In situ ethylation of organolead, organotin and organomercury species by bromomagnesium tetraethylborate prior to GC-ICP-MS analysis

Journal of Separation Science

Volumn 32, Issue 14, 2009, Pages 2426-2433

  Nsengimana, Hermogène ^a   Cukrowska, Ewa M ^a   Dinsmore, Andrew ^a   Tessier, Emmanuel ^b   Amouroux, David ^b  

^a UNIVERSITY OF THE WITWATERSRAND   (South Africa)

^b UNIVERSITÉ DE PAU ET DES PAYS DE L'ADOUR   (France)

Author keywords

Bromomagnesium tetraethylborate; Derivatisation; Ethylation; Organometallic compounds

Indexed keywords

ANALYTICAL METHOD; AQUEOUS SAMPLES; BROMOMAGNESIUM TETRAETHYLBORATE; DERIVATISATION; EFFECT OF PH; ETHYLATION; IN-SITU; ORGANOMERCURY; ORGANOMERCURY COMPOUNDS; ORGANOMETALLIC COMPOUNDS; ORGANOTINS; SPECIES-SPECIFIC ISOTOPE DILUTION; TETRAETHYLBORATE;

INDUCTIVELY COUPLED PLASMA; INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY; ISOTOPES; LEAD; LEAD COMPOUNDS; MASS SPECTROMETERS; MERCURY (METAL); METAL RECOVERY; ORGANOMETALLICS; PH EFFECTS; TIN;

MERCURY COMPOUNDS;

BROMOMAGNESIUM TETRAETHYLBORATE; CHEMICAL COMPOUND; ORGANOLEAD COMPOUND; ORGANOMERCURY COMPOUND; ORGANOTIN COMPOUND; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CHEMICAL ANALYSIS; CHEMICAL MODIFICATION; CHEMICAL REACTION; CONTROLLED STUDY; DERIVATIZATION; ISOTOPE DILUTION ASSAY; MASS FRAGMENTOGRAPHY; PH; PRIORITY JOURNAL; PROCESS DEVELOPMENT; PROCESS OPTIMIZATION; PRODUCT RECOVERY; VALIDATION STUDY;

BORANES; ENVIRONMENTAL POLLUTANTS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HYDROGEN-ION CONCENTRATION; ORGANOMETALLIC COMPOUNDS;

EID: 70349177760     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200900204     Document Type: Article

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