Spectrometry, Ph.D. Dissertation, University of Massachusetts, Amherst, 1997.
37. Hoppstock K., and Lippert H. An improved gas-liquid separator for the selective determination of sulfide by ICP-OES using the evolution of hydrogen sulfide. At. Spectrosc. 18 (1997) 35-40
38. Tsalev D.L., Sperling M., and Welz B. Speciation determination of arsenic in urine by high-performance liquid chromatography hydride generation atomic absorption spectromety with on-line ultraviolet photooxidation. Analyst 123 (1998) 1703-1710
39. Vargas-Razo C., and Tyson J.F. Determination of cadmium by flow injection-chemical vapor generation-atomic absorption spectrometry. Fresenius J. Anal. Chem. 366 (2000) 182-190
40. Ebdon L.C., Hill S.J., Jameel M., Corns W.T., and Stockwell P.B. Automated determination of sulfide as hydrogen sulfide in waste streams by gas-phase molecular absorption spectrometry. Analyst 122 (1997) 689-693
41. Bogdanski S.L., Shakir I.M.A., Stephen W.I., and Townshend A. Determination of trace amounts of sulfate by molecular emission cavity analysis using a vaporization system. Analyst 104 (1979) 886-890