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The minor peaks including m/z = 4439.9 shown in Figure 4a is assignable to the [M - N2 Na] . This experimental fact that an azido group has undergone decomposition during the ionization process of the MALDI-TOF MS analysis was already reported. Please see ref 33 and the following reference
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Hiki S.,Kataoka K.;Bioconjugate Chem.;The minor peaks including m/z = 4439.9 shown in Figure 4a is assignable to the [M - N2 Na] . This experimental fact that an azido group has undergone decomposition during the ionization process of the MALDI-TOF MS analysis was already reported. Please see ref 33 and the following reference.
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3- PVL-Ct≡CH during the ionization process of the MALDI-TOF MS measurement was not completely observed (Figure 4b).
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3- PVL-Ct≡CH during the ionization process of the MALDI-TOF MS measurement was not completely observed (Figure 4b).
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42
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67651126724
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The decomposition reaction of polyester main chain during the click cyclization was found when we used THF as solvent.In addition, we performed the click cyclization in DMF at the lower temperatures than 120-C, at which the click condensation reaction predominantly occurred compared with click cyclization reaction.
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The decomposition reaction of polyester main chain during the click cyclization was found when we used THF as solvent. In addition, we performed the click cyclization in DMF at the lower temperatures than 120-C, at which the click condensation reaction predominantly occurred compared with click cyclization reaction.
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