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66249087154
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Hydrazine 11 and (S)-ethyl butyrate were not readily available in bulk quantities at the time of this work.
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Hydrazine 11 and (S)-ethyl butyrate were not readily available in bulk quantities at the time of this work.
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66249131531
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The low temperature for crystallization was required due to the low melting point of 27.
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The low temperature for crystallization was required due to the low melting point of 27.
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66249140121
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The use of higher concentrations of substrates 33 and 34 in the presence of acid resulted in substantial polymerization to polyester-type products.
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The use of higher concentrations of substrates 33 and 34 in the presence of acid resulted in substantial polymerization to polyester-type products.
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51
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66249119903
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Optical purity of 9 was 93% starting from 10 at 94% ee.
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Optical purity of 9 was 93% starting from 10 at 94% ee.
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