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Volumn 38, Issue 7, 2009, Pages 694-695

Synthesis and structural characterization of a novel three-dimensional molybdenum-oxygen framework constructed from Mo3O9 units

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EID: 67650487492 PISSN: 03667022 EISSN: 13480715 Source Type: Journal
DOI: 10.1246/cl.2009.694 Document Type: Article

Times cited : (6)

References (24)

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- Preparation of 1: A mixture of Na2MoO 4·2H2O (5.99 mmol, 1.45 g, NH 2OH·HCl (1.58 mmol, 0.11 g, and water (556 mmol, 10 mL) was stirred for 2 h in air, and its pH was adjusted to 1-2 with hydrochloric acid (2 mol·L-1, The resulting mixture was sealed in a 20-mL Telfon-lined reactor, heated to 180°C, and kept for 5 days. After cooling to room temperature, light blue block crystals were collected in 70% yield based on Na2MoO4·2H2O, by filtration, washed with water, and dried at ambient temperature. Anal. Calcd for H2Mo3O10, Mo, 63.98. Found: Mo, 63.72. IR spectrum: 3506, 1625, 1417, 974, 907, 611, 520 cm-1. Experimental results proved that when NH2OH·HCl was removed from the reaction system, 1 could not be isolated. The role of NH 2OH·HCl is not well unders
- 2OH·HCl is not well understood.

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