Synthesis and characterization of two new fac-tricarbonylrhenium(i) biscarbene complexes

European Journal of Inorganic Chemistry

Volumn , Issue 13 SPEC. ISS., 2009, Pages 1825-1831

  Hiltner, Oliver ^a   Herdtweck, Eberhardt ^a   Drees, Markus ^a   Herrmann, Wolfgang A ^a   Kühn, Fritz E ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

Author keywords

Carbenes; Carbonyl ligands; Imidazole; N Heterocyclic carbenes; Rhenium

Indexed keywords

CHELATION; LIGANDS; ORGANIC COMPOUNDS; SYNTHESIS (CHEMICAL); X RAY DIFFRACTION;

BIS-CARBENE; CARBENES; CARBONYL LIGAND; IMIDAZOL; IMIDAZOLINES; METAL PRECURSOR; N-HETEROCYCLIC CARBENES; SYNTHESIS AND CHARACTERIZATIONS; X- RAY DIFFRACTIONS;

RHENIUM COMPOUNDS;

EID: 66149168824     PISSN: 14341948     EISSN: 10990682     Source Type: Journal    
DOI: 10.1002/ejic.200801164     Document Type: Article

References (39)

1. K. Öfele, J. Organomet. Chem.1968, 12, 42-43;
2. H.-W. Wanzlick, H. J. SchÖnherr, Angew. Chem. 1968, 80, 154-154;
3. Angew. Chem. Int. Ed. Engl. 1968, 7, 141-142.
4. A. J. Arduengo III, R. L. Harlow, M. Kline, J. Am. Chem. Soc. 1991, 113, 361-363.
5. W. A. Herrmann, Angew. Chem. Int. Ed.2002, 41, 1290-1309;
6. E. A. B. Kantchev, C. J. O'Brien, M. G. Organ, Angew. Chem. Int. Ed. 2007, 46, 2768-2813;
7. S. Díez-González, S. P. Nolan, Coord. Chem. Rev. 2007, 251, 874-883.
8. W. A. Herrmann, K. Öfele, M. Elison, F. E. Kühn, P. W. Roesky, J. Organomet. Chem. 1994,480, C7-C9;
9. K. R. Jain,W. A. Herrmann, F. E. Kühn, Curr. Org. Chem. 2008, 12, 1468-1478.
10. H. Braband, T. I. Zahn, U. Abram, Inorg. Chem.2003, 42, 6160-6162;
11. T. I. Kückmann, U. Abram, Inorg. Chem.2004, 43, 7068-7074;
12. H. Braband, D. Przyrembel, U. Abram, Z. Anorg. Allg. Chem.2006, 632, 779-785;
13. H. Braband, E. Oehlke, U. Abram, Z. Anorg. Allg. Chem.2006, 632, 1051-1056;
14. E. Oehlke, T. Kückmann, U. Abram, Z. Anorg. Allg. Chem. 2007, 633, 830-834.
15. C.-Y. Liu, D.-Y. Chen, G.-H. Lee, S.-M. Peng, S.-T. Liu, Organometallics 1996, 15, 1055-1061;
16. W.-M. Xue, M. C.-W. Chan, Z.-M. Su, K.-K. Cheung, S.-T. Liu, C.-M. Che, Organo-metallics 1998, 17, 1622-1630.
17. O. Kaufhold, A. Stasch, P. G. Edwards, F. E. Hahn, Chem. Commun. 2007, 1822-1824.
18. W. A. Herrmann, D. Mihalios, K. Ofele, P. Kiprof, F. Belmedjahed, Chem. Ber.1992, 125, 1795-1799;
19. M. A. Huertos, J. Ṕrez, L. Riera, A. Meńndez- Velázquez, J. Am. Chem. Soc. 2008, 130, 13530-13531.
20. A. J. Arduengo III, US 5077414, 1991.
21. R. Alberto, R. Schibli, A. Egli, A. Schubiger, W. A. Herrm-ann, G. Artus, U. Abram, T. A. Kaden, J. Organomet. Chem.1995, 493, 119-127;
22. R. Alberto, A. Egli, U. Abram, K. Heg-etschweiler, V. Gramlich, P. A. Schubiger, J. Chem. Soc., Dalton Trans. 1994, 2815-2820.
