Applying analytical ultracentrifugation to nanocrystal suspensions

Nanotechnology

Volumn 20, Issue 35, 2009, Pages

  Jamison, Jennifer A ^a   Krueger, Karl M ^a   Mayo, J T ^a   Yavuz, Cafer T ^a   Redden, Jacina J ^a   Colvin, Vicki L ^a  

^a RICE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ANALYSIS METHOD; ANALYTICAL APPROACH; ANALYTICAL ULTRACENTRIFUGATION; BEST PRACTICE; CADMIUM SELENIDES; DATA COLLECTION; HYDRODYNAMIC SIZE; INORGANIC NANOCRYSTALS; NANO-MATERIALS; NANOCRYSTAL DENSITY; NANOCRYSTAL SOLUTION; PROTEIN COMPLEXES; QUANTITATIVE ANALYSIS; QUANTITATIVE INTERPRETATION; SAMPLE TEMPERATURE; SEDIMENTATION COEFFICIENTS; SOLUTION PHASE; SOLUTION PROPERTY; THEORETICAL MODELS;

BIOCHEMISTRY; CADMIUM; CADMIUM COMPOUNDS; CENTRIFUGATION; FLUID DYNAMICS; SEDIMENTATION;

NANOCRYSTALS;

CADMIUM SELENIDE; NANOCRYSTAL;

ARTICLE; CONTROLLED STUDY; HYDRODYNAMICS; OPTICAL DENSITY; PARTICLE SIZE; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SEDIMENTATION; TEMPERATURE SENSITIVITY; TRANSMISSION ELECTRON MICROSCOPY; ULTRACENTRIFUGATION;

EID: 70349162939     PISSN: 09574484     EISSN: 13616528     Source Type: Journal    
DOI: 10.1088/0957-4484/20/35/355702     Document Type: Article

References (67)

