Development and validation of a multi-residue method for the determination of pesticides in honeybees using acetonitrile-based extraction and gas chromatography-tandem quadrupole mass spectrometry

Journal of Chromatography A

Volumn 1216, Issue 37, 2009, Pages 6522-6531

  Walorczyk, Stanisław ^a   Gnusowski, Bogusław ^a  

^a INSTITUTE OF PLANT PROTECTION NATIONAL RESEARCH INSTITUTE   (Poland)

Author keywords

Gas chromatography; Honeybees; Pesticide residue analysis; Tandem quadrupole mass spectrometry

Indexed keywords

ACETONITRILE-WATER MIXTURE; ANALYTICAL METHOD; CALIBRATION CURVES; CITRATE BUFFER; CONCENTRATION LEVELS; CONCENTRATION RANGES; CONFIDENCE LEVELS; COVERAGE FACTORS; DISPERSIVE SOLID PHASE EXTRACTION; EMPIRICAL MODEL; GC-MS/MS; GRAPHITIZED CARBON BLACK; HONEYBEES; LOW TEMPERATURES; MAGNESIUM SULPHATES; MATRIX; OCTADECYL; PESTICIDE RESIDUE ANALYSIS; REAL SAMPLES; RELATIVE STANDARD DEVIATIONS; SALTING OUT; SAMPLE PREPARATION; SECONDARY AMINES; SPE CLEAN-UP; TANDEM QUADRUPOLE; TANDEM QUADRUPOLE MASS SPECTROMETRY; TOPDOWN;

ACETONITRILE; AGRICULTURAL CHEMICALS; AMINES; CARBON BLACK; CHROMATOGRAPHIC ANALYSIS; EXTRACTION; MAGNESIUM; MASS SPECTROMETERS; MASS SPECTROMETRY; PESTICIDES; RECOVERY; SODIUM; SODIUM CHLORIDE; SOLAR RADIATION; UNCERTAINTY ANALYSIS;

GAS CHROMATOGRAPHY;

ACETOCHLOR; ACETONITRILE; AMINE; BUFFER; CARBON; CARBOXIN; CITRIC ACID; CLOMAZONE; DIFLUFENICAN; DIMOXYSTROBIN; DINICONAZOLE; ETHOFUMESATE; ETOFENPROX; FENBUCONAZOLE; FLUFENACET; FLUQUINCONAZOLE; FLUTIAFOL; FLUXASTROBIN; MAGNESIUM SULFATE; METHACRIFOS; MEVINPHOS; PENCYCURON; PESTICIDE; PICOXYSTROBIN; PYRAZOPHOS; PYRIDABEN; SODIUM CHLORIDE; TRIFLUMIZOLE; UNCLASSIFIED DRUG; WATER;

ARTICLE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; FOOD CONTAMINATION; FREEZING; GAS CHROMATOGRAPHY; HONEYBEE; LOW TEMPERATURE; PESTICIDE SPRAYING; PRECIPITATION; PRIORITY JOURNAL; QUADRUPOLE MASS SPECTROMETRY; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

ACETONITRILES; AGROCHEMICALS; ANALYTIC SAMPLE PREPARATION METHODS; ANIMALS; BEES; CHROMATOGRAPHY, GAS; ENVIRONMENTAL POLLUTANTS; PESTICIDE RESIDUES; POLAND; TANDEM MASS SPECTROMETRY;

APOIDEA; HEXAPODA;

EID: 68749094047     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.07.045     Document Type: Article

References (36)

