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Volumn 74, Issue 14, 2009, Pages 5111-5114

One-pot iodination of hydroxypyridines

Author keywords

[No Author keywords available]

Indexed keywords

CHEMICAL EQUATIONS; CHROMATOGRAPHIC PURIFICATION; HIGH YIELD; HYDROXYQUINOLINES; ONE POT;

EID: 67650401420     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo900726f     Document Type: Article
Times cited : (28)

References (24)
  • 4
    • 2042507954 scopus 로고
    • For a review, see
    • For a review, see: Miyaura, N.; Suzuki, A. Chem. Rev. 1995, 95, 2457-2483.
    • (1995) Chem. Rev , vol.95 , pp. 2457-2483
    • Miyaura, N.1    Suzuki, A.2
  • 6
    • 0000157513 scopus 로고    scopus 로고
    • For reviews, see: a
    • For reviews, see: (a) Buchwald, S. L. Top. Curr. Chem. 2002, 219, 131-209.
    • (2002) Top. Curr. Chem , vol.219 , pp. 131-209
    • Buchwald, S.L.1
  • 7
    • 24144441333 scopus 로고    scopus 로고
    • 2nd ed, De Meijere, A, Diederich, F, Eds, Wiley-VCH: New York
    • (b) Jiang, L.; Buchwald, S. L. In Metal-Catalyzed Cross-Coupling Reactions, 2nd ed.; De Meijere, A., Diederich, F., Eds.; Wiley-VCH: New York, 2004; pp 699-760.
    • (2004) Metal-Catalyzed Cross-Coupling Reactions , pp. 699-760
    • Jiang, L.1    Buchwald, S.L.2
  • 9
  • 16
    • 38849119012 scopus 로고    scopus 로고
    • For examples of the two-step transformation of phenols to aryl iodides via sulfonate esters, see: (a) Wang, Z, Shangguan, N, Cusick, J. R, Williams, L. J. Synlett 2008, 213-216
    • For examples of the two-step transformation of phenols to aryl iodides via sulfonate esters, see: (a) Wang, Z.; Shangguan, N.; Cusick, J. R.; Williams, L. J. Synlett 2008, 213-216.
  • 19
    • 85177097705 scopus 로고    scopus 로고
    • For examples of Brønsted acid activation of pyridines, see: Comins, D. L, Joseph, S. P. In Comprehensive Heterocyclic Chemistry II; Katritzky, A. R, Rees, C. W, Scriven, F. V, McKillop, A, Eds, Pergamon Press: New York, 1996; 5, pp 37-86
    • For examples of Brønsted acid activation of pyridines, see: Comins, D. L.; Joseph, S. P. In Comprehensive Heterocyclic Chemistry II; Katritzky, A. R., Rees, C. W., Scriven, F. V., McKillop, A., Eds.; Pergamon Press: New York, 1996; Vol. 5, pp 37-86.
  • 20
    • 67650488856 scopus 로고    scopus 로고
    • a calculation program from Advanced Chemistry Development, Inc, Version 11.01
    • a calculation program from Advanced Chemistry Development, Inc., Version 11.01).
  • 21
    • 67650495006 scopus 로고    scopus 로고
    • With catalytic acid, the iodination could be pushed to completion with increased temperature (reflux) and reaction time >7 days
    • With catalytic acid, the iodination could be pushed to completion with increased temperature (reflux) and reaction time (>7 days).
  • 22
    • 67650469483 scopus 로고    scopus 로고
    • 13C) analysis.
    • 13C) analysis.
  • 23
    • 67650492053 scopus 로고    scopus 로고
    • Attempts to conduct the one-pot iodination without pyridine were unsuccessful due to incomplete triflate (2a) formation
    • Attempts to conduct the one-pot iodination without pyridine were unsuccessful due to incomplete triflate (2a) formation.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.