2D and 3D DOSY 1H NMR, a useful tool for analysis of complex mixtures: Application to herbal drugs or dietary supplements for erectile dysfunction

Journal of Pharmaceutical and Biomedical Analysis

Volumn 50, Issue 4, 2009, Pages 602-612

  Balayssac, Stéphane ^a   Trefi, Saleh ^a   Gilard, Véronique ^a   Malet Martino, Myriam ^a   Martino, Robert ^a   Delsuc, Marc André ^b  

^a UPS)   (France)

^b INSTITUT DE GÉNÉTIQUE ET DE BIOLOGIE MOLÉCULAIRE ET CELLULAIRE   (France)

Author keywords

2D and 3D DOSY 1H NMR; Adulteration; Herbal dietary supplements; PDE 5 inhibitors; Thiomethisosildenafil

Indexed keywords

ACTIVE MAN HERB; ACTIVE WOMEN HERB; AMINO ACID; ASCORBIC ACID; CHUI HUA SAN; DEXPANTHENOL; EXCIPIENT; HERBACEOUS AGENT; HERBAL V; HERBAL VIVA; HYDROXYHOMOSILDENAFIL; MASCULIN 1; MAX SIZE; NICOTINIC ACID; PENIS KRAFT; PENIS VOLUME PLUS; PHOSPHODIESTERASE V INHIBITOR; POWER TAB; PYRIDOXINE; SEX GOLD; SILDENAFIL; STAMINA RX; START UP; SUGAR; TADALAFIL; THIOMETHISOSILDENAFIL; THIOSILDENAFIL; UNCLASSIFIED DRUG; VARDENAFIL; VIAGER; VIAMAX SENSITIVE DESIRE; VIGUEUR 7; YEILUS MIRACULE;

ANALYTIC METHOD; ARTICLE; DIET SUPPLEMENTATION; DRUG FORMULATION; DRUG MARKETING; DRUG MIXTURE; DRUG STRUCTURE; ERECTILE DYSFUNCTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; SEXUAL FUNCTION;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DIETARY SUPPLEMENTS; DRUG CONTAMINATION; ERECTILE DYSFUNCTION; EXCIPIENTS; HUMANS; MAGNETIC RESONANCE SPECTROSCOPY; MALE; PHOSPHODIESTERASE 5 INHIBITORS; PHOSPHODIESTERASE INHIBITORS; PHYTOTHERAPY; PLANTS, MEDICINAL; PYRIMIDINES; SULFONES;

EID: 67849096871     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2008.10.034     Document Type: Article

References (30)

1. Shin M.-H., Hong M.-K., Kim W.-S., Lee Y.-J., and Jeoung Y.-C. Food Addit. Contam. 20 (2003) 793-796
2. Shin C., Hong M., Kim D., and Lim Y. Magn. Reson. Chem. 42 (2004) 1060-1062
3. Blok-Tip L., Zomer B., Bakker F., Hartog K.D., Hamzink M., ten Hove J., Vredenbregt M., and de Kaste D. Food Addit. Contam. 21 (2004) 737-748
4. Gratz S.R., Flurer C.L., and Wolnik K.A. J. Pharm. Biomed. Anal. 36 (2004) 525-533
5. Zhu X., Xiao S., Chen B., Zhang F., Yao S., Wan Z., Yang D., and Han H. J. Chromatogr. A 1066 (2005) 89-95
6. Fleshner N., Harvey M., Adomat H., Wood C., Eberding A., Hersey K., and Guns E. J. Urol. 174 (2005) 636-641
7. Zou P., Oh S.S.-Y., Hou P., Low M.Y., and Koh H.L. J. Chromatogr. A 1104 (2006) 113-122
8. Zou P., Hou P., Low M.Y., and Koh H.L. Food Addit. Contam. 23 (2006) 446-451
9. Kuo-Chih L., Yi-Chu L., Mu-Chang T., and Jer-Huei L. J. Food Drug Anal. 14 (2008) 19-23
10. Reepmeyer J.C., and Woodruff J.T. J. Chromatogr. A 1125 (2006) 67-75
11. Gratz S.R., Gamble B.M., and Flurer R.A. Rapid Commun. Mass Spectrom. 20 (2006) 2317-2327
12. Abdel-Hamid M.E. J. Liq. Chromatogr. Relat. Technol. 29 (2006) 591-603
13. Park H.J., Jeong H.K., Chang M.I., Im M.H., Jeong J.Y., Choi D.M., Park K., Hong M.K., Youm J., Han S.B., Kim D.J., Park J.H., and Kwon S.W. Food Addit. Contam. 24 (2007) 122-129
14. Reepmeyer J.C., and Woodruff J.T. J. Pharm. Biomed. Anal. 44 (2007) 887-893
15. Reepmeyer J.C., Woodruff J.T., and Avignon D.A. J. Pharm. Biomed. Anal. 43 (2007) 1615-1621
16. Lam Y.H., Poon W.T., Lai C.K., Chan A.Y.-W., and Mak T.W.-L. J. Pharm. Biomed. Anal. 46 (2008) 804-807
17. Venhuis B.J., Blok-Tip L., and de Kaste D. Forensic Sci. Int. 177 (2008) e25-e27
18. Venhuis B.J., Zomer G., and de Kaste D. J. Pharm. Biomed. Anal. 46 (2008) 814-817
19. Zou P., Hou P., Oh S.S.-Y., Chong Y.M., Bloodworth B.C., Low M.Y., and Koh H.L. J. Pharm. Biomed. Anal. 47 (2008) 279-284
20. Zou P., Hou P., Oh S.S.-Y., Ge X., Bloodworth B.C., Low M.Y., and Koh H.L. J. Pharm. Biomed. Anal. 47 (2008) 255-259
21. Trefi S., Gilard V., Malet-Martino M., and Martino R. J. Pharm. Biomed. Anal. 44 (2007) 743-754
22. Trefi S., Gilard V., Balayssac S., Malet-Martino M., and Martino R. J. Pharm. Biomed. Anal. 46 (2008) 707-722
23. Trefi S., Routaboul C., Hamieh S., Gilard V., Malet-Martino M., and Martino R. J. Pharm. Biomed. Anal. 47 (2008) 103-113
24. Newman J.M., and Jerschow A. Anal. Chem. 79 (2007) 2957-2960
25. Tramesel D., Catherinot V., and Delsuc M.A. J. Magn. Reson. 188 (2007) 56-67
26. NMRtec, Available from http://www.nmrtec.com.
27. Zhong D., Xing J., Zhang S., and Sun L. Rapid Commun. Mass Spectrom. 16 (2002) 1836-1843
28. Poon W.T., Lam Y.H., Lai C.K., Chan A.Y.W., and Mak T.W.L. Hong Kong Med. J. 13 (2007) 359-363
29. Nilsson M., Gil A.M., Delgadillo I., and Morris G.A. Chem. Commun. (2005) 1737-1739
30. Wu D., Chen A., and Johnson Jr. C.S. J. Magn. Reson. Ser. A 121 (1996) 88-91