Solid State Nuclear Magnetic Resonance as a Tool to Explore Solvent-Free MALDI Samples

Journal of the American Society for Mass Spectrometry

Volumn 20, Issue 10, 2009, Pages 1906-1911

  Pizzala, Hélène ^a   Barrère, Caroline ^a   Mazarin, Michaël ^a   Ziarelli, Fabio ^b   Charles, Laurence ^a  

^a AIX MARSEILLE UNIVERSITY   (France)

^b Aix Marseille University   (France)

Author keywords

[No Author keywords available]

Indexed keywords

ANALYTES; ANALYTICAL SYSTEMS; CATIONIZATION; DIHYDROXYBENZOIC ACIDS; IONIZATION EFFICIENCY; MASS ANALYSIS; MASS SPECTRA; MATRIX; MATRIX ASSISTED LASER DESORPTION/IONIZATION; MOLAR RATIO; MOLECULAR ORGANIZATION; NMR SPECTRUM; SALT CONCENTRATION; SOLID SAMPLES; SOLID-STATE NUCLEAR MAGNETIC RESONANCE; SOLVENT FREE; STRONG INTERACTION; STRUCTURAL CHARACTERISTICS; SYNTHETIC POLYMERS; WATER MOLECULE;

CESIUM; DESORPTION; ETHYLENE; IONIZATION OF LIQUIDS; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYETHYLENE OXIDES; POLYMERS; POSITIVE IONS; RESONANCE;

NUCLEAR MAGNETIC RESONANCE;

CARBON 13; CESIUM; FLUORINE; GENTISIC ACID; MACROGOL; SOLVENT;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL INTERACTION; CHEMICAL MODIFICATION; CHEMICAL STRUCTURE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; IONIZATION; MATRIX ASSISTED LASER DESORPTION IONIZATION TIME OF FLIGHT MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLID STATE; STRUCTURE ANALYSIS;

EID: 70349216551     PISSN: 10440305     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jasms.2009.06.021     Document Type: Article

References (39)