1. Barnett E.A., Charlton A.J., and Fletcher M.R. Pest Manag. Sci. 63 (2007) 1051
2. Rossi S., Dalpero A.P., Ghini S., Colombo R., Sabatini A.G., and Girotti S. J. Chromatogr. A 905 (2001) 223
3. Fernández M., Padrón C., Marconi L., Ghini S., Colombo R., Sabatini A.G., and Girotti S. J. Chromatogr. A 922 (2001) 257
4. Fernández M., Picó Y., Girotti S., and Mañes J. J. Agric. Food Chem. 49 (2001) 3540
5. Morzycka B. J. Chromatogr. A 982 (2002) 267
6. Rancan M., Rossi S., and Sabatini A.G. J. Chromatogr. A (2006) 60
7. Totti S., Fernández M., Ghini S., Picó Y., Fini F., Mañes J., and Girotti S. Talanta 69 (2006) 724
8. Charlton A.J.A., and Jones A. J. Chromatogr. A 1141 (2007) 117
9. Fernández-Alba A.R., and García-Reyes J.F. Trends Anal. Chem. 27 (2008) 973
10. Anastassiades M., Lehotay S.J., Stajnbaher D., and Schenck F.J. J. AOAC Int. 86 (2003) 412
11. Lehotay S.J., de Kok A., Hiemstra M., and van Bodegraven P. J. AOAC Int. 88 (2005) 595
12. Lehotay S.J., Maštovská K., and Lightfield A.R. J. AOAC Int. 88 (2005) 615
13. Kmellár B., Fodor P., Pareja L., Ferrer C., Martínez M.A., Valverde A., and Fernandez-Alba A.R. J. Chromatogr. A 1215 (2008) 37
14. Fernández Moreno J.L., Garrido Frenich A., Plaza Bolaños P., and Martínez Vidal J.L. J. Mass Spectrom. 43 (2008) 1235
15. Lesueur C., Knittl P., Gartner M., Mentler A., and Fuerhacker M. Food Control 19 (2008) 906
16. Romero-González R., Garrido Frenich A., and Martínez Vidal J.L. Talanta 76 (2008) 211
17. Payá P., Anastassiades M., Mack D., Sigalova I., Tasdelen B., Oliva J., and Barba A. Anal. Bioanal. Chem. 389 (2007) 1697
18. Diéz C., Traag W.A., Zommer P., Marinero P., and Atienza J. J. Chromatogr. A 1131 (2006) 11
19. Walorczyk S. J. Chromatogr. A 1165 (2007) 200
20. Nguyen T.D., Lee B.S., Lee B.R., and Lee G.H. Rapid Commun. Mass Spectrom. 21 (2007) 3115
21. Walorczyk S. J. Chromatogr. A 1208 (2008) 202
22. Nguyen T.D., Han E.M., Seo M.S., Kim S.R., Yun M.Y., Lee D.M., and Lee G.H. Anal. Chim. Acta 619 (2008) 67
23. Lesueur C., Gartner M., Mentler A., and Fuerhacker M. Talanta 75 (2008) 284
24. Cunha S.C., Lehotay S.J., Maštovská K., Fernandes J.O., Beatriz M., and Oliveira P.P. J. Sep. Sci. 30 (2007) 620
25. Lehotay S.J., Maštovská K., and Yun S.J. J. AOAC Int. 88 (2005) 630
26. Štěpán R., Hajšlová J., Kocourek V., and Tichá J. Anal. Chim. Acta 520 (2004) 245
27. Pool C.F. J. Chromatogr. A 1158 (2007) 241
28. Fernández M., Picó Y., and Mañes J. J. Food Protect. 65 (2002) 1602
29. Jimínez J.J., Bernal J.L., del Nozal M.J., Martín M.T., and Bernal J. J. Chromatogr. A 1129 (2006) 262
30. Lentza-Rizos C., Avramides E.J., and Cherasco F. J. Chromatogr. A 912 (2001) 135
31. Li L., Xu Y., Pan C., Zhou Z., Jiang S., and Liu F. J. AOAC Int. 90 (2007) 1387
32. Goulart S.M., de Queiroz M.E., Neves A.A., and de Queiroz J.H. Talanta 75 (2008) 1320
33. Chen S., Yu X., He X., Xie D., Fan Y., and Peng J. Food Chem. 113 (2009) 1297
34. Walorczyk S. Rapid Commun. Mass Spectrom. 22 (2008) 3791
35. Method validation and quality control procedures for pesticide residues analysis in food and feed, document no. SANCO/2007/3131, European Commission, Brusseld, October 31, 2007.
36. van der Lee M.K., van der Weg G., Traag W.A., and Mol H.G.J. J. Chromatogr. A 1186 (2008) 325