1. Calabretta M, Jamison J A, Falkner J C, Liu Y, Yuhas B D, Matthews K S and Colvin V L 2005 Analytical ultracentrifugation for characterizing nanocrystals and their bioconjugates Nano Lett. 5 963-7
2. Colfen H, Tirosh S and Zaban A 2003 Nanocrystal surface structure analysis by analytical ultracentrifugation Langmuir 19 10654-9
3. Niederberger M, Garnweiter G, Krumeich F, Nesper R, Colfen H and Antonietti M 2004 Tailoring the surface and solubility properties of nanocrystalline titania by a nonaqueous in situ functionalization process Chem. Mater. 16 1202-8
4. Nichols J B, Kraemer E O and Bailey E D 1932 The particle size and constitution of colloidal ferric oxide J. Phys. Chem. 36 326-39
5. Pinna N, Grancharov S, Beato P, Bonville P, Antonietti M and Niederberger M 2005 Magnetite nanocrystals: nonaqueous synthesis, characterization, and solubility Chem. Mater. 17 3044-9 (Pubitemid 40844708)
6. Bronstein L, Sidorov S N, Valetsky P M, Hartmann J, Colfen H and Antonietti M 1999 Induced micellization by interaction of poly(2-vinylpyridine)- block-poly(ethylene oxide) with metal compounds. Micelle characteristics and metal nanoparticle formation Langmuir 15 6256-62
7. Colfen H, Schnablegger H, Fisher A, Jentoft F C, Weinberg G and Schlogl R 2002 Particle growth kinetics in zirconium sulfate aqueous solutions followed by dynamic light scattering and analytical ultracentrifugation: implications for thin film deposition Langmuir 18 3500-9
8. Svedberg E B, Ahner J, Sukla N, Ehrman S H and Schilling K 2005 FePt nanoparticle hydrodynamic size and densities form the polyol process as determined by analytical ultracentrifugation Nanotechnology 16 953-6
9. Bootz A, Vogel V, Schubert D and Kreuter J 2004 Comparison of scanning electron microscopy, dynamic light scattering and analytical ultracentrifugation for the sizing of poly(butylcyanoacrylate) nanoparticles Eur. J. Pharm. Biopharm. 57 369-75
10. Bronstein L, Chernyshov D M, Timofeeva G I, Dubrovina L V, Valetsky P M, Obolonkova E S and Khokhlov A R 2000 Interaction of polystyrene-block- poly(ethylene oxide) micelles with cationic surfactant in aqueous solutions. Metal colloid formation in hybrid systems Langmuir 16 3626-32 (Pubitemid 30858702)
11. Bronstein L M et al 2006 Morphology of hybrid poly styrene-block- poly(ethylene oxide) micelles: analytical ultracentrifugation and sans studies J. Colloid Interface Sci. 299 944-52
12. Colfen H, Volkel A, Shinichi E, Kobold U, Kaufmann J, Puhlmann A, Goltner C and Wachernig H 2002 Mechanism of nanoparticle-enhanced turbidimetric assays applying nanoparticles of different size and immunoreactivity Langmuir 18 7623-8
13. Colfen H 2004 Analytical ultracentrifugation of nanoparticles Polym. News 29 101-16
14. Colfen H 2004 Analysis of nanoparticles<10 nm by analytical ultracentrifugation ACS Symposium Series vol 881 pp119-37
15. Colfen H and Pauck T 1997 Determination of particle size distributions with angstrom resolution Colloid Polym. Sci. 275 175-80
16. Deshpande A S, Pinna N, Beato P, Antonietti M and Niederberger M 2004 Synthesis and characterization of stable and crystalline Ce(1-x)ZrxO2 nanoparticle sols Chem. Mater. 16 2599-604
17. Gittins D I and Caruso F 2001 Tailoring the polyelectrolyte coating of metal nanoparticles J. Phys. Chem. B 105 6846-52
18. Gohon Y, Giusti F, Prata C, Charvolin D, Timmins P, Ebel C, Tribet C and Popot J L 2006 Well-defined nanoparticles formed by hydrophobic assembly of a short and polydisperse random terpolymer, amphipol A8-35 Langmuir 22 1281-90
19. Joralemon M J, Murthy K S, Remsen E E, Becker M L and Wooley K L 2004 Synthesis, characterization, and bioavailability of mannosylated shell cross-linked nanoparticles Biomacromolecules 5 903-13
20. Joralemon M J, Smith N L, Holowka D, Baird B and Wooley K L 2005 Antigen-decorated shell cross-linked nanoparticles: synthesis, characterization, and antibody interactions Bioconjug. Chem. 16 1246-56
