Sensitive, selective, precise and accurate LC-MS method for determination of clonidine in human plasma

Chromatographia

Volumn 69, Issue 11-12, 2009, Pages 1227-1232

  Ghosh, Chinmoy ^a   Singh, Rajendra P ^a   Inamdar, Shafi ^a   Mote, Mandar ^a   Chakraborty, Bhaswat S ^a  

^a Cadila Pharmaceuticals Limited   (India)

Author keywords

Clonidine; Column liquid chromatography; Tandem mass spectrometry

Indexed keywords

ACETIC ACID ETHYL ESTER; ACETONITRILE; CARBAMAZEPINE; CLONIDINE; FORMIC ACID; NITROGEN; WATER;

ACCURACY; ADULT; ANALYTIC METHOD; AREA UNDER THE CURVE; ARTICLE; CALIBRATION; CLINICAL TRIAL; CONTROLLED CLINICAL TRIAL; CONTROLLED STUDY; CROSSOVER PROCEDURE; DRUG DETERMINATION; DRUG STRUCTURE; ELECTROSPRAY; EVAPORATION; HUMAN; HUMAN EXPERIMENT; LIQUID CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; MALE; NORMAL HUMAN; PH; PLASMA; PRIORITY JOURNAL; RANDOMIZED CONTROLLED TRIAL; SENSITIVITY AND SPECIFICITY; SINGLE DRUG DOSE; STATISTICAL ANALYSIS; TANDEM MASS SPECTROMETRY; VALIDITY;

EID: 67649989189     PISSN: 00095893     EISSN: 16121112     Source Type: Journal    
DOI: 10.1365/s10337-009-1102-3     Document Type: Article

References (15)

1. National Institute of Neurological Disorders and Stroke (2002) http://www.ninds.nih.gov/news-and-events/news-articles/news-article-adhd.htm
2. Schapiro NA (2002) Dude, you don't have Tourette's: Tourette's syndrome, beyond the tics. Pediatr Nurs. 28: 243-246, 249-253. PMID 12087644
3. Howard S (2008) Illustrated pharmacology memory cards: pharmnemonics. Minireview, 12. ISBN 1-59541-101-1
4. Gourlay SG, Stead LF, Benowitz NL (2004) Clonidine for smoking cessation. Cochrane Database Syst Rev 2004, (2) Art. No.: CD000058. doi: 10.1002/14651858.CD000058.pub2
5. Müller C, Ramic M, Harlfinger S, Hünseler C, Theisohn M, Roth B (2007) J Chromatogr A 1139(2). doi: 10.1016/j.chroma.2006.11.020
6. Gergov M, Ojanperä I, Vuori E (2003) J Chromatogr B 795(1). doi: 10.1016/S1570-0232(03)00498-7
7. Pelzer M, Addison T, Li W, Jiang X, Weng N (2002) J Liq Chromatogr Relat Technol 25(7). doi: 10.1081/JLC-120003421
8. Parekh SA, Pudage A, Joshi SS, Vaidya VV, Gomes NA (2008) J Chromatogr B 867 (2). doi: 10.1016/j.jchromb.2008.03.030
9. Ke GM, Wang L, Xue HY, Lu WL, Zhang X, Zhang Q, Guo HY (2005) Biol Pharm Bull 28
10. Wenzl T, Lankmayr EP, Wintersteiger R, Sadjak A, Likar R, Zakel D (2002) J Biochem Biophys Methods 53(1-3). doi: 10.1016/S0165-022X(02)00101-X
11. Guidance for Industry, Bioanalytical Method Validation (2001) Food and Drug Administration, Center for Drug Evaluation and Research (CDER)
12. VP Shah KK Midha JWA Findlay HM Hill JD Hulse IJ McGilvery G McKay KJ Miller RN Patnaik ML Powel A Tonelli CT Viswanathan A Yacobi 2000 Pharm Res 17 1551 10.1023/A:1007669411738
13. McDoall RD, Hartman C, Penninkx W, Hayden YV, Pankeerberghen V, Massart DL (1995) In: Blume HH, Midha KK bio'94, bio-international 2, bioavailability, bioequivalence and pharmacokinetic studies, Medpharm Scientific, Stuttguart, Germany, p 331
14. NV Nagaraja JK Paliwal RC Gupta 1999 J Pharm Biomed Anal 20 433 10.1016/S0731-7085(98)00256-8
15. AM Almeida MM CastelBranco AC Falcao 2002 J Chromatogr B 774 215 10.1016/S1570-0232(02)00244-1