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Inorganic Chemistry

Volumn 48, Issue 16, 2009, Pages 7800-7804

Synthesis, structure, and properties of the noncentrosymmetric hydrated borate Na2B5O8(OH)·2H2O

(7) Wang, Yongjiang a,b Pan, Shilie a Tian, Xuelin a Zhou, Zhongxiang a Liu, Gang c Wang, Jide c Jia, Dianzeng c

a XINJIANG TECHNICAL INSTITUTE OF PHYSICS AND CHEMISTRY (China)

b UNIVERSITY OF CHINESE ACADEMY OF SCIENCES (China)

c XINJIANG UNIVERSITY (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 68949161565 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic900700u Document Type: Article

Times cited : (71)

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- During the process of synthesizing Na2B5Og(OH)·2H 2O, when the reagents and initial chemical ratio were changed, another crystal Na2B4O5-(OH)4 · 3H2O was obtained, which was reported by Carmelo et al (Carmelo, G, Silivo, M, Fernando, S. Am. Mineral. 1973, 58, 523, The detailed information is as follows: 0.8013 g (2.00 × 10-2 mol) of NaOH and 3.7099 g (6.00 × 10-2 mol) of H3BO3 were combined with 1 mL of H2O in Teflon-lined autoclave. The autoclave was heated to 180 °C gradually, held for 2 days, and cooled to room temperature for 3 days. The crystal with sizes up to 6 × 5 × 4 mm was obtained in the autoclave. The photograph of Na2B4O5(OH)4 · 3H 2O crystal is shown in Figure S2a in the Supporting Information, and the crystal purity
- 2O crystal is shown in Figure S2a in the Supporting Information, and the crystal purity was verified using X-ray diffraction, shown in Figure S2b in the Supporting Information. Its crystal data and structure refinement information are summarized in Table S2a in the Supporting Information. Final atomic coordinates and equivalent isotropic displacement parameters of the compound are listed in Table S2b in the Supporting Information. Selected interatomic distances and angles are given in Tables S2c and d in the Supporting Information.

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