Near-infrared luminescent properties and natural lifetime calculation of a novel Er3+ complex

Inorganic Chemistry Communications

Volumn 12, Issue 7, 2009, Pages 675-677

  Li, Xiyan ^a   Si, Zhenjun ^a   Pan, Chengling ^a   Zhou, Liang ^a   Li, Zhefeng ^a   Li, Xiaona ^a   Tang, Jinkui ^a   Zhang, Hongjie ^a  

^a CHANGCHUN INSTITUTE OF APPLIED CHEMISTRY   (China)

Author keywords

Er3+ complex; Judd Ofelt theory; NIR luminescence; Optical amplifier

Indexed keywords

EID: 67649361180     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2009.05.022     Document Type: Article

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18. Syntheses: A mixture of PT (30 mmol), a solution of ErCl3 (10 mmol) in ethanol and TPPO (10 mmol) in ethanol (200 mL) was stirred for several minutes until the solids were completely dissolved. This solution was treated with sodium hydroxide (30 mL of 1 mol/L solution), which resulted in the immediate formation of a pale precipitate, and refluxed for 5 h. The pale precipitate was then collected by vacuum filtration, washed with water, and dried under 80 °C to give the product as pale solid (10.10 g, 70%). Calcd. for C81H78ErN6O7P: C, 67.23; H, 5.40; N, 5.81. Found: C, 67.53; H, 5.19; N, 5.68%.
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