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Volumn 37, Issue 11, 2008, Pages 1108-1109

Guest entrapment via type and size of dibenzo-monoaza-crowns-based N,N-bis(alkyl-2-hydroxybenzyl)alkylamine host

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EID: 67149093804 PISSN: 03667022 EISSN: 13480715 Source Type: Journal
DOI: 10.1246/cl.2008.1108 Document Type: Article

Times cited : (7)

References (14)

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- Spectroscopic results of macrocycles 4-6 were shown as follows. 4: 80% yield; mp 124.5 °C; FTIR (KBr, cm1, 1480 (vs, tri-substituted benzene, 1213 (vs. C-N stretching, 1053 (s, C-O-C, 1 H NMR (400 MHz, CDCl3, δH 1.94 (3H, s, N-CH3, 2.11 (2H, t, CH2-CH2-CH2, 2.25 (12H, s, Ar-CH3, 3.62 (4H, s, Ar-CH2-N, 4.11 (4H, t, Ar-O-CH2, 6.79 (2H, s. Ar-H, 6.91 (2H, s, Ar-H, MALDI-TOF MS: m/z 340.23 [M+H, Anal. Calcd for C22H 29NO2: C, 77.84; H, 8.61; N, 4.13, Found: C, 77.63; H, 8.40; N, 4.12, 5: 76% yield; mp 172.8°C; FTIR (KBr, cm -1, 1481 (vs, tri-substituted benzene, 1213 (vs, C-N stretching, 1076 (s, C-O-C, 1HNMR (400MHz, CDCl3, δH 1.96 (3H, s, N-CH3, 2.00 (4H, t, O-CH 2-CH2, 2.25 15H, s, Ar-CH3
- 3: C, 75.53; H, 8.87; N, 3.52%. Found: C, 75.24; H, 8.76; N, 3.49%.

11
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- Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication number CCDC 671193 (4), 671194 (5), 692237 (6), and 692236 (7). Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html.
- Crystallographic data reported in this manuscript have been deposited with Cambridge Crystallographic Data Centre as supplementary publication number CCDC 671193 (4), 671194 (5), 692237 (6), and 692236 (7). Copies of the data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html.

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