Specific GC-MS/MS stable-isotope dilution methodology for free 9- and 10-nitro-oleic acid in human plasma challenges previous LC-MS/MS reports

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 877, Issue 26, 2009, Pages 2895-2908

  Tsikas, Dimitrios ^a   Zoerner, Alexander ^a   Mitschke, Anja ^a   Homsi, Yahya ^a   Gutzki, Frank Mathias ^a   Jordan, Jens ^a  

^a HANNOVER MEDICAL SCHOOL   (Germany)

Author keywords

Fatty acids; Lipids; Nitration; Stable isotopes; Standardization; Validation

Indexed keywords

3-NITROTYROSINE; CHEMICAL IONIZATION; COLLISION-INDUCED DISSOCIATION; ELECTRON CAPTURE; GC-MS/MS; HEALTHY SUBJECTS; HUMAN BLOOD SAMPLES; HUMAN PLASMAS; INTERNAL STANDARDS; ISOTOPE DILUTIONS; LC-MS/MS; MEAN CONCENTRATIONS; PARENT IONS; PHYSIOLOGICAL CONDITION; PLASMA CONCENTRATION; PLASMA SAMPLES; REACTION MONITORING; SPE EXTRACTION; STABLE ISOTOPES; UNSATURATED FATTY ACIDS; VALIDATION;

AMINO ACIDS; BIOLOGICAL SYSTEMS; BIOMOLECULES; ESTERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; ISOMERS; ISOTOPES; LABELS; LIPIDS; NITRATION; OLEIC ACID; PLASMA (HUMAN); PLASMAS; SOLVENT EXTRACTION; SOLVENTS; STANDARDIZATION;

ACIDS;

10 NITRO OLEIC ACID; 3 NITROTYROSINE; 9 NITRO OLEIC ACID; BENZYL DERIVATIVE; NITROGEN 15; OLEIC ACID; PENTAFLUOROBENZYL; STABLE ISOTOPE; TYROSINE; UNCLASSIFIED DRUG; UNSATURATED FATTY ACID;

ARTICLE; BLOOD SAMPLING; COLLISIONALLY ACTIVATED DISSOCIATION; CONTROLLED STUDY; DILUTION; ELECTRON CAPTURE NEGATIVE ION CHEMICAL IONIZATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; IONIZATION; LIQUID CHROMATOGRAPHY; MASS FRAGMENTOGRAPHY; NITRATION; PLASMA; PRIORITY JOURNAL; SOLVENT EXTRACTION;

ADULT; CHROMATOGRAPHY, LIQUID; FEMALE; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; MALE; MIDDLE AGED; NITROGEN ISOTOPES; OLEIC ACIDS; TANDEM MASS SPECTROMETRY;

EID: 67650713019     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2008.12.062     Document Type: Article

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