1. Montaudo G., Montaudo M.S., and Samperi F. Matrix-Assisted Laser Desorption/Ionization Mass Spectrometry of Polymers (MALDI-MS). Mass Spectrometry of Polymers (2002), CRC Press, New York 419-522
2. Pasch H., and Schrepp W. Mass Spectrometry of Synthetic Polymers (2003), Springer, New York
3. Wallace, W. E.; Bauer, B. J.; Blair, W. R.; Flynn, K. M.; Gutman, C. M.; Kearsley, A. J. http://polymers.msel.nist.gov/maldirecipes/index.cfm.
4. Skelton R., Dubois F., and Zenobi R. A MALDI sample preparation method suitable for insoluble polymers. Anal. Chem. 72 (2000) 1707-1710
5. Trimpin S., Rouhanipour A., Az R., Rader H.J., and Mullen K. New Aspects in Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry: A Universal Solvent-Free Sample Preparation. Rapid Commun. Mass Spectrom. 15 (2001) 1364-1373
6. Doktycz S.J., Savickas P.J., and Krueger D.A. Matrix Sample Interactions in Ultraviolet Laser-Desorption of Proteins. Rapid Commun. Mass Spectrom. 5 (1991) 145-148
7. Preston L.M., Murray K.K., and Russell D.H. Reproducibility and Quantitation of Matrix-Assisted Laser-Desorption Ionization Mass-Spectrometry-Effects of Nitrocellulose on Peptide Ion Yields. Biol. Mass Spectrom. 22 (1993) 544-550
8. Chan T.W.D., Colburn A.W., Derrick P.J., Gardiner D.J., and Bowden M. Suppression of Matrix Ions in Ultraviolet-Laser Desorption-Scanning Electron-Microscopy and Raman-Spectroscopy of the Solid Samples. Org. Mass Spectrom. 27 (1992) 188-194
9. Westman A., Huthfehre T., Demirev P., and Sundqvist B.U.R. Sample Morphology Effects in Matrix-Assisted Laser-Desorption Ionization Mass-Spectrometry of Proteins. J. Mass Spectrom. 30 (1995) 206-211
10. Gusev A.I., Wilkinson W.R., Proctor A., and Hercules D.M. Improvement of Signal Reproducibility and Matrix/Co-Matrix Effects in MALDI Analysis. Anal. Chem. 67 (1995) 1034-1041
11. Horneffer V., Reichelt R., and Strupat K. Protein Incorporation into MALDI-Matrix Crystals Investigated by High Resolution Field Emission Scanning Electron Microscopy. Int. J. Mass Spectrom. 226 (2003) 117-131
12. Hanton S.D., Hyder I.Z., Stets J.R., Owens K.G., Blair W.R., Guttman C.M., and Giuseppetti A.A. Investigations of Electrospray Sample Deposition for Polymer MALDI Mass Spectrometry. J. Am. Soc. Mass Spectrom. 15 (2004) 168-179
13. Horneffer V., Forsmann A., Strupat K., Hillenkamp F., and Kubitscheck U. Localization of Analyte Molecules in MALDI Preparations by Confocal Laser Scanning Microscopy. Anal. Chem. 73 (2001) 1016-1022
14. Horneffer V., Strupat K., and Hillenkamp F. Localization of Noncovalent Complexes in MALDI Preparations by CLSM. J. Am. Soc. Mass Spectrom. 17 (2006) 1599-1604
15. Hanton S.D., Clark P.A.C., and Owens K.G. Investigations of Matrix-Assisted Laser Desorption/Ionization Sample Preparation by Time-of-Flight Secondary Ion Mass Spectrometry. J. Am. Soc. Mass Spectrom. 10 (1999) 104-111
16. Garden R.W., and Sweedler J.V. Heterogeneity Within MALDI Samples as Revealed by Mass Spectrometric Imaging. Anal. Chem. 72 (2000) 30-36
17. Mele A., and Malpezzi L. Noncovalent Association Phenomena of 2,5-Dihydroxybenzoic Acid with Cyclic and Linear Oligosaccharides. A Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometric and X-ray Crystallographic Study. J. Am. Soc. Mass Spectrom. 11 (2000) 228-236
18. Strupat K., Kampmeier J., and Horneffer V. Investigations of 2,5-DHB and Succinic Acid as Matrices for UV and IR MALDI. Part II: Crystallographic and Mass Spectrometric Analysis. Int. J. Mass Spectrom. 169 (1997) 43-50
19. Hanton S.D., McEvoy T.M., and Stets J.R. Imaging the Morphology of Solvent-Free Prepared MALDI Samples. J. Am. Soc. Mass Spectrom. 19 (2008) 874-881
20. Andrew E.R. Magic Angle Spinning. In: Grant D.M., and Harris R.K. (Eds). Encyclopedia of NMR (1996), Wiley, Chichester 2891-2901
21. Schaefer J., and Stejskal E.O. C. -13 Nuclear Magnetic-Resonance of Polymers Spinning at Magic Angle. J. Am. Chem. Soc. 98 (1976) 1031-1032
22. Sroka-Bartnicka A., Olejniczak S., Sochacki M., Biela T., and Potrzebowski M.J. Solid-State NMR Spectroscopy as a Tool Supporting Optimization of MALDI-TOF MS Analysis of Polylactides. J. Am. Soc. Mass Spectrom. 20 (2009) 67-72
23. Spickermann J., Martin K., Rader H.J., Mullen K., Schlaad H., Muller A.H.E., and Kruger R.P. Quantitative Analysis of Broad Molecular Weight Distributions Obtained by Matrix-Assisted Laser Desorption Ionization Time-of-Flight Mass Spectrometry. Eur. Mass Spectrom. 2 (1996) 161-165
24. Knochenmuss R., Lehmann E., and Zenobi R. Polymer Cationization in Matrix-Assisted Laser Desorption/Ionization. Eur. Mass Spectrom. 4 (1998) 421-426
25. Massiot D., Fayon F., Capron M., King I., Le Calve S., Alonso B., Durand J.O., Bujoli B., Gan Z.H., and Hoatson G. Modeling One- and Two-Dimensional Solid-State NMR Spectra. Magn. Reson. Chem. 40 (2002) 70-76
26. Gross U., Rudiger S., Grimmer A.R., and Kemnitz E.F. -19-NMR Solid State Investigations of Monovalent Alkali Metal Fluorides and Tetra-Alkylammonium Fluorides. J. Fluorine Chem. 115 (2002) 193-199
27. Hayashi S., and Hayamizu K. Accurate Determination of NMR Chemical-Shifts in Alkali-Halides and Their Correlation with Structural Factors. Bull. Chem. Soc. Jpn. 63 (1990) 913-919
28. Miller J.M. Fluorine-19 Magic-Angle Spinning NMR. Progr. Nucl. Magn. Reson. Spectrosc. 28 (1996) 255-281
29. Haisa M., Kashino S., Hanada S.I., Tanaka K., Okazaki S., and Shibagaki M. The Structures of 2-Hydroxy-5-Methylbenzoic Acid and Dimorphs of 2,5-Dihydroxybenzoic Acid. Acta Crystallogr. Sect. B Struct. Sci. 38 (1982) 1480-1485
30. Asseid F.M., Miller J.M., and Clark J.H. FT-IR and Si-29, Al-27, and F-19 Mas NMR-Studies of the Adsorption of CdF2, ZnF2, and CuF2 onto Montmorillonite K10-Activity Towards Friedel-Crafts Alkylation. Can. J. Chem. 70 (1992) 2398-2404
31. Wong A., Sham S., Wang S.N., and Wu G. A Solid-State Cs-133 Nuclear Magnetic Resonance and X-ray Crystallographic Study of Cesium Complexes with Macrocyclic Ligands. Can. J. Chem. 78 (2000) 975-985
32. Wiesbrock F., and Schmidbaur H. Crystal Structures of Rubidium and Cesium Anthranilates and Salicylates. Inorg. Chem. 42 (2003) 7283-7289
33. Claramunt R.M., Garcia M.A., Lopez C., and Elguero J. The Structure of 3,5-Dimethylpyrazole/Carboxylic Acids Co-Crystals. ARKIVOC (2005) 91-101
34. Fernandez-Bertran J., and Reguera E. Proton Transfer in the Solid State: Mechano-Chemical Reactions of Fluorides with Acidic Substances. Solid State Ionics 112 (1998) 351-354
35. Fernandez-Bertran J., Alvarez J.C., and Reguera E. Proton Transfer in the Solid State: Reactions of Organic Acids and Amines. Solid State Ionics 106 (1998) 129-135
36. Paneque A., Reguera E., Fernandez-Bertran J., and Yee-Madeira H. Mechano-Chemical Reactions of Fluorides with Hemin. J. Fluorine Chem. 113 (2002) 1-5
37. Gerken M., Boatz J.A., Kornath A., Haiges R., Schneider S., Schroer T., and Christe K.O. The F-19 NMR shifts are not a measure for the nakedness of the fluoride anion. J. Fluorine Chem. 116 (2002) 49-58
38. Dogruel D., Nelson R.W., and Williams P. The effects of matrix pH and cation availability on the matrix-assisted laser desorption ionization mass spectrometry of poly(methyl methacrylate). Rapid Commun. Mass Spectrom. 10 (1996) 801-804
39. King, R. C.; Owens, K. G. Proceedings of the 43rd Annual Conference on Mass Spectrometry and Allied Topics; Atlanta, GA, 1995.