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Volumn 20, Issue 7, 2009, Pages 775-778

Asymmetric synthesis of pedamide using I2-induced heterocyclization to construct the skeleton

Author keywords

Pedamide; Pederin; Synthesis

Indexed keywords


EID: 67349146998     PISSN: 10018417     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cclet.2009.03.026     Document Type: Article
Times cited : (2)

References (27)
  • 22
    • 67349274872 scopus 로고    scopus 로고
    • 3, δ ppm): 138.7, 128.3, 127.5, 127.4, 81.8, 77.9, 76.2, 74.1, 72.1, 71.5, 59.2, 56.9, 37.2, 31.3, 29.9, 22.7, 19.7, 10.3; MS (EI) m/z: 430, 417, 385, 359, 303, 253, 223, 197, 169, 91.
    • 3, δ ppm): 138.7, 128.3, 127.5, 127.4, 81.8, 77.9, 76.2, 74.1, 72.1, 71.5, 59.2, 56.9, 37.2, 31.3, 29.9, 22.7, 19.7, 10.3; MS (EI) m/z: 430, 417, 385, 359, 303, 253, 223, 197, 169, 91.
  • 25
    • 67349112300 scopus 로고    scopus 로고
    • +) 375.2142, found 375.2136.
    • +) 375.2142, found 375.2136.
  • 26
    • 67349153265 scopus 로고    scopus 로고
    • Data of compound 2b: [α]20D -26 (c 1.0, CHCl3, 1H NMR (300 MHz, CDCl3, δ ppm, 7.33 (m, 5H, ArH, 4.62 (d, 1H, J, 11.7 Hz, ArCH2O, 4.40 (d, 1H, J, 11.7 Hz, ArCH2O, 3.64 (t, 1H, J, 6.0 Hz, 3.35 (m, 10H, 3.22 (s, 1H, 2.95 (d, 1H, J, 8.4 Hz, CH2N, 2.86 (d, 1H, J, 8.4 Hz,CH2N, 2.73 (s, 6H, NMe2, 1.72 (m, 1H, 1.59 (m, 3H, 0.86 (s, 3H, CMe2, 0.84 (s, 3H, CMe2, 13C NMR (75 MHz, CDCl3, δ ppm, 138.5, 128.3, 127.7, 127.6, 80.8, 78.5, 76.6, 73.9, 71.6, 68.3, 61.6, 59.2, 56.9, 43.9, 37.1, 30.9, 29.6, 29.2, 23.0, 19.5; MS (EI, 379, 364, 348, 334, 318, 288, 121, 91, 58; HRMS calcd for C22H38NO4 M, H, 380.2795, found 380.2793
    • +) 380.2795, found 380.2793.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.