A 13C solid-state NMR analysis of vitamin D compounds

Solid State Nuclear Magnetic Resonance

Volumn 36, Issue 1, 2009, Pages 24-31

  Mousavi, Mansoureh ^a   Yu, Steve S F ^a   Tzou, Der Lii M ^a,b  

^a INSTITUTE OF CHEMISTRY   (Taiwan)

^b NATIONAL CHIAYI UNIVERSITY   (Taiwan)

Author keywords

13C chemical shifts; NMR; Sterol ring conformation; Vitamin D2; Vitamin D3

Indexed keywords

13C CHEMICAL SHIFTS; ANGLE SPINNING; CARBON ATOMS; CHEMICAL SHIFT TENSORS; COMPUTER MOLECULAR MODELING; ENERGY MINIMIZATION; HETERONUCLEAR CORRELATION; MOLECULAR CONFORMATION; MOLECULAR CONFORMERS; MULTIPLET PATTERNS; NMR; NMR SPECTRUM; PROTONATED; RING CONFORMATIONS; S-TRANS; SOLID STATE NMR; SOLID-STATE NMR SPECTROSCOPY; SOLUTION NMR; STEROL RING CONFORMATION; VITAMIN-D;

ALCOHOLS; ATOMIC SPECTROSCOPY; ATOMS; CHEMICAL ELEMENTS; CHEMICAL SHIFT; MOLECULAR DYNAMICS; MOLECULAR GRAPHICS; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RESONANCE; SOLID STATE PHYSICS;

CONFORMATIONS;

VITAMIN D;

ANISOTROPY; ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; COMPUTER SIMULATION; CONFORMATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ANISOTROPY; COMPUTER SIMULATION; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, MOLECULAR; MOLECULAR CONFORMATION; VITAMIN D;

EID: 67651055006     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ssnmr.2009.04.003     Document Type: Article

References (39)

1. Cantorna M.T., and Mahon B.D. Exp. Biol. Med. (Maywood) 229 (2004) 1136-1142
2. Cantorna M.T., Hayes C.E., and DeLuca H.F. Proc. Natl. Acad. Sci. USA 93 (1996) 7861-7864
3. Zella J.B., and DeLuca H.F. J. Cell Biochem. 88 (2003) 216-222
4. Adorini L., Amuchastegui S., and Daniel K.C. Immunol. Lett. 100 (2005) 34-41
5. Adorini L. Cell Immunol. 233 (2005) 115-124
6. Sanders G.M., Pot J., and Havinga E. Fortschr. Chem. Org. Naturst. 27 (1969) 131-157
7. Braun P.B., Hornstra J., Knoble C., Rutten E.W.M., and Romers C. Acta Cryst. B 29 (1973) 463-469
8. Knoble C., Braun P.B., Romers C., and Hornstra J. Acta Cryst. B 28 (1972) 2097-2103
9. Hull S.E., Leban I., Main P., White P.S., and Woolfson M.M. Acta Cryst. 32 (1976) 2374-2381
10. Toan T., DeLuca H.F., and Dahl L.F. J. Org. Chem. 41 (1976) 3476-3478
11. Antzutkin O.N., Balbach J.J., Leapman R.D., Rizzo N.W., Reed J., and Tycko R. Proc. Natl. Acad. Sci. USA 97 (2000) 13045-13050
12. Jack E., Newsome M., Stockley P.G., Radford S.E., and Middleton D.A. J. Am. Chem. Soc. 128 (2006) 8098-8099
13. Tycko R. Curr. Opin. Chem. Biol. 4 (2000) 500-506
14. Hartmann S.R., and Hahn E.L. Phys. Rev. 128 (1962) 2042-2053
15. Andrew E.R., Bradbury A., and Eades R.G. Nature 182 (1958) 1659
16. Yang J.H., Ho Y., and Tzou D.L. Magn. Reson. Chem. 46 (2008) 718-725
17. Cuffini S.L., Ellena J.F., Mascarenhas Y.P., Ayala A.P., Sielser H.W., Filho J.M., Monti G.A., Aiassa V., and Sperandeo N.R. Steroids 72 (2007) 261-269
18. Park J.S., Kang H.W., Park S.J., and Kim C.K. Eur. J. Pharm. Biopharm. 60 (2005) 407-412
19. Lesage A., Bardet M., and Emsley L. J. Am. Chem. Soc. 121 (1999) 10987-10993
20. Wing R.M., Okamura W.H., Pirio M.R., Sine S.M., and Norman A.W. Science 186 (1974) 939-941
21. Okamura W.H., Norman A.W., and Wing R.M. Proc. Natl. Acad. Sci. USA 71 (1974) 4194-4197
22. Wing R.M., Okamura W.H., Rego A., Pirio M.R., and Norman A.W. J. Am. Chem. Soc. 97 (1975) 4980-4985
23. Mueller L.J., Elliott D.W., Kim K.C., Reed C.A., and Boyd P.D. J. Am. Chem. Soc. 124 (2002) 9360-9361
24. Olsen R.A., Struppe J., Elliott D.W., Thomas R.J., and Mueller L.J. J. Am. Chem. Soc. 125 (2003) 11784-11785
25. Kolodziejski W., Wozniak K., Herold J., Dominiak P.M., and Kutner A. J. Mol. Struct. 734 (2005) 149-155
26. Bennett A.E., Rienstra C.M., Auger M., Lakshmi K.V., and Griffin R.G. J. Chem. Phys. 103 (1995) 6951-6954
27. Burum D.P., Linder M., and Ernst R.R. J. Magn. Reson. 44 (1981) 173-188
28. Burum D.P., and Bielecki A. J. Magn. Reson. 94 (1991) 645-652
29. Caravatti P., Braunschweiler L., and Ernst R.R. Chem. Phys. Lett. 100 (1983) 305-310
30. Sun H. J. Phys. Chem. B 102 (1998) 7338-7364
31. Fletton R.A., Harris R.K., Kenwright A.M., Lancaster R.W., Packer K.J., and Sheppard N. Spectrochim. Acta Part A 43 (1987) 1111-1120
32. Harris R.K., Joyce S.A., Pickard C.J., Cadars S., and Emsley L. Phys. Chem. Chem. Phys. 8 (2006) 137-143
33. Bhacca N.S., Giannini D.D., Jankowski W.S., and Wolff M.E. J. Am. Chem. Soc. 95 (1973) 8421-8426
34. Commodari F., Sclavos G., Ibrahimi S., Khiat A., and Boulanger Y. Magn. Reson. Chem. 43 (2005) 444-450
35. Furuta T., Suzuki A., Matsuzawa M., Shibasaki H., and Kasuya Y. Steroids 68 (2003) 693-703
36. Jacobsen N.E., Kover K.E., Murataliev M.B., Feyereisen R., and Walker F.A. Magn. Reson. Chem. 44 (2006) 467-474
37. Ho Y., Tzou D.L., and Chu F.I. Magn. Reson. Chem. 44 (2006) 581-585
38. Maricq M.M., and Waugh J.S. J. Chem. Phys. 70 (1979) 3300-3316
39. Herzfeld J., and Berger A.E. J. Chem. Phys. 73 (1980) 6021-6030