Quantification of organic acids in particulate matter by coupling of thermally assisted hydrolysis and methylation with thermodesorption-gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1216, Issue 38, 2009, Pages 6642-6650

  Beiner, K ^a   Plewka, A ^a   Haferkorn, S ^a   Iinuma, Y ^a   Engewald, W ^b   Herrmann, H ^a  

^a LEIBNIZ INSTITUTE FOR TROPOSPHERIC RESEARCH   (Germany)

^b UNIVERSITY OF LEIPZIG   (Germany)

Author keywords

On line derivatisation; Organic acids; Size segregated atmospheric particles; Thermally assisted hydrolysis and methylation; Thermodesorption

Indexed keywords

A-THERMAL; AMBIENT AEROSOLS; ATMOSPHERIC PARTICLES; CALIBRATION DATA; COUPLED MASS; CURIE POINTS; DERIVATISATION; DETERMINATION OF ORGANIC ACIDS; DICARBOXYLIC ACID; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HEATING TEMPERATURES; IMPACTORS; LIMITS OF DETECTION; LITERATURE DATA; MINIMAL SAMPLE; NANOGRAMS; ON-LINE DERIVATISATION; PARTICULATE MATTER; QUANTIFICATION LIMIT; QUANTITATIVE METHOD; REACTION TIME; RELATIVE STANDARD DEVIATIONS; REPRODUCIBILITIES; SAMPLE PREPARATION; SAMPLING TECHNIQUE; SAMPLING TIME; SIZE SEGREGATED ATMOSPHERIC PARTICLES; TETRAMETHYL AMMONIUM HYDROXIDE; TETRAMETHYLAMMONIUM; THERMALLY ASSISTED HYDROLYSIS AND METHYLATION; THERMODESORPTION; VOLATILE ORGANIC ACID; VOLUME CONCENTRATION;

ALKYLATION; CALIBRATION; CAPILLARY ELECTROPHORESIS; CHROMATOGRAPHIC ANALYSIS; FATTY ACIDS; HYDROLYSIS; MASS SPECTROMETERS; MASS SPECTROMETRY; METHYLATION; ORGANIC ACIDS; SAMPLING; SEMICONDUCTOR SWITCHES; SURFACE CHEMISTRY; TEMPERATURE PROGRAMMED DESORPTION; THERMAL DESORPTION;

GAS CHROMATOGRAPHY;

ADIPIC ACID; AMMONIUM DERIVATIVE; ARACHIDIC ACID; AZELAIC ACID; BEHENIC ACID; CARBOXYLIC ACID; DECANOIC ACID; DICARBOXYLIC ACID; FATTY ACID; LAURIC ACID; PHENYLRIMETHYLAMMONIUM HYDROXIDE; PIMELIC ACID; SEBACIC ACID; STEARIC ACID; TERPENE; TETRAMETHYLAMMONIUM ACETATE; TETRAMETHYLAMMONIUM HYDROXIDE; UNCLASSIFIED DRUG;

AIR ANALYSIS; AIR SAMPLING; AMBIENT AIR; ARTICLE; CAPILLARY ELECTROPHORESIS; CONTROLLED STUDY; DERIVATIZATION; DESORPTION; GAS CHROMATOGRAPHY; HEATING; HYDROLYSIS; MASS SPECTROMETRY; METHYLATION; PARTICULATE MATTER; PRIORITY JOURNAL; PYROLYSIS; QUANTITATIVE ANALYSIS; REACTION TIME; REPRODUCIBILITY; SENSITIVITY ANALYSIS; TEMPERATURE;

AIR POLLUTANTS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HYDROLYSIS; METHYLATION; PARTICULATE MATTER; QUATERNARY AMMONIUM COMPOUNDS; SENSITIVITY AND SPECIFICITY;

EID: 68949180235     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.07.054     Document Type: Article

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