21. Joralemon M J, O'Reilly R K, Hawker C J and Wooley K L 2005 Shell click-crosslinked (Scc) nanoparticles: a new methodology for synthesis and orthogonal functionalization J. Am. Chem. Soc. 127 16892-99
22. Lechner M D and Machtle W 1999 Characterization of nanoparticles Macromol. Symp. 145 1-7
23. Lechner M D and Machtle W 2000 Characterization of nanoparticles Trends in Advanced Materials and Processes vol 352 (Zurich-Uetikon: Trans Tech Publications) pp87-90
24. Machtle W 1999 High-resolution, submicron particle size distribution analysis using gravitational-sweep sedimentation Biophys. J. 76 1080-91
25. Machtle W and Borger L 2006 Analytical Ultracentrifugation of Polymers and Nanoparticles 1st edn (Berlin: Springer)
26. Mayya K S, Schoeler B and Caruso F 2003 Preparation and organization of nanoscale polyelectrolyte-coated gold nanoparticles Adv. Funct. Mater. 13 183-8
27. Mayya K S and Caruso F 2003 Phase transfer of surface-modified gold nanoparticles by hydrophobization with alkylamines Langmuir 19 6987-93
28. 6 J. Phys. Chem. B 101 4175-83
29. Remsen E E, Thurmond K B II and Wooley K L 1999 Solution and surface charge properties of shell cross-linked Knedel nanoparticles Macromolecules 32 3685-9
30. Sokolova V, Prymak O, Meyer-Zaika W, Colfen H, Rehage H, Shukla A and Epple M 2006 Synthesis and characterization of DNA-functionalized calcium phosphate nanoparticles Mater.wiss. Werkst.tech. 37 441-5 (Pubitemid 44012805)
31. ThiesWeesie D M E, Philipse A P and Lekkerkerker H N W 1996 Sedimentation of bidisperse uncharged colloidal sphere suspensions: influence of viscosity and irregular surfaces J. Colloid Interface Sci. 177 427-38
32. ThiesWeesie D M E, Philipse A P, Nagele G, Mandl B and Klein R 1995 Nonanalytical concentration-dependence of sedimentation of charged silica spheres in an organic-solvent-experiments and calculations J. Colloid Interface Sci. 176 43-54
33. Tziatos C, Precup A A, Weidl C H, Schubert U S, Schuck P, Durchschlag H, Machtle W, van den Broek J A and Schubert D 2002 Studies on the partial specific volume of a poly(ethylene glycol) derivative in different solvent systems Prog. Colloid Polym. Sci. 119 24-30
34. Vogel V, Langer K, Balthasar S, Schuck P, Machtle W, Haase W, van den Broek J A, Tziatzios C and Schubert D 2002 Characterization of serum albumin nanoparticles by sedimentation velocity analysis and electron microscopy Prog. Colloid Polym. Sci. 119 31-6
35. Vogel V, Gohy J-F, Lohnmeijer B G G, van der Broek J A, Haase W, Schubert U S and Schubert D 2003 Metallo-supramolecular micelles: studies by analytical ultracentrifugation and electron microscopy J. Polym. Sci. A 41 3159-68
36. Vogel V et al 2005 Oligonucleotide-protamine-albumin nanoparticles: preparation, physical properties, and intracellular distribution J. Control. Release 103 99-111
37. Wang H and Wen C S 1999 Concentration-dependent sedimentation of stable magnetic dispersions J. Colloid Interface Sci. 213 606-8
38. Arnold M S, Suntivich J, Stupp S I and Hersam M C 2008 Hydrodynamic characterization of surfactant encapsulated carbon nanotubes using an analytical ultracentrifuge ACS Nano 2 2291-300
39. Liu T, Luo S D, Xiao Z W, Zhang C and Wang B 2008 Preparative ultracentrifuge method for characterization of carbon nanotube dispersions J. Phys. Chem. C 112 19193-202
40. Lange H 1995 Comparative test of methods to determine particle-size and particle-size distribution in the submicron range Part. Part. Syst. Charact. 12 148-57
41. Jamison J A, Krueger K M, Yavuz C T, Mayo J T, Lecrone D, Redden J J and Colvin V L 2008 Size-dependent sedimentation properties of nanocrystals ACS Nano 2 311-9
42. Svedberg T and Nichols J B 1923 Determination of size and distribution of size of particles by centrifugal methods J. Am. Chem. Soc. 45 2910-7
43. Yu W W and Peng X G 2002 Formation of high-quality CdS and other II-VI semiconductor nanocrystals in noncoordinating solvents: tunable reactivity of monomers Angew. Chem. 41 2368-71
