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Inorganic Chemistry

Volumn 48, Issue 14, 2009, Pages 6329-6331

Chair-Boat Form Transformation of Piperazine-Containing Ligand toward the Preparation of Dirhenium Metallacycles

(4) Lee, Chung Chou a Hsu, Shu Chun a,b Lai, Long Li b Lu, Kuang Lieh a

a INSTITUTE OF CHEMISTRY (Taiwan)

b NATIONAL CHI NAN UNIVERSITY (Taiwan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 67650465918 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic900040a Document Type: Article

Times cited : (35)

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- Synthesis for 1: A mixture of Re2(CO)10 (65.3 mg, 0.10 mmol, bpp (24.0 mg, 0.10 mmol, and H2dhnq (19.0 mg, 0.10 mmol) in toluene (6 mL) in a 20 mL Teflon flask was placed in a steel bomb. The bomb was placed in an oven maintained at 160 °C for 72 h and then cooled to 25 °C Compound 1 was contained as black crystals and powder that were filtered off, washed with butanol and n-hexane, and then air-dried. Yield: 73.0 mg (69, 1H NMR (400 MHz, DMSO-d6, δ 7.68 (d, 4H, J=4.5 Hz, Hα-Py, 7.07 (s, 4H, dhnq, 6.60 (d, 4H, J=4.5 Hz, H β-Py, 3.78 (d, 4H, J=8.4 Hz, piperazine, 3.44 (d, 4H, J, 8.4 Hz, piperazine, IR (THF, cm-1, v(C≡0) 2016 (sh, 2010 (vs, 1910 (vs, 1890 (vs, FAB-MS: m\z 968.1 (M, Anal. Caled for C 37H28N4O10Re2 1 ·toluene, C, 41.88; H, 2.66; N, 5.28. Found: C, 41.43; H, 2.71; N
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