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Volumn 48, Issue 15, 2009, Pages 7000-7002

Solution structure of physiological cu(His)2: Novel considerations into imidazole coordination

Author keywords

[No Author keywords available]

Indexed keywords

COPPER BIS(HISTIDINATE); DIETHYL PYROCARBONATE; HISTIDINE; IMIDAZOLE; IMIDAZOLE DERIVATIVE; ORGANOMETALLIC COMPOUND;

EID: 68149092704     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9010983     Document Type: Article
Times cited : (17)

References (26)
  • 1
    • 0016260535 scopus 로고    scopus 로고
    • Sundberg, R..; Martin, B. Chem. Rev. 1974, 74, 471-517.
    • Sundberg, R.).; Martin, B. Chem. Rev. 1974, 74, 471-517.
  • 3
    • 0001139290 scopus 로고    scopus 로고
    • Sarkar, B. Chem. Rev. 1999, 99, 2535-2544.
    • (1999) Chem. Rev , vol.99 , pp. 2535-2544
    • Sarkar, B.1
  • 19
    • 0017054425 scopus 로고    scopus 로고
    • Loosemore, M. 1; Pratt, R. F. FEBS Lett. 1976, 72, 155-158.
    • Loosemore, M. 1; Pratt, R. F. FEBS Lett. 1976, 72, 155-158.
  • 20
    • 68149172176 scopus 로고    scopus 로고
    • 2O). One set was then treated with a 10 molar excess ethanolic solution of DEPC for 30 min at 27 °C, while the other set acting as the control was treated just with ethanol. The reaction was terminated using excess Tris-HC1 buffer (pH 8.3). The optical density of the DEPC-containing tubes was measured at around 240 nm using respective control tubes containing ethanol on a Shimatzu 1601 spectrophotometer.
    • 2O). One set was then treated with a 10 molar excess ethanolic solution of DEPC for 30 min at 27 °C, while the other set acting as the control was treated just with ethanol. The reaction was terminated using excess Tris-HC1 buffer (pH 8.3). The optical density of the DEPC-containing tubes was measured at around 240 nm using respective control tubes containing ethanol on a Shimatzu 1601 spectrophotometer.
  • 21
    • 68149157767 scopus 로고    scopus 로고
    • 2] (pH 7.4) were treated with various concentrations of ethanolic solutions of DEPC (0-50 mM) for 30 min at 27 °C. The reaction was terminated using excess Tris-HCl buffer (pH 8.3). Spectra were measured between 400 and 800 nm against water containing equal of ethanol on a Jasco V630 spectrophotometer.
    • 2] (pH 7.4) were treated with various concentrations of ethanolic solutions of DEPC (0-50 mM) for 30 min at 27 °C. The reaction was terminated using excess Tris-HCl buffer (pH 8.3). Spectra were measured between 400 and 800 nm against water containing equal volumes of ethanol on a Jasco V630 spectrophotometer.
  • 23
    • 68149161594 scopus 로고    scopus 로고
    • MS experiments were carried out on Applied Biosystem's API 4000Q trap system coupled with an Agilent 1200 series liquid Chromatograph provided with Analyst 1.4.2 software. A mobile phase was methanol and water with 0.1% formic acid. The electrospray ionization was used in positive polarity. The source parameters are ion spray voltage 5.5k, nebulizer gas 20 psi, heater gas 55 psi, and source temperature 350 °C. A C18 column (55 × 2 × 3 μm) was used with a flow rate of 0.3 mL/min.
    • MS experiments were carried out on Applied Biosystem's API 4000Q trap system coupled with an Agilent 1200 series liquid Chromatograph provided with Analyst 1.4.2 software. A mobile phase was methanol and water with 0.1% formic acid. The electrospray ionization was used in positive polarity. The source parameters are ion spray voltage 5.5k, nebulizer gas 20 psi, heater gas 55 psi, and source temperature 350 °C. A C18 column (55 × 2 × 3 μm) was used with a flow rate of 0.3 mL/min.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.