44. Krueger K M, Al-Somali A M, Falkner J C and Colvin V L 2005 Characterization of nanocrystalline CdSe by size exclusion chromatography Anal. Chem. 77 3511-5
45. Yu W W, Qu L, Guo W and Peng X 2003 Experimental determination of the extinction coefficient of CdTe, CdSe, and CdS nanocrystals Chem. Mater. 15 2854-60
46. 4 nanocrystals Science 314 964-7
47. Schuck P 2000 Size-distribution analysis of macromolecules by sedimentation velocity ultracentrifugation and Lamm equation modeling Biophys. J. 78 1606-19
48. Schuck P and Rossmanith P 2000 Determination of the sedimentation coefficient distribution G*(S) by least-squares boundary modeling Biopolymers 54 328-41
49. Lechner M D and Machtle W 1999 Determination of the particle size distribution of 5-100 nm nanoparticles with the analytical ultracentrifuge: consideration and correction of diffusion effects Prog. Colloid Polym. Sci. 113 37-43
50. Leibowitz J, Lewis M S and Schuck P 2002 Modern analytical ultracentrifugation in protein science: a tutorial review Protein Sci. 11 2067-79
51. Demeler B, Saber H and Hansen J C 1997 Identification and interpretation of complexity in sedimentation velocity boundaries Biophys. J. 72 397-407
52. van Holde K E and Weischet W O 1978 Boundary analysis of sedimentation velocity experiments with monodisperse and paucidisperse solutes Biopolymers 17 1387-403
53. Sood S M and Slattery C W 2001 Association of mixtures of the two major forms of beta-casein from human milk J. Dairy Sci. 84 2163-9
54. Cole J L 1996 Characterization of human cytomegalovirus protease dimerization by analytical centrifugation Biochemistry 35 15601-10
55. Lavrenko P, Okatova O, Korneeva E and Finkelmann H 1999 Temperature effects in hydrodynamic properties of comb-like polymer with laterally attached mesogenic units Polymer 40 1701-7
56. Hahn M, Gornitz E and Dautzenberg H 1998 Synthesis and properties of ionically modified polymers with Lcst behavior Macromolecules 31 5616-23
57. Colfen H, Harding S E, Wilson E K, Scrutton N S and Winzor D J 1997 Low temperature solution behaviour of methylophilus methylotrophus electron transferring flavoprotein: a study by analytical ultracentrifugation Eur. Biophys. J. 25 411-6
58. Colfen H, Harding S E, Wilson E K, Packman L C and Scrutton N S 1996 Homodimeric and expanded behaviour of trimethylamine dehydrogenase in solution at different temperatures Eur. Biophys. J. 24 159-64
59. Beck K, Gambee J E, Bohan C A and Bachinger H P 1996 The C-terminal domain of cartilage matrix protein assembles into a triple-stranded alpha-helical coiled-coil structure J. Mol. Biol. 256 909-23
60. Pathmamanoharan C and Philipse A P 1998 Preparation and properties of monodisperse magnetic cobalt colloids grafted with polyisobutene J. Colloid Interface Sci. 205 340-53
61. van der Kooij F M, Philipse A P and Dhont J K G 2000 Sedimentation and diffusion in suspensions of sterically stabilized colloidal platelets Langmuir 16 5317-23
62. Dogic Z, Philipse A P, Fraden S and Dhont J K G 2000 Concentration- dependent sedimentation of colloidal rods J. Chem. Phys. 113 8368-80
63. Donselaar L N and Philipse A P 1999 Interactions between silica colloids with magnetite cares: diffusion, sedimentation and light scattering J. Colloid Interface Sci. 212 14-23
64. Donselaar L N, Philipse A P and Suurmond J 1997 Concentration-dependent sedimentation of dilute magnetic fluids and magnetic silica dispersions Langmuir 13 6018-25
65. Schulte C, Morrison C A and Garrett R A 1974 Ribosomal proteins. 76. protein-ribonucleic acid interactions in Escherichia coli ribosomes. Solution studies on S4-16s ribonucleic acid and L24-23s ribonucleic acid binding Biochemistry 13 1032-7
66. Stowell C and Korgel B A 2001 Self-assembled honeycomb networks of gold nanocrystals Nano Lett. 1 595-600
67. Lisiecki I, Albouy P A and Pileni M P 2004 'Supra' crystal: control of the ordering of self-organization of cobalt nanocrystals at the mesoscopic scale J. Phys. Chem. B 108 20050-5