23. APEX suite of crystallographic software. APEX 2 Version 2008.4. Bruker AXS Inc.,Madison, WI, USA, 2008;
24. SAINT,Version 7.56a and SADABS Version 2008/1. Bruker AXS Inc.,Madison, WI, USA, 2008;
25. SIR97, a new tool for crystalstructure determination and refinement: A. Altomare, G. Cas-carano, C. Giacovazzo, A. Guagliardi, G. G. Moliterni,A. M. C. Burla, G. Polidori, M. Camalli, R. Spagna, J. Appl. Crystallogr. 1999, 32, 115-119;
26. A. J. C. Wilson (Ed.), Inter-national Tables for Crystallography, Kluwer Academic Publish-ers, Dordrecht, The Netherlands, 1992, vol. C, Tables 6.1.1.4(pp. 500-502), 4.2.6.8 (pp. 219-222), and 4.2.4.2 (pp. 193-199);
27. G. M. Sheldrick, SHELXL-97, University of GÖttingen, GÖttingen, Germany, 1998;
28. A. L. Spek, PLATON, A Multi-purpose Crystallographic Tool, Utrecht University, Utrecht,The Netherlands, 2007;
29. WinGX, Version 1.70.01, January 2005: L. J. Farrugia, J. Appl. Crystallogr. 1999, 32, 837-838;
30. K. Brandenburg, Version 3.1d, Crystal Impact GbR,Bonn, Germany, 2006.
31. M. J. Frisch, G. W. Trucks, H. B. Schlegel, G. E. Scuseria,M. A. Robb, J. R. Cheeseman, J. Montgomery, J. A. T. Vreven,K. N. Kudin, J. C. Burant, J. M. Millam, S. S. Iyengar, J. Tom-asi, V. Barone, B. Mennucci, M. Cossi, G. Scalmani, N. Rega,G. A. Petersson, H. Nakatsuji, M. Hada, M. Ehara, K. Toyota,R. Fukuda, J. Hasegawa, M. Ishida, T. Nakajima, Y. Honda,O. Kitao, H. Nakai, M. Klene, X. Li, J. E. Knox, H. P. Hratch-ian, J. B. Cross, V. Bakken, C. Adamo, J. Jaramillo, R. Gom-perts, R. E. Stratmann, O. Yazyev, A. J. Austin, R. Cammi, C. Pomelli, J. W. Ochterski, P. Y. Ayala, K. Morokuma, G. A. Voth, P. Salvador, J. J. Dannenberg, V. G. Zakrzewski, S. Dap-prich, A. D. Daniels, M. C. Strain, O. Farkas, D. K. Malick,A. D. Rabuck, K. Raghavachari, J. B. Foresman, J. V. Ortiz, Q. Cui, A. G. Baboul, S. Clifford, J. Cioslowski, B. B. Stefanov,G. Liu, A. Liashenko, P. Piskorz, I. Komaromi, R. L. Martin,D. J. Fox, T. Keith, M. A. Al-Laham, C. Y. Peng, A. Nanayak-kara, M. Challacombe, P. M. W. Gill, B. Johnson, W. Chen,M. W. Wong, C. Gonzalez, J. A. Pople, Gaussian03, RevisionC.02, Gaussian, Inc., Wallingford, CT, 2004.
32. S H. Vosko, L. Wilk, M. Nusair, Can. J. Phys. 1980, 58,1200-1211;
33. C. Lee, W. Yang, R. G. Parr, Phys. Rev. B 1988,37, 785-789;
34. A. D. Becke, J. Chem. Phys. 1993, 98, 5648-5652.
35. W. J. Hehre, R. Ditchfield, J. A. Pople, J. Chem. Phys. 1972, 56, 2257-2261;
36. M. M. Francl, W. J. Petro, W. J. Hehre, J. S. Binkley, M. S. Gordon, D. J. DeFrees, J. A. Pople, J. Chem. Phys. 1982, 77, 3654-3665.
37. P. J. Hay, W. R. Wadt, J. Chem. Phys. 1985, 82, 270-283;
38. P. J. Hay, W. R. Wadt, J. Chem. Phys. 1985, 82, 299-310.
39. J. W. Ponder, TINKER - Tools for Molecular Design, Version4.2, June, 2004, source code: http://dasher.wustl.edu/tinker/.