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2
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17444392475
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Piel J., Butzke D., Fusetani D., Hui D., Platzer M., Wen G., and Matsunaga S. J. Nat. Prod. 68 (2005) 472
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Piel, J.1
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7
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0037025953
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Takemura T., Nishii Y., Takahashi S., Kobayashi J., and Nakata T. Tetrahedron 58 (2002) 6359
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, pp. 6359
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Takemura, T.1
Nishii, Y.2
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Kobayashi, J.4
Nakata, T.5
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9
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0001212549
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(1990)
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, vol.46
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Willson, T.M.1
Kocienski, P.2
Jarowicki, K.3
Isaac, K.4
Faller, A.5
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10
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0000476198
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14
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34547153679
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(2007)
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Huang, X.1
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Aslanian, R.4
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15
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46449128747
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(2008)
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Liu, D.1
Xue, J.2
Xie, Z.3
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Zhang, X.5
Li, Y.6
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20
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-
2542489323
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(2004)
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Kang, A.1
Kang, S.Y.2
Choi, H.W.3
Kim, C.M.4
Jun, H.S.5
Younb, J.H.6
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22
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-
67349274872
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-
3, δ ppm): 138.7, 128.3, 127.5, 127.4, 81.8, 77.9, 76.2, 74.1, 72.1, 71.5, 59.2, 56.9, 37.2, 31.3, 29.9, 22.7, 19.7, 10.3; MS (EI) m/z: 430, 417, 385, 359, 303, 253, 223, 197, 169, 91.
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3, δ ppm): 138.7, 128.3, 127.5, 127.4, 81.8, 77.9, 76.2, 74.1, 72.1, 71.5, 59.2, 56.9, 37.2, 31.3, 29.9, 22.7, 19.7, 10.3; MS (EI) m/z: 430, 417, 385, 359, 303, 253, 223, 197, 169, 91.
-
-
-
-
25
-
-
67349112300
-
-
+) 375.2142, found 375.2136.
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+) 375.2142, found 375.2136.
-
-
-
-
26
-
-
67349153265
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-
Data of compound 2b: [α]20D -26 (c 1.0, CHCl3, 1H NMR (300 MHz, CDCl3, δ ppm, 7.33 (m, 5H, ArH, 4.62 (d, 1H, J, 11.7 Hz, ArCH2O, 4.40 (d, 1H, J, 11.7 Hz, ArCH2O, 3.64 (t, 1H, J, 6.0 Hz, 3.35 (m, 10H, 3.22 (s, 1H, 2.95 (d, 1H, J, 8.4 Hz, CH2N, 2.86 (d, 1H, J, 8.4 Hz,CH2N, 2.73 (s, 6H, NMe2, 1.72 (m, 1H, 1.59 (m, 3H, 0.86 (s, 3H, CMe2, 0.84 (s, 3H, CMe2, 13C NMR (75 MHz, CDCl3, δ ppm, 138.5, 128.3, 127.7, 127.6, 80.8, 78.5, 76.6, 73.9, 71.6, 68.3, 61.6, 59.2, 56.9, 43.9, 37.1, 30.9, 29.6, 29.2, 23.0, 19.5; MS (EI, 379, 364, 348, 334, 318, 288, 121, 91, 58; HRMS calcd for C22H38NO4 M, H, 380.2795, found 380.2793
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+) 380.2795, found 380.2793.
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