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67349169314
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Analytical and spectroscopic data for the representative compound 14DMABAA: Yield 21, EI-MS m/z (rel. int, 451 (6, M+1, 450 (20, M, 240 (100, IR (KBr, cm-1, 2953, 2918, 2850 (C-H aliphatic, 1752 (C{double bond, long}O ester, 1608 (C{double bond, long}N, 1590, 1498 (C{double bond, long}C aromatic, 1H NMR (300 MHz, CDCl3, δ ppm, 0.90 (t, 3H, J, 6.5 Hz, CH3, 1.28-1.42 {m, 20H, CH3(CH2)10, 1.77 (qt, 2H, J, 7.3 Hz, CH2CH2COO, 2.58 (t, 2H, J, 7.4 Hz, CH2COO, 6.74 (d, 2H, J, 8.9 Hz, Ar-H, 7.07 (d, 2H, J, 8.8 Hz, Ar-H, 7.20 (d, 1H, J, 8.8 Hz, Ar-H, 7.76 (d, 1H, J, 8.9, Ar-H, 8.33 (s, 1H, CH{double bond, long}N, 13C NMR (75 MHz, CDCl3 δ ppm, 14.63 (CH3, 23.17, 29.57, 29.74, 29.83, 29.93, 30.06, 30.11, 30.14, 32.38 for methylene carbons (CH3(CH2)10
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2: C, 77.29%, H, 9.39%, N, 6.22%; found: C, 77.37%, H, 9.47%, N, 6.16%.
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20
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12344286973
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Han S.H., Yoshida H., Nobe Y., Fujiwara M., Kamizori J., Kikuchi A., Iwahori F., and Abe J. J. Mol. Struct. 735/736 (2005) 375
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Han, S.H.1
Yoshida, H.2
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Fujiwara, M.4
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Kikuchi, A.6
Iwahori, F.7
Abe, J.8
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