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See Supporting Information
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See Supporting Information.
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84869727146
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X-ray data for 1a · (C5H12) 3: Red platelet (0. 3 × 0. 2 × 0. 2 mm3J from 1-chloronaphthalene/C5H12. Space group: Pnma; a, 21. 661(3) Å; b, 22. 721(4) Å; c, 17. 128(3) Å; V, 8430(2) Å3; Z, 4; T, 100(2) K; Nrefunique, 11 521; R1, 0. 076; Rw, 0. 196
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w = 0. 196.
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15
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84869727147
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X-ray data for 1b · CHCl3: red platelet (0. 4 × 0. 1 × 0. 1 mm3) from CHCl3/CS2. Space group: Pnma; a, 18. 298(5) Å; b, 17. 955(5) Å; c, 17. 352(5) Å; V, 5701(3) Å3; Z, 4; T, 100(2) K; Nref(unique, 7277; R 1, 0. 077; Rw, 0. 200. 1b · CS2: Red prism (0. 2 × 0. 2 × 0. 05 mm3) from CS2/C5H12. Space group: Pnma; a, 18. 311(5) Å; b, 17. 969(4) Å; c, 17. 344(5) Å; V, 5707(3) Å3; Z, 4; T, 100(2) K; Nrefunique, 7858; R1, 0. 063; Rw, 0. 171. For 1b · 1, 2-C6H 4 Cl2, 1b · C6H5CH 3, an
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1.875, see Supporting